Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques
A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thicknes...
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Veröffentlicht in: | Dental Materials Journal 2011, Vol.30(5), pp.754-761 |
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description | A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thickness of approximately 6 micrometers and was mainly composed of zirconium dioxide (ZrO2) with both tetragonal and monoclinic crystal structures. The surface of the specimen was hardened by this technique, and the hardness of the specimen was significantly larger than that of untreated Ti and MAO-treated Ti without Zr layer. The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. From these results, this technique has an advantage for the development of novel dental materials with excellent mechanical and aesthetic properties. |
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The oxide layer grown by MAO treatment had a porous structure with a thickness of approximately 6 micrometers and was mainly composed of zirconium dioxide (ZrO2) with both tetragonal and monoclinic crystal structures. The surface of the specimen was hardened by this technique, and the hardness of the specimen was significantly larger than that of untreated Ti and MAO-treated Ti without Zr layer. The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. From these results, this technique has an advantage for the development of novel dental materials with excellent mechanical and aesthetic properties.</description><identifier>ISSN: 0287-4547</identifier><identifier>EISSN: 1881-1361</identifier><identifier>DOI: 10.4012/dmj.2011-067</identifier><identifier>PMID: 21946498</identifier><language>eng</language><publisher>Japan: The Japanese Society for Dental Materials and Devices</publisher><subject>Adhesiveness ; Aesthetic ; Ceramics - chemical synthesis ; Ceramics - chemistry ; Coated Materials, Biocompatible - chemical synthesis ; Coated Materials, Biocompatible - chemistry ; Color ; Crystallography ; Dental Bonding ; Dental materials ; Dental Materials - chemical synthesis ; Dental Materials - chemistry ; Dental Stress Analysis - instrumentation ; Dentistry ; Deposition ; Electrochemical Techniques ; Electroplating - methods ; Hardness ; Humans ; Materials Testing ; Micro-arc oxidation ; Micrometers ; Microscopy, Electron, Scanning ; Oxidation ; Oxidation-Reduction ; Oxides ; Porosity ; Spectrometry, X-Ray Emission ; Sputter deposition ; Stress, Mechanical ; Surface Properties ; Teeth ; Titanium ; Titanium - chemistry ; Titanium base alloys ; X-Ray Diffraction ; Zirconium - chemistry ; Zirconium dioxide ; Zirconium oxide</subject><ispartof>Dental Materials Journal, 2011, Vol.30(5), pp.754-761</ispartof><rights>2011 The Japanese Society for Dental Materials and Devices</rights><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c675t-74dd5fac1bc5a1f39c6c7391e9515ac59381d3dab78847f07d85931200bdd6563</citedby><cites>FETCH-LOGICAL-c675t-74dd5fac1bc5a1f39c6c7391e9515ac59381d3dab78847f07d85931200bdd6563</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,1883,4024,27923,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/21946498$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>NYAN, Myat</creatorcontrib><creatorcontrib>TSUTSUMI, Yusuke</creatorcontrib><creatorcontrib>OYA, Kei</creatorcontrib><creatorcontrib>DOI, Hisashi</creatorcontrib><creatorcontrib>NOMURA, Naoyuki</creatorcontrib><creatorcontrib>KASUGAI, Shohei</creatorcontrib><creatorcontrib>HANAWA, Takao</creatorcontrib><creatorcontrib>Tokyo Medical and Dental University</creatorcontrib><creatorcontrib>Graduate School of Engineering</creatorcontrib><creatorcontrib>Kogakuin University</creatorcontrib><creatorcontrib>The University of Tokyo</creatorcontrib><creatorcontrib>Institute of Biomaterials and Bioengineering</creatorcontrib><creatorcontrib>Graduate School of Medical and Dental Sciences</creatorcontrib><creatorcontrib>Research Institute of Science and Technology</creatorcontrib><creatorcontrib>Department of Materials Engineering</creatorcontrib><title>Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques</title><title>Dental Materials Journal</title><addtitle>Dent. Mater. J.