Identification of Epoxide Functionalities in Protonated Monofunctional Analytes by Using Ion/Molecule Reactions and Collision-Activated Dissociation in Different Ion Trap Tandem Mass Spectrometers

A mass spectrometric method has been delineated for the identification of the epoxide functionalities in unknown monofunctional analytes. This method utilizes gas-phase ion/molecule reactions of protonated analytes with neutral trimethyl borate (TMB) followed by collision-activated dissociation (CAD...

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Veröffentlicht in:	Journal of the American Society for Mass Spectrometry 2012-01, Vol.23 (1), p.12-22
Hauptverfasser:	Eismin, Ryan J., Fu, Mingkun, Yem, Sonoeun, Widjaja, Fanny, Kenttämaa, Hilkka I.
Format:	Artikel
Sprache:	eng
Schlagworte:	Amides Analytical Chemistry Basic oxides Bioinformatics Biotechnology Borates - chemistry Carbonyls Carboxylic acids Cascade chemical reactions catalysis (homogeneous), catalysis (heterogeneous), biofuels (including algae and biomass), bio-inspired, materials and chemistry by design, synthesis (self-assembly), synthesis (scalable processing) Chemistry Chemistry and Materials Science Cyclotron resonance Diagnostic systems Epoxy Compounds - chemistry Ethyl Ethers - chemistry Exact sciences and technology Fourier Analysis Identification Ions Ions - chemistry Mass spectrometers Mass spectrometry Methanol Methanol - chemistry Organic Chemistry Oxygen - chemistry Propylene Propylene oxide Proteomics Protons Quadrupoles Reactivity and mechanisms Research Article Spectrometers Spectrometry Tandem Mass Spectrometry - instrumentation Tandem Mass Spectrometry - methods
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