A study on hydrogen-storage behaviors of nickel-loaded mesoporous MCM-41
The hydrogen-storage capacities of the Ni/MCM-41 as a function of Ni content are described. The objective of the present work was to investigate the possibility of improving the hydrogen-storage capacity of mesoporous MCM-41 containing nickel (Ni) oxides (Ni/MCM-41). The MCM-41 and Ni/MCM-41 were pr...
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| Veröffentlicht in: | Journal of colloid and interface science 2010-06, Vol.346 (1), p.194-198 |
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| creator | Park, Soo-Jin Lee, Seul-Yi |
| description | The hydrogen-storage capacities of the Ni/MCM-41 as a function of Ni content are described.
The objective of the present work was to investigate the possibility of improving the hydrogen-storage capacity of mesoporous MCM-41 containing nickel (Ni) oxides (Ni/MCM-41). The MCM-41 and Ni/MCM-41 were prepared using a hydrothermal process as a function of Ni content (2, 5, and 10
wt.% in the MCM-41). The surface functional groups of the Ni/MCM-41 were identified by Fourier transform infrared spectroscopy (FTIR). The structure and morphology of the Ni/MCM-41 were characterized by X-ray diffraction (XRD) and field emission transmission electron microscopy (FE-TEM). XRD results showed a well-ordered hexagonal pore structure; FE-TEM also revealed, as a complementary technique, the structure and pore size. The textural properties of the Ni/MCM-41 were analyzed using N
2 adsorption isotherms at 77
K. The hydrogen-storage capacity of the Ni/MCM-41 was evaluated at 298
K/100
bar. It was found that the presence of Ni on mesoporous MCM-41 created hydrogen-favorable sites that enhanced the hydrogen-storage capacity by a spillover effect. Furthermore, it was concluded that the hydrogen-storage capacity was greatly influenced by the amount of nickel oxide, resulting in a chemical reaction between Ni/MCM-41 and hydrogen molecules. |
| doi_str_mv | 10.1016/j.jcis.2010.02.047 |
| format | Article |
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The objective of the present work was to investigate the possibility of improving the hydrogen-storage capacity of mesoporous MCM-41 containing nickel (Ni) oxides (Ni/MCM-41). The MCM-41 and Ni/MCM-41 were prepared using a hydrothermal process as a function of Ni content (2, 5, and 10
wt.% in the MCM-41). The surface functional groups of the Ni/MCM-41 were identified by Fourier transform infrared spectroscopy (FTIR). The structure and morphology of the Ni/MCM-41 were characterized by X-ray diffraction (XRD) and field emission transmission electron microscopy (FE-TEM). XRD results showed a well-ordered hexagonal pore structure; FE-TEM also revealed, as a complementary technique, the structure and pore size. The textural properties of the Ni/MCM-41 were analyzed using N
2 adsorption isotherms at 77
K. The hydrogen-storage capacity of the Ni/MCM-41 was evaluated at 298
K/100
bar. It was found that the presence of Ni on mesoporous MCM-41 created hydrogen-favorable sites that enhanced the hydrogen-storage capacity by a spillover effect. Furthermore, it was concluded that the hydrogen-storage capacity was greatly influenced by the amount of nickel oxide, resulting in a chemical reaction between Ni/MCM-41 and hydrogen molecules.</description><identifier>ISSN: 0021-9797</identifier><identifier>EISSN: 1095-7103</identifier><identifier>DOI: 10.1016/j.jcis.2010.02.047</identifier><identifier>PMID: 20347449</identifier><identifier>CODEN: JCISA5</identifier><language>eng</language><publisher>Amsterdam: Elsevier Inc</publisher><subject>Chemistry ; Colloidal state and disperse state ; Diffraction ; Exact sciences and technology ; Field emission ; Fourier transforms ; General and physical chemistry ; Hydrogen - chemistry ; Hydrogen storage ; Iron ; MCM-41 ; Morphology ; Nickel ; Nickel - chemistry ; Oxides ; Particle Size ; Porosity ; Porous materials ; Silicon Dioxide - chemistry ; Spillover effect ; Surface Properties</subject><ispartof>Journal of colloid and interface science, 2010-06, Vol.346 (1), p.194-198</ispartof><rights>2010</rights><rights>2015 INIST-CNRS</rights><rights>Crown Copyright © 2010. Published by Elsevier Inc. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c417t-b2dd8f9299c9ca784cfabfe77caead9f2dcdce9da2360e00747abf01798c67ec3</citedby><cites>FETCH-LOGICAL-c417t-b2dd8f9299c9ca784cfabfe77caead9f2dcdce9da2360e00747abf01798c67ec3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jcis.2010.02.047$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3541,27915,27916,45986</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22835471$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/20347449$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Park, Soo-Jin</creatorcontrib><creatorcontrib>Lee, Seul-Yi</creatorcontrib><title>A study on hydrogen-storage behaviors of nickel-loaded mesoporous MCM-41</title><title>Journal of colloid and interface science</title><addtitle>J Colloid Interface Sci</addtitle><description>The hydrogen-storage capacities of the Ni/MCM-41 as a function of Ni content are described.
