Characterization of polar polycyclic aromatic compounds in a heavy-duty diesel exhaust particulate by capillary column gas chromatography and high-resolution mass spectrometry
Polar normal-phase HPLC fractions of a heavy-duty diesel exhaust particulate, a National Bureau of Standards (NBS) standard reference material (SRM) 1650, were analyzed by capillary column GC coupled to both low- and high resolution mass spectrometry (HRMS) using electron impact (EI) and negative io...
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| Veröffentlicht in: | Environ. Sci. Technol.; (United States) 1988-12, Vol.22 (12), p.1440-1447 |
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| container_title | Environ. Sci. Technol.; (United States) |
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| creator | Bayona, Jose M Markides, Karin E Lee, Milton L |
| description | Polar normal-phase HPLC fractions of a heavy-duty diesel exhaust particulate, a National Bureau of Standards (NBS) standard reference material (SRM) 1650, were analyzed by capillary column GC coupled to both low- and high resolution mass spectrometry (HRMS) using electron impact (EI) and negative ion chemical ionization (NICI). Over 80 polycyclic aromatic compounds (PAC), belonging to many different chemical classes (anhydrides, carboxaldehydes, diazaarenes cyclic imides, nitrohydroxy-PAC, nitroaza-PAC, nitrodiaza-PAC, nitrolactones, and quinones) were tentatively identified. Ten of them were positively identified by comparison of retention times with authentic standards. |
| doi_str_mv | 10.1021/es00177a009 |
| format | Article |
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Over 80 polycyclic aromatic compounds (PAC), belonging to many different chemical classes (anhydrides, carboxaldehydes, diazaarenes cyclic imides, nitrohydroxy-PAC, nitroaza-PAC, nitrodiaza-PAC, nitrolactones, and quinones) were tentatively identified. 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Sci. Technol.; (United States)</title><addtitle>Environ. Sci. Technol</addtitle><description>Polar normal-phase HPLC fractions of a heavy-duty diesel exhaust particulate, a National Bureau of Standards (NBS) standard reference material (SRM) 1650, were analyzed by capillary column GC coupled to both low- and high resolution mass spectrometry (HRMS) using electron impact (EI) and negative ion chemical ionization (NICI). Over 80 polycyclic aromatic compounds (PAC), belonging to many different chemical classes (anhydrides, carboxaldehydes, diazaarenes cyclic imides, nitrohydroxy-PAC, nitroaza-PAC, nitrodiaza-PAC, nitrolactones, and quinones) were tentatively identified. 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Sci. Technol.; (United States)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bayona, Jose M</au><au>Markides, Karin E</au><au>Lee, Milton L</au><aucorp>Brigham Young Univ., Provo, UT (USA)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterization of polar polycyclic aromatic compounds in a heavy-duty diesel exhaust particulate by capillary column gas chromatography and high-resolution mass spectrometry</atitle><jtitle>Environ. Sci. Technol.; (United States)</jtitle><addtitle>Environ. Sci. Technol</addtitle><date>1988-12-01</date><risdate>1988</risdate><volume>22</volume><issue>12</issue><spage>1440</spage><epage>1447</epage><pages>1440-1447</pages><issn>0013-936X</issn><eissn>1520-5851</eissn><coden>ESTHAG</coden><abstract>Polar normal-phase HPLC fractions of a heavy-duty diesel exhaust particulate, a National Bureau of Standards (NBS) standard reference material (SRM) 1650, were analyzed by capillary column GC coupled to both low- and high resolution mass spectrometry (HRMS) using electron impact (EI) and negative ion chemical ionization (NICI). Over 80 polycyclic aromatic compounds (PAC), belonging to many different chemical classes (anhydrides, carboxaldehydes, diazaarenes cyclic imides, nitrohydroxy-PAC, nitroaza-PAC, nitrodiaza-PAC, nitrolactones, and quinones) were tentatively identified. Ten of them were positively identified by comparison of retention times with authentic standards.</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><pmid>22200471</pmid><doi>10.1021/es00177a009</doi><tpages>8</tpages></addata></record> |
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| source | ACS Publications |
| subjects | 500200 - Environment, Atmospheric- Chemicals Monitoring & Transport- (-1989) AIR POLLUTION Analysis methods Applied sciences AROMATICS Atmospheric pollution CHEMICAL COMPOSITION CHROMATOGRAPHY DATA DIESEL ENGINES ENGINES ENVIRONMENTAL SCIENCES Exact sciences and technology EXHAUST GASES EXPERIMENTAL DATA FLUIDS GAS CHROMATOGRAPHY GASEOUS WASTES GASES HEAT ENGINES HYDROCARBONS INFORMATION INTERNAL COMBUSTION ENGINES MASS SPECTROSCOPY NUMERICAL DATA ORGANIC COMPOUNDS PARTICLES PARTICULATES POLLUTION POLYCYCLIC AROMATIC HYDROCARBONS SEPARATION PROCESSES SPECTROSCOPY WASTES |
| title | Characterization of polar polycyclic aromatic compounds in a heavy-duty diesel exhaust particulate by capillary column gas chromatography and high-resolution mass spectrometry |
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