Characterization of nano-crystalline ZrO2 synthesized via reactive plasma processing
Nano-crystalline ZrO2 powder has been synthesized via reactive plasma processing. The synthesized ZrO2 powders were characterized by X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM) and FTIR spectroscopy. The synthesized powder consists of a mixture of tetragonal a...
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| Veröffentlicht in: | Materials science & engineering. B, Solid-state materials for advanced technology Solid-state materials for advanced technology, 2011-07, Vol.176 (12), p.894-899 |
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| container_title | Materials science & engineering. B, Solid-state materials for advanced technology |
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| creator | Jayakumar, S Ananthapadmanabhan, P V Perumal, K Thiyagarajan, T K Mishra, S C Su, L T Tok, AIY Guo, J |
| description | Nano-crystalline ZrO2 powder has been synthesized via reactive plasma processing. The synthesized ZrO2 powders were characterized by X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM) and FTIR spectroscopy. The synthesized powder consists of a mixture of tetragonal and monoclinic phases of zirconia. Average crystallite size calculated from the XRD pattern shows that particles with crystallite size 20nm or less than 20nm are in tetragonal phase, whereas particles greater than 20nm are in the monoclinic phase. TEM results show that particles have spherical morphology with maximum percentage of particles distributed in a narrow size from about 15nm to 30nm. |
| doi_str_mv | 10.1016/j.mseb.2011.05.013 |
| format | Article |
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TEM results show that particles have spherical morphology with maximum percentage of particles distributed in a narrow size from about 15nm to 30nm.</description><subject>Crystallites</subject><subject>Diffraction</subject><subject>Mathematical analysis</subject><subject>Nanocrystals</subject><subject>Phases</subject><subject>Plasma processing</subject><subject>Transmission electron microscopy</subject><subject>Zirconium dioxide</subject><issn>0921-5107</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp9kDtPwzAUhT2ARHn8ASZvsCRcv-JkRBUvqVKXsrBYjn1DXeVR7LRS--tJVWams3znHOkj5J5BzoAVT5u8S1jnHBjLQeXAxAWZQcVZphjoK3Kd0gYAGOd8RlbztY3WjRjD0Y5h6OnQ0N72Q-biIY22bUOP9CsuOU2HflxjCkf0dB8sjTj1wh7ptrWps3QbB4cphf77llw2tk1495c35PP1ZTV_zxbLt4_58yJzQpdjpgqpvagFeFtaXUul6hoZ8EIKVTJR-sIrWVeulhUW1nulJTIGUnnPy8Y7cUMezrvT9c8O02i6kBy2re1x2CVTga6klCVM5OO_JNMFZ1wXVTmh_Iy6OKQUsTHbGDobD4aBOQk2G3MSbE6CDSgzCRa_pzZyqw</recordid><startdate>20110725</startdate><enddate>20110725</enddate><creator>Jayakumar, S</creator><creator>Ananthapadmanabhan, P V</creator><creator>Perumal, K</creator><creator>Thiyagarajan, T K</creator><creator>Mishra, S C</creator><creator>Su, L T</creator><creator>Tok, AIY</creator><creator>Guo, J</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20110725</creationdate><title>Characterization of nano-crystalline ZrO2 synthesized via reactive plasma processing</title><author>Jayakumar, S ; Ananthapadmanabhan, P V ; Perumal, K ; Thiyagarajan, T K ; Mishra, S C ; Su, L T ; Tok, AIY ; Guo, J</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c378t-5647d3b30da8a7b455bbe10264358138d6d54b9cb49e6add574e11045dd28fdc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Crystallites</topic><topic>Diffraction</topic><topic>Mathematical analysis</topic><topic>Nanocrystals</topic><topic>Phases</topic><topic>Plasma processing</topic><topic>Transmission electron microscopy</topic><topic>Zirconium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jayakumar, S</creatorcontrib><creatorcontrib>Ananthapadmanabhan, P V</creatorcontrib><creatorcontrib>Perumal, K</creatorcontrib><creatorcontrib>Thiyagarajan, T K</creatorcontrib><creatorcontrib>Mishra, S C</creatorcontrib><creatorcontrib>Su, L T</creatorcontrib><creatorcontrib>Tok, AIY</creatorcontrib><creatorcontrib>Guo, J</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Materials science & engineering. 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| ispartof | Materials science & engineering. B, Solid-state materials for advanced technology, 2011-07, Vol.176 (12), p.894-899 |
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| language | eng |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Crystallites Diffraction Mathematical analysis Nanocrystals Phases Plasma processing Transmission electron microscopy Zirconium dioxide |
| title | Characterization of nano-crystalline ZrO2 synthesized via reactive plasma processing |
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