</addtitle><description>A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thickness of approximately 6 micrometers and was mainly composed of zirconium dioxide (ZrO2) with both tetragonal and monoclinic crystal structures. The surface of the specimen was hardened by this technique, and the hardness of the specimen was significantly larger than that of untreated Ti and MAO-treated Ti without Zr layer. The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. From these results, this technique has an advantage for the development of novel dental materials with excellent mechanical and aesthetic properties.</description><subject>Adhesiveness</subject><subject>Aesthetic</subject><subject>Ceramics - chemical synthesis</subject><subject>Ceramics - chemistry</subject><subject>Coated Materials, Biocompatible - chemical synthesis</subject><subject>Coated Materials, Biocompatible - chemistry</subject><subject>Color</subject><subject>Crystallography</subject><subject>Dental Bonding</subject><subject>Dental materials</subject><subject>Dental Materials - chemical synthesis</subject><subject>Dental Materials - chemistry</subject><subject>Dental Stress Analysis - instrumentation</subject><subject>Dentistry</subject><subject>Deposition</subject><subject>Electrochemical Techniques</subject><subject>Electroplating - methods</subject><subject>Hardness</subject><subject>Humans</subject><subject>Materials Testing</subject><subject>Micro-arc oxidation</subject><subject>Micrometers</subject><subject>Microscopy, Electron, Scanning</subject><subject>Oxidation</subject><subject>Oxidation-Reduction</subject><subject>Oxides</subject><subject>Porosity</subject><subject>Spectrometry, X-Ray Emission</subject><subject>Sputter deposition</subject><subject>Stress, Mechanical</subject><subject>Surface Properties</subject><subject>Teeth</subject><subject>Titanium</subject><subject>Titanium - chemistry</subject><subject>Titanium base alloys</subject><subject>X-Ray Diffraction</subject><subject>Zirconium - chemistry</subject><subject>Zirconium dioxide</subject><subject>Zirconium oxide</subject><issn>0287-4547</issn><issn>1881-1361</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kc1v1DAQxS0EokvhxhnlBoemeOLPHGkFBakSB-BsObbDepXYi-1U5L_Hu9vukctYevPzm7EfQm8BX1MM3Uc77647DNBiLp6hDUgJLRAOz9EGd1K0lFFxgV7lvMOY9lzKl-iig55y2ssNyj_WULYu-9zEsQnxwU1N_Outaya9ulTV0BRfdPDL3AxrY-I8-KCLr3q9kPdLKS411u1j9kdVB9vM3qTY6mSOXie6OLMN_s_i8mv0YtRTdm8ez0v068vnn7df2_vvd99uP923hgtWWkGtZaM2MBimYSS94UaQHlzPgGnDeiLBEqsHISUVIxZWVg06jAdrOePkEr0_-e5TPMwtavbZuGnSwcUlK9kLCZRJqOSH_5LABRAATkRFr05ofWHOyY1qn_ys06oAq0MgqgaiDoGoGkjF3z06L8Ps7Bl-SqACdyegdr3RUwyTD07t4pJC_RxlV2xdOFtigjFTuCMKC0Zr4dABwazrq9PNyWmXi_7tzqN0Kt5M7rgXwYodytN-56bZ6qRcIP8AKBS16w</recordid><startdate>2011</startdate><enddate>2011</enddate><creator>NYAN, Myat</creator><creator>TSUTSUMI, Yusuke</creator><creator>OYA, Kei</creator><creator>DOI, Hisashi</creator><creator>NOMURA, Naoyuki</creator><creator>KASUGAI, Shohei</creator><creator>HANAWA, Takao</creator><general>The Japanese Society for Dental Materials and Devices</general><general>Japanese Society for Dental Materials and Devices</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><scope>7X8</scope></search><sort><creationdate>2011</creationdate><title>Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques</title><author>NYAN, Myat ; TSUTSUMI, Yusuke ; OYA, Kei ; DOI, Hisashi ; NOMURA, Naoyuki ; KASUGAI, Shohei ; HANAWA, Takao</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c675t-74dd5fac1bc5a1f39c6c7391e9515ac59381d3dab78847f07d85931200bdd6563</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Adhesiveness</topic><topic>Aesthetic</topic><topic>Ceramics - chemical synthesis</topic><topic>Ceramics - chemistry</topic><topic>Coated Materials, Biocompatible - chemical synthesis</topic><topic>Coated Materials, Biocompatible - chemistry</topic><topic>Color</topic><topic>Crystallography</topic><topic>Dental Bonding</topic><topic>Dental materials</topic><topic>Dental Materials - chemical synthesis</topic><topic>Dental Materials - chemistry</topic><topic>Dental Stress Analysis - instrumentation</topic><topic>Dentistry</topic><topic>Deposition</topic><topic>Electrochemical Techniques</topic><topic>Electroplating - methods</topic><topic>Hardness</topic><topic>Humans</topic><topic>Materials Testing</topic><topic>Micro-arc oxidation</topic><topic>Micrometers</topic><topic>Microscopy, Electron, Scanning</topic><topic>Oxidation</topic><topic>Oxidation-Reduction</topic><topic>Oxides</topic><topic>Porosity</topic><topic>Spectrometry, X-Ray