The objective of the present work was to investigate the possibility of improving the hydrogen-storage capacity of mesoporous MCM-41 containing nickel (Ni) oxides (Ni/MCM-41). The MCM-41 and Ni/MCM-41 were prepared using a hydrothermal process as a function of Ni content (2, 5, and 10
wt.% in the MCM-41). The surface functional groups of the Ni/MCM-41 were identified by Fourier transform infrared spectroscopy (FTIR). The structure and morphology of the Ni/MCM-41 were characterized by X-ray diffraction (XRD) and field emission transmission electron microscopy (FE-TEM). XRD results showed a well-ordered hexagonal pore structure; FE-TEM also revealed, as a complementary technique, the structure and pore size. The textural properties of the Ni/MCM-41 were analyzed using N
2 adsorption isotherms at 77
K. The hydrogen-storage capacity of the Ni/MCM-41 was evaluated at 298
K/100
bar. It was found that the presence of Ni on mesoporous MCM-41 created hydrogen-favorable sites that enhanced the hydrogen-storage capacity by a spillover effect. Furthermore, it was concluded that the hydrogen-storage capacity was greatly influenced by the amount of nickel oxide, resulting in a chemical reaction between Ni/MCM-41 and hydrogen molecules.</description><subject>Chemistry</subject><subject>Colloidal state and disperse state</subject><subject>Diffraction</subject><subject>Exact sciences and technology</subject><subject>Field emission</subject><subject>Fourier transforms</subject><subject>General and physical chemistry</subject><subject>Hydrogen - chemistry</subject><subject>Hydrogen storage</subject><subject>Iron</subject><subject>MCM-41</subject><subject>Morphology</subject><subject>Nickel</subject><subject>Nickel - chemistry</subject><subject>Oxides</subject><subject>Particle Size</subject><subject>Porosity</subject><subject>Porous materials</subject><subject>Silicon Dioxide - chemistry</subject><subject>Spillover effect</subject><subject>Surface Properties</subject><issn>0021-9797</issn><issn>1095-7103</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkE1v2zAMhoVhxZJ-_IEeBl-GnZxRsmxZwC5BsDYDWvSynQWFoluljpVJToH8-ylImuN2IkA-fEk8jN1ymHHgzbf1bI0-zQTkBogZSPWBTTnoulQcqo9sCiB4qZVWE3aZ0hqA87rWn9hEQCWVlHrKlvMijTu3L8JQvOxdDM80lGkM0T5TsaIX--ZDTEXoisHjK_VlH6wjV2wohW2IYZeKx8VjKfk1u-hsn-jmVK_Y77sfvxbL8uHp_udi_lCi5GosV8K5ttNCa9RoVSuxs6uOlEJL1ulOOHRI2llRNUAASqo8B650i40irK7Y12PuNoY_O0qj2fiE1Pd2oPyN0dlMk0_V_yVbXbe10I3MpDiSGENKkTqzjX5j495wMAfVZm0Oqs1BtQFhsuq89PkUv1ttyJ1X3t1m4MsJsAlt30U7HDLOnGirWiqeue9HjrK2N0_RJPQ0IDkfCUfjgv_XH38BQvGcxQ</recordid><startdate>20100601</startdate><enddate>20100601</enddate><creator>Park, Soo-Jin</creator><creator>Lee, Seul-Yi</creator><general>Elsevier Inc</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20100601</creationdate><title>A study on hydrogen-storage behaviors of nickel-loaded mesoporous MCM-41</title><author>Park, Soo-Jin ; Lee, Seul-Yi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c417t-b2dd8f9299c9ca784cfabfe77caead9f2dcdce9da2360e00747abf01798c67ec3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Chemistry</topic><topic>Colloidal state and disperse state</topic><topic>Diffraction</topic><topic>Exact sciences and technology</topic><topic>Field