Mechanosynthesis and magnetic characterization of nanocrystalline manganese ferrites

Manganese ferrites, MnFe 2 O 4±δ , synthesized via mechanosynthesis from different manganese sources, MnO, Mn 2 O 3 and MnO 2 , and mixed with Fe 2 O 3 , were studied. XRD, SEM and magnetometry were used to characterize the synthesized powders. The MnFe 2 O 4 spinel phase appeared after 12 h of mill...

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Veröffentlicht in:Journal of materials science. Materials in electronics 2011-08, Vol.22 (8), p.1046-1052
Hauptverfasser: Bolarín-Miró, Ana M., Vera-Serna, Pedro, Sánchez-De Jesús, Félix, Cortés-Escobedo, Claudia A., Martínez-Luevanos, Antonia
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container_end_page 1052
container_issue 8
container_start_page 1046
container_title Journal of materials science. Materials in electronics
container_volume 22
creator Bolarín-Miró, Ana M.
Vera-Serna, Pedro
Sánchez-De Jesús, Félix
Cortés-Escobedo, Claudia A.
Martínez-Luevanos, Antonia
description Manganese ferrites, MnFe 2 O 4±δ , synthesized via mechanosynthesis from different manganese sources, MnO, Mn 2 O 3 and MnO 2 , and mixed with Fe 2 O 3 , were studied. XRD, SEM and magnetometry were used to characterize the synthesized powders. The MnFe 2 O 4 spinel phase appeared after 12 h of milling when MnO and MnO 2 mixed with Fe 2 O 3 were used as the precursors and showed the maximum saturation magnetization value (49.77 emu/g). Manganese ferrite did not form when MnO 2 was used. Manganese ferrite obtained from Mn 2 O 3 showed the lowest saturation magnetization value. An increase in the milling time promoted the increase in the saturation magnetization values.
doi_str_mv 10.1007/s10854-010-0257-x
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XRD, SEM and magnetometry were used to characterize the synthesized powders. The MnFe 2 O 4 spinel phase appeared after 12 h of milling when MnO and MnO 2 mixed with Fe 2 O 3 were used as the precursors and showed the maximum saturation magnetization value (49.77 emu/g). Manganese ferrite did not form when MnO 2 was used. Manganese ferrite obtained from Mn 2 O 3 showed the lowest saturation magnetization value. An increase in the milling time promoted the increase in the saturation magnetization values.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-010-0257-x</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Applied sciences ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Cross-disciplinary physics: materials science; rheology ; Deltas ; Domain effects, magnetization curves, and hysteresis ; Electronics ; Exact sciences and technology ; Ferrites ; Instruments, apparatus, components and techniques common to several branches of physics and astronomy ; Magnetic properties and materials ; Magnetization curves, magnetization reversal, hysteresis, barkhausen and related effects ; Manganese ; Materials Science ; Materials synthesis; materials processing ; Metals. 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XRD, SEM and magnetometry were used to characterize the synthesized powders. The MnFe 2 O 4 spinel phase appeared after 12 h of milling when MnO and MnO 2 mixed with Fe 2 O 3 were used as the precursors and showed the maximum saturation magnetization value (49.77 emu/g). Manganese ferrite did not form when MnO 2 was used. Manganese ferrite obtained from Mn 2 O 3 showed the lowest saturation magnetization value. An increase in the milling time promoted the increase in the saturation magnetization values.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10854-010-0257-x</doi><tpages>7</tpages></addata></record>
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subjects Applied sciences
Characterization and Evaluation of Materials
Chemistry and Materials Science
Condensed matter: electronic structure, electrical, magnetic, and optical properties
Cross-disciplinary physics: materials science
rheology
Deltas
Domain effects, magnetization curves, and hysteresis
Electronics
Exact sciences and technology
Ferrites
Instruments, apparatus, components and techniques common to several branches of physics and astronomy
Magnetic properties and materials
Magnetization curves, magnetization reversal, hysteresis, barkhausen and related effects
Manganese
Materials Science
Materials synthesis
materials processing
Metals. Metallurgy
Nanocrystals
Optical and Electronic Materials
Physics
Powder metallurgy. Composite materials
Precursors
Production techniques
Saturation
Saturation (magnetic)
Scanning probe microscopes, components and techniques
Spinel
Technology
title Mechanosynthesis and magnetic characterization of nanocrystalline manganese ferrites
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