Synthesis, characterization and application of a two-fold 13C-labeled calibration standard for the analysis of arsenobetaine using HPLC–ESI-MS/MS without high resolution mass spectrometry
A procedure has been developed for the determination of arsenobetaine in fish matrix by HPLC–ESI-MS/MS. Hereby (trimethylarsonium)-1,2-13C-acetate (arsenobetaine) is used as internal calibration standard. Arsenobetaine was determined in a fish material (Sea Bass) with an expanded uncertainty of 3.8%...
Gespeichert in:
| Veröffentlicht in: | Talanta (Oxford) 2011-09, Vol.85 (4), p.1996-1999 |
|---|---|
| Hauptverfasser: | , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 1999 |
|---|---|
| container_issue | 4 |
| container_start_page | 1996 |
| container_title | Talanta (Oxford) |
| container_volume | 85 |
| creator | Lischka, S. Körte, F. Faust, R. Nehls, I. Piechotta, Ch |
| description | A procedure has been developed for the determination of arsenobetaine in fish matrix by HPLC–ESI-MS/MS. Hereby (trimethylarsonium)-1,2-13C-acetate (arsenobetaine) is used as internal calibration standard. Arsenobetaine was determined in a fish material (Sea Bass) with an expanded uncertainty of 3.8%. |
| doi_str_mv | 10.1016/j.talanta.2011.07.047 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_885906524</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0039914011006229</els_id><sourcerecordid>885906524</sourcerecordid><originalsourceid>FETCH-LOGICAL-c2390-7d51192968ffd32d75a64317ce042110cdf272c24a48614740fda91d24aba2ca3</originalsourceid><addsrcrecordid>eNqFkcFu1DAQhiMEokvhEUC-IC4kHdvJZnNCaFXaSluBtHC2Zu1J16skXmyHajnxDjwPL9MnwW0WOHKybH3_P9Z8WfaSQ8GBz892RcQOh4iFAM4LqAso60fZjC9qmcuqlo-zGYBs8oaXcJI9C2EHAEKCfJqdiEQJqGCW_VofhrilYMNbprfoUUfy9jtG6waGg2G433dWT3fXMmTx1uWt6wzjcpl3uKGODNPY2Y2fqBBTDr1hrfMsdaca7A5pwkPeBxrchiLagdgY7HDDLj-tlnc_fp6vr_Lr9dn1mt3auHVjZFt7s2WeguvGh-YeQ2BhTzp611P0h-fZkxa7QC-O52n25cP55-Vlvvp4cbV8v8q1kA3ktak4b0QzX7StkcLUFc5LyWtNUArOQZtW1EKLEsvFnJd1Ca3Bhpv0sEGhUZ5mb6bevXdfRwpR9TZo6pIAcmNQi0XVwLwSZSKridTeheCpVXtve_QHxUHdi1M7dRSn7sUpqFUSl3KvjhPGTU_mb-qPqQS8PgIY0rZbj4O24R9XVlxI2STu3cRR2sc3S14FbWnQZKxPi1PG2f985Tf2lb0-</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>885906524</pqid></control><display><type>article</type><title>Synthesis, characterization and application of a two-fold 13C-labeled calibration standard for the analysis of arsenobetaine using HPLC–ESI-MS/MS without high resolution mass spectrometry</title><source>MEDLINE</source><source>ScienceDirect Journals (5 years ago - present)</source><creator>Lischka, S. ; Körte, F. ; Faust, R. ; Nehls, I. ; Piechotta, Ch</creator><creatorcontrib>Lischka, S. ; Körte, F. ; Faust, R. ; Nehls, I. ; Piechotta, Ch</creatorcontrib><description>A procedure has been developed for the determination of arsenobetaine in fish matrix by HPLC–ESI-MS/MS. Hereby (trimethylarsonium)-1,2-13C-acetate (arsenobetaine) is used as internal calibration standard. Arsenobetaine was determined in a fish material (Sea Bass) with an expanded uncertainty of 3.8%.</description><identifier>ISSN: 0039-9140</identifier><identifier>EISSN: 1873-3573</identifier><identifier>DOI: 10.1016/j.talanta.2011.07.047</identifier><identifier>PMID: 21872050</identifier><identifier>CODEN: TLNTA2</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>13C ; Analytical chemistry ; Arsenicals - analysis ; Arsenicals - chemistry ; Arsenobetaine ; Calibration ; Carbon Isotopes - chemistry ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Chromatography, High Pressure Liquid - standards ; ESI-MS/MS ; Exact sciences and technology ; Isotopic labeled ; Other chromatographic methods ; Reference Standards ; Spectrometric and optical methods ; Spectrometry, Mass, Electrospray Ionization - standards ; Tandem Mass Spectrometry - standards</subject><ispartof>Talanta (Oxford), 2011-09, Vol.85 (4), p.1996-1999</ispartof><rights>2011 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><rights>Copyright © 2011 Elsevier B.V. