Continuous synthesis of carbon-encapsulated magnetic nanoparticles with a minimum production of amorphous carbon

The continuous synthesis of carbon-encapsulated magnetic nanoparticles is described using an inductively coupled radio frequency thermal plasma torch. The synthesis uses the simultaneous vaporization of iron powder and a liquid carbon source in the plasma jet. It was found that the process parameter...

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Veröffentlicht in:Carbon (New York) 2009-07, Vol.47 (8), p.2040-2048
Hauptverfasser: Bystrzejewski, M., Karoly, Z., Szepvolgyi, J., Kaszuwara, W., Huczko, A., Lange, H.
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container_end_page 2048
container_issue 8
container_start_page 2040
container_title Carbon (New York)
container_volume 47
creator Bystrzejewski, M.
Karoly, Z.
Szepvolgyi, J.
Kaszuwara, W.
Huczko, A.
Lange, H.
description The continuous synthesis of carbon-encapsulated magnetic nanoparticles is described using an inductively coupled radio frequency thermal plasma torch. The synthesis uses the simultaneous vaporization of iron powder and a liquid carbon source in the plasma jet. It was found that the process parameters could be adjusted to minimize the amorphous carbon content in the product. It could be achieved using either aliphatic alcohols (processed in Ar plasma) or hydrocarbons (processed in Ar–O 2 plasma). In such circumstances the oxygen etches any amorphous carbon particles produced. Complete reduction of amorphous carbon was achieved when ethanol was used as a carbon feedstock.
doi_str_mv 10.1016/j.carbon.2009.03.054
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subjects Chemistry
Colloidal state and disperse state
Cross-disciplinary physics: materials science
rheology
Exact sciences and technology
Fullerenes and related materials
diamonds, graphite
General and physical chemistry
Materials science
Physical and chemical studies. Granulometry. Electrokinetic phenomena
Physics
Specific materials
title Continuous synthesis of carbon-encapsulated magnetic nanoparticles with a minimum production of amorphous carbon
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