Emission</topic><topic>Sputter deposition</topic><topic>Stress, Mechanical</topic><topic>Surface Properties</topic><topic>Teeth</topic><topic>Titanium</topic><topic>Titanium - chemistry</topic><topic>Titanium base alloys</topic><topic>X-Ray Diffraction</topic><topic>Zirconium - chemistry</topic><topic>Zirconium dioxide</topic><topic>Zirconium oxide</topic><toplevel>online_resources</toplevel><creatorcontrib>NYAN, Myat</creatorcontrib><creatorcontrib>TSUTSUMI, Yusuke</creatorcontrib><creatorcontrib>OYA, Kei</creatorcontrib><creatorcontrib>DOI, Hisashi</creatorcontrib><creatorcontrib>NOMURA, Naoyuki</creatorcontrib><creatorcontrib>KASUGAI, Shohei</creatorcontrib><creatorcontrib>HANAWA, Takao</creatorcontrib><creatorcontrib>Tokyo Medical and Dental University</creatorcontrib><creatorcontrib>Graduate School of Engineering</creatorcontrib><creatorcontrib>Kogakuin University</creatorcontrib><creatorcontrib>The University of Tokyo</creatorcontrib><creatorcontrib>Institute of Biomaterials and Bioengineering</creatorcontrib><creatorcontrib>Graduate School of Medical and Dental Sciences</creatorcontrib><creatorcontrib>Research Institute of Science and Technology</creatorcontrib><creatorcontrib>Department of Materials Engineering</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Dental Materials Journal</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>NYAN, Myat</au><au>TSUTSUMI, Yusuke</au><au>OYA, Kei</au><au>DOI, Hisashi</au><au>NOMURA, Naoyuki</au><au>KASUGAI, Shohei</au><au>HANAWA, Takao</au><aucorp>Tokyo Medical and Dental University</aucorp><aucorp>Graduate School of Engineering</aucorp><aucorp>Kogakuin University</aucorp><aucorp>The University of Tokyo</aucorp><aucorp>Institute of Biomaterials and Bioengineering</aucorp><aucorp>Graduate School of Medical and Dental Sciences</aucorp><aucorp>Research Institute of Science and Technology</aucorp><aucorp>Department of Materials Engineering</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques</atitle><jtitle>Dental Materials Journal</jtitle><addtitle>Dent. Mater. J.</addtitle><date>2011</date><risdate>2011</risdate><volume>30</volume><issue>5</issue><spage>754</spage><epage>761</epage><pages>754-761</pages><issn>0287-4547</issn><eissn>1881-1361</eissn><abstract>A novel coating technique of thin ceramic layer resembling teeth color on titanium (Ti) surface was developed by combination of sputter deposition of metal zirconium (Zr) and subsequent micro-arc oxidation (MAO) treatment. The oxide layer grown by MAO treatment had a porous structure with a thickness of approximately 6 micrometers and was mainly composed of zirconium dioxide (ZrO2) with both tetragonal and monoclinic crystal structures. The surface of the specimen was hardened by this technique, and the hardness of the specimen was significantly larger than that of untreated Ti and MAO-treated Ti without Zr layer. The bonding strength test revealed that fracture occurred inside the oxide layer, indicating that adhesion between the oxide layer and the Ti substrate was sufficiently strong. From these results, this technique has an advantage for the development of novel dental materials with excellent mechanical and aesthetic properties.</abstract><cop>Japan</cop><pub>The Japanese Society for Dental Materials and Devices</pub><pmid>21946498</pmid><doi>10.4012/dmj.2011-067</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record> |
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subjects | Adhesiveness Aesthetic Ceramics - chemical synthesis Ceramics - chemistry Coated Materials, Biocompatible - chemical synthesis Coated Materials, Biocompatible - chemistry Color Crystallography Dental Bonding Dental materials Dental Materials - chemical synthesis Dental Materials - chemistry Dental Stress Analysis - instrumentation Dentistry Deposition Electrochemical Techniques Electroplating - methods Hardness Humans Materials Testing Micro-arc oxidation Micrometers Microscopy, Electron, Scanning Oxidation Oxidation-Reduction Oxides Porosity Spectrometry, X-Ray Emission Sputter deposition Stress, Mechanical Surface Properties Teeth Titanium Titanium - chemistry Titanium base alloys X-Ray Diffraction Zirconium - chemistry Zirconium dioxide Zirconium oxide |
title | Synthesis of novel oxide layers on titanium by combination of sputter deposition and micro-arc oxidation techniques |
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