Processing of Tellurite-Based Glass with Low OH Content
We report results on the processing and characterization of tellurite‐based glass in the TeO2–Bi2O3–ZnO (TBZ) glass family and efforts to reduce their absorption loss due to residual hydroxyl (OH) content. We show that the introduction of alkaline or alkaline earth in the glass network, drying of th...
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| Veröffentlicht in: | Journal of the American Ceramic Society 2011-01, Vol.94 (1), p.130-136 |
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| container_title | Journal of the American Ceramic Society |
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| creator | Massera, Jonathan Haldeman, Adam Jackson, Jessica Rivero-Baleine, Clara Petit, L. Richardson, Kathleen |
| description | We report results on the processing and characterization of tellurite‐based glass in the TeO2–Bi2O3–ZnO (TBZ) glass family and efforts to reduce their absorption loss due to residual hydroxyl (OH) content. We show that the introduction of alkaline or alkaline earth in the glass network, drying of the batch with fluorine‐based raw materials before melting, and melting of the glass in O2‐rich atmosphere can lead to a significant reduction in OH content. Employing these steps in TBZ glass processing resulted in a 93% reduction of OH content as compared with a reference composition. The reduction in OH content was verified by a decrease of the absorption band center at 3000 cm−1 as well as a decrease of the free volume in the glass. The addition of F in the glass network was found to reduce the fraction of nonbridging oxygen associated with OH. X‐ray fluorescence spectrometry was used to determine the amount of remaining F. |
| doi_str_mv | 10.1111/j.1551-2916.2010.04031.x |
| format | Article |
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We show that the introduction of alkaline or alkaline earth in the glass network, drying of the batch with fluorine‐based raw materials before melting, and melting of the glass in O2‐rich atmosphere can lead to a significant reduction in OH content. Employing these steps in TBZ glass processing resulted in a 93% reduction of OH content as compared with a reference composition. The reduction in OH content was verified by a decrease of the absorption band center at 3000 cm−1 as well as a decrease of the free volume in the glass. The addition of F in the glass network was found to reduce the fraction of nonbridging oxygen associated with OH. 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X‐ray fluorescence spectrometry was used to determine the amount of remaining F.</description><subject>Ceramics</subject><subject>Drying</subject><subject>Earth</subject><subject>Fluorescence</subject><subject>Glass</subject><subject>Materials science</subject><subject>Melting</subject><subject>Networks</subject><subject>Oxygen</subject><subject>Raw materials</subject><subject>Reduction</subject><issn>0002-7820</issn><issn>1551-2916</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkc1PwjAchhujiYj-D4sXvQz7a7t2vZjgwodIhAOG4y-DdTocm64jwH9vJ4aDB-2lX0_evs1DiAe0A27crToQBOAzDbLDqDulgnLo7E5I63hxSlqUUuarkNFzcmHtym1Bh6JF1LQql8barHj1ytSbmTzfVFlt_IfYmsQb5LG13jar37xxufUmQy8qi9oU9SU5S-PcmqufuU1e-r1ZNPTHk8Fj1B37S8EU-EIYaRQsmte0XGgRuHoLmaQ8TRUIZmIahBoCSGDBwzSRBmKhJRPAhFgmnLfJzSH3oyo_N8bWuM7s0rWMC1NuLLpUCJlgwf9kEEgdctWQt3-SIDXjEjRv0Otf6KrcVIX7MYZCCekw5aD7A7TNcrPHjypbx9UegWJjCFfYiMBGBDaG8NsQ7nDUjXrN0gX4h4DM1mZ3DIird5TKNcb58wBH_fHTaDCNcM6_AFKVkb4</recordid><startdate>201101</startdate><enddate>201101</enddate><creator>Massera, Jonathan</creator><creator>Haldeman, Adam</creator><creator>Jackson, Jessica</creator><creator>Rivero-Baleine, Clara</creator><creator>Petit, L.</creator><creator>Richardson, Kathleen</creator><general>Blackwell Publishing Inc</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>201101</creationdate><title>Processing of Tellurite-Based Glass with Low OH Content</title><author>Massera, Jonathan ; Haldeman, Adam ; Jackson, Jessica ; Rivero-Baleine, Clara ; Petit, L. ; Richardson, Kathleen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4271-44e6e71b019896b945040b6df3ff7142ea0589151d1b38fd6e1a496241244cd33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Ceramics</topic><topic>Drying</topic><topic>Earth</topic><topic>Fluorescence</topic><topic>Glass</topic><topic>Materials science</topic><topic>Melting</topic><topic>Networks</topic><topic>Oxygen</topic><topic>Raw materials</topic><topic>Reduction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Massera, Jonathan</creatorcontrib><creatorcontrib>Haldeman, Adam</creatorcontrib><creatorcontrib>Jackson, Jessica</creatorcontrib><creatorcontrib>Rivero-Baleine, Clara</creatorcontrib><creatorcontrib>Petit, L.</creatorcontrib><creatorcontrib>Richardson, Kathleen</creatorcontrib><collection>Istex</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of the American Ceramic Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Massera, Jonathan</au><au>Haldeman, Adam</au><au>Jackson, Jessica</au><au>Rivero-Baleine, Clara</au><au>Petit, L.</au><au>Richardson, Kathleen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Processing of Tellurite-Based Glass with Low OH Content</atitle><jtitle>Journal of the American Ceramic Society</jtitle><date>2011-01</date><risdate>2011</risdate><volume>94</volume><issue>1</issue><spage>130</spage><epage>136</epage><pages>130-136</pages><issn>0002-7820</issn><eissn>1551-2916</eissn><coden>JACTAW</coden><abstract>We report results on the processing and characterization of tellurite‐based glass in the TeO2–Bi2O3–ZnO (TBZ) glass family and efforts to reduce their absorption loss due to residual hydroxyl (OH) content. 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| ispartof | Journal of the American Ceramic Society, 2011-01, Vol.94 (1), p.130-136 |
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| language | eng |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Ceramics Drying Earth Fluorescence Glass Materials science Melting Networks Oxygen Raw materials Reduction |
| title | Processing of Tellurite-Based Glass with Low OH Content |
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