Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques

A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thicknes...

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Veröffentlicht in:Dental Materials Journal 2011, Vol.30(5), pp.754-761
Hauptverfasser: NYAN, Myat, TSUTSUMI, Yusuke, OYA, Kei, DOI, Hisashi, NOMURA, Naoyuki, KASUGAI, Shohei, HANAWA, Takao
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container_issue 5
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container_title Dental Materials Journal
container_volume 30
creator NYAN, Myat
TSUTSUMI, Yusuke
OYA, Kei
DOI, Hisashi
NOMURA, Naoyuki
KASUGAI, Shohei
HANAWA, Takao
description A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thickness of approximately 6 micrometers and was mainly composed of zirconium dioxide (ZrO2) with both tetragonal and monoclinic crystal structures. The surface of the specimen was hardened by this technique, and the hardness of the specimen was significantly larger than that of untreated Ti and MAO-treated Ti without Zr layer. The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. From these results, this technique has an advantage for the development of novel dental materials with excellent mechanical and aesthetic properties.
doi_str_mv 10.4012/dmj.2011-067
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Mater. J.</addtitle><description>A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thickness of approximately 6 micrometers and was mainly composed of zirconium dioxide (ZrO2) with both tetragonal and monoclinic crystal structures. The surface of the specimen was hardened by this technique, and the hardness of the specimen was significantly larger than that of untreated Ti and MAO-treated Ti without Zr layer. The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. 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The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. From these results, this technique has an advantage for the development of novel dental materials with excellent mechanical and aesthetic properties.</abstract><cop>Japan</cop><pub>The Japanese Society for Dental Materials and Devices</pub><pmid>21946498</pmid><doi>10.4012/dmj.2011-067</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record>
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source J-STAGE Free; MEDLINE; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals
subjects Adhesiveness
Aesthetic
Ceramics - chemical synthesis
Ceramics - chemistry
Coated Materials, Biocompatible - chemical synthesis
Coated Materials, Biocompatible - chemistry
Color
Crystallography
Dental Bonding
Dental materials
Dental Materials - chemical synthesis
Dental Materials - chemistry
Dental Stress Analysis - instrumentation
Dentistry
Deposition
Electrochemical Techniques
Electroplating - methods
Hardness
Humans
Materials Testing
Micro-arc oxidation
Micrometers
Microscopy, Electron, Scanning
Oxidation
Oxidation-Reduction
Oxides
Porosity
Spectrometry, X-Ray Emission
Sputter deposition
Stress, Mechanical
Surface Properties
Teeth
Titanium
Titanium - chemistry
Titanium base alloys
X-Ray Diffraction
Zirconium - chemistry
Zirconium dioxide
Zirconium oxide
title Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques
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