emission</topic><topic>Fourier transforms</topic><topic>General and physical chemistry</topic><topic>Hydrogen - chemistry</topic><topic>Hydrogen storage</topic><topic>Iron</topic><topic>MCM-41</topic><topic>Morphology</topic><topic>Nickel</topic><topic>Nickel - chemistry</topic><topic>Oxides</topic><topic>Particle Size</topic><topic>Porosity</topic><topic>Porous materials</topic><topic>Silicon Dioxide - chemistry</topic><topic>Spillover effect</topic><topic>Surface Properties</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Park, Soo-Jin</creatorcontrib><creatorcontrib>Lee, Seul-Yi</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of colloid and interface science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Park, Soo-Jin</au><au>Lee, Seul-Yi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A study on hydrogen-storage behaviors of nickel-loaded mesoporous MCM-41</atitle><jtitle>Journal of colloid and interface science</jtitle><addtitle>J Colloid Interface Sci</addtitle><date>2010-06-01</date><risdate>2010</risdate><volume>346</volume><issue>1</issue><spage>194</spage><epage>198</epage><pages>194-198</pages><issn>0021-9797</issn><eissn>1095-7103</eissn><coden>JCISA5</coden><abstract>The hydrogen-storage capacities of the Ni/MCM-41 as a function of Ni content are described.
The objective of the present work was to investigate the possibility of improving the hydrogen-storage capacity of mesoporous MCM-41 containing nickel (Ni) oxides (Ni/MCM-41). The MCM-41 and Ni/MCM-41 were prepared using a hydrothermal process as a function of Ni content (2, 5, and 10
wt.% in the MCM-41). The surface functional groups of the Ni/MCM-41 were identified by Fourier transform infrared spectroscopy (FTIR). The structure and morphology of the Ni/MCM-41 were characterized by X-ray diffraction (XRD) and field emission transmission electron microscopy (FE-TEM). XRD results showed a well-ordered hexagonal pore structure; FE-TEM also revealed, as a complementary technique, the structure and pore size. The textural properties of the Ni/MCM-41 were analyzed using N
2 adsorption isotherms at 77
K. The hydrogen-storage capacity of the Ni/MCM-41 was evaluated at 298
K/100
bar. It was found that the presence of Ni on mesoporous MCM-41 created hydrogen-favorable sites that enhanced the hydrogen-storage capacity by a spillover effect. Furthermore, it was concluded that the hydrogen-storage capacity was greatly influenced by the amount of nickel oxide, resulting in a chemical reaction between Ni/MCM-41 and hydrogen molecules.</abstract><cop>Amsterdam</cop><pub>Elsevier Inc</pub><pmid>20347449</pmid><doi>10.1016/j.jcis.2010.02.047</doi><tpages>5</tpages></addata></record> |
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| subjects | Chemistry Colloidal state and disperse state Diffraction Exact sciences and technology Field emission Fourier transforms General and physical chemistry Hydrogen - chemistry Hydrogen storage Iron MCM-41 Morphology Nickel Nickel - chemistry Oxides Particle Size Porosity Porous materials Silicon Dioxide - chemistry Spillover effect Surface Properties |
| title | A study on hydrogen-storage behaviors of nickel-loaded mesoporous MCM-41 |
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