Investigation of the mechanism of self-propagating high-temperature synthesis of TiNi

An improved combustion front quenching method was used to investigate the mechanism of self-propagating high-temperature synthesis (SHS) of TiNi from Ti and Ni powders. The microstructural evolution in the quenched sample was observed with scanning electron microscope (SEM) and analyzed with energy...

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Veröffentlicht in:Journal of materials science 2011-04, Vol.46 (8), p.2437-2444
Hauptverfasser: Che, Han-Qing, Ma, Yan, Fan, Qun-Cheng
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Ma, Yan
Fan, Qun-Cheng
description An improved combustion front quenching method was used to investigate the mechanism of self-propagating high-temperature synthesis (SHS) of TiNi from Ti and Ni powders. The microstructural evolution in the quenched sample was observed with scanning electron microscope (SEM) and analyzed with energy dispersive X-ray spectrometry. Also, the combustion temperature of the reaction was measured, and the phase constituent of the synthesized product was inspected by X-ray diffraction. Based on those experimental results, a dissolution–precipitation–diffusion mechanism was proposed and compared with those mechanisms concluded by other authors, thus the mechanism for the SHS of TiNi was systematically discussed. In addition, the influence and necessity of pre-heating before the ignition was discussed.
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subjects Characterization and Evaluation of Materials
Chemistry and Materials Science
Classical Mechanics
Combustion temperature
Crystallography and Scattering Methods
Diffraction
Electron microscopes
High temperature
Intermetallic compounds
Intermetallics
Investigations
Materials Science
Nickel base alloys
Nickel compounds
Nickel titanides
Polymer Sciences
Powders
Precipitation (Meteorology)
Scanning electron microscopy
Self propagating high temperature synthesis
Self-propagating synthesis
Shape memory alloys
Solid Mechanics
Titanium compounds
X-rays
title Investigation of the mechanism of self-propagating high-temperature synthesis of TiNi
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