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2390-7d51192968ffd32d75a64317ce042110cdf272c24a48614740fda91d24aba2ca3</citedby><cites>FETCH-LOGICAL-c2390-7d51192968ffd32d75a64317ce042110cdf272c24a48614740fda91d24aba2ca3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.talanta.2011.07.047$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3549,27923,27924,45994</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24512339$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/21872050$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Lischka, S.</creatorcontrib><creatorcontrib>Körte, F.</creatorcontrib><creatorcontrib>Faust, R.</creatorcontrib><creatorcontrib>Nehls, I.</creatorcontrib><creatorcontrib>Piechotta, Ch</creatorcontrib><title>Synthesis, characterization and application of a two-fold 13C-labeled calibration standard for the analysis of arsenobetaine using HPLC–ESI-MS/MS without high resolution mass spectrometry</title><title>Talanta (Oxford)</title><addtitle>Talanta</addtitle><description>A procedure has been developed for the determination of arsenobetaine in fish matrix by HPLC–ESI-MS/MS. Hereby (trimethylarsonium)-1,2-13C-acetate (arsenobetaine) is used as internal calibration standard. Arsenobetaine was determined in a fish material (Sea Bass) with an expanded uncertainty of 3.8%.</description><subject>13C</subject><subject>Analytical chemistry</subject><subject>Arsenicals - analysis</subject><subject>Arsenicals - chemistry</subject><subject>Arsenobetaine</subject><subject>Calibration</subject><subject>Carbon Isotopes - chemistry</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Chromatography, High Pressure Liquid - standards</subject><subject>ESI-MS/MS</subject><subject>Exact sciences and technology</subject><subject>Isotopic labeled</subject><subject>Other chromatographic methods</subject><subject>Reference Standards</subject><subject>Spectrometric and optical methods</subject><subject>Spectrometry, Mass, Electrospray Ionization - standards</subject><subject>Tandem Mass Spectrometry - standards</subject><issn>0039-9140</issn><issn>1873-3573</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkcFu1DAQhiMEokvhEUC-IC4kHdvJZnNCaFXaSluBtHC2Zu1J16skXmyHajnxDjwPL9MnwW0WOHKybH3_P9Z8WfaSQ8GBz892RcQOh4iFAM4LqAso60fZjC9qmcuqlo-zGYBs8oaXcJI9C2EHAEKCfJqdiEQJqGCW_VofhrilYMNbprfoUUfy9jtG6waGg2G433dWT3fXMmTx1uWt6wzjcpl3uKGODNPY2Y2fqBBTDr1hrfMsdaca7A5pwkPeBxrchiLagdgY7HDDLj-tlnc_fp6vr_Lr9dn1mt3auHVjZFt7s2WeguvGh-YeQ2BhTzp611P0h-fZkxa7QC-O52n25cP55-Vlvvp4cbV8v8q1kA3ktak4b0QzX7StkcLUFc5LyWtNUArOQZtW1EKLEsvFnJd1Ca3Bhpv0sEGhUZ5mb6bevXdfRwpR9TZo6pIAcmNQi0XVwLwSZSKridTeheCpVXtve_QHxUHdi1M7dRSn7sUpqFUSl3KvjhPGTU_mb-qPqQS8PgIY0rZbj4O24R9XVlxI2STu3cRR2sc3S14FbWnQZKxPi1PG2f985Tf2lb0-</recordid><startdate>20110930</startdate><enddate>20110930</enddate><creator>Lischka, S.</creator><creator>Körte, F.</creator><creator>Faust, R.</creator><creator>Nehls, I.</creator><creator>Piechotta, Ch</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20110930</creationdate><title>Synthesis, characterization and application of a two-fold 13C-labeled calibration standard for the analysis of arsenobetaine using HPLC–ESI-MS/MS without high resolution mass spectrometry</title><author>Lischka, S. ; Körte, F. ; Faust, R. ; Nehls, I. ; Piechotta, Ch</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2390-7d51192968ffd32d75a64317ce042110cdf272c24a48614740fda91d24aba2ca3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>13C</topic><topic>Analytical chemistry</topic><topic>Arsenicals - analysis</topic><topic>Arsenicals - chemistry</topic><topic>Arsenobetaine</topic><topic>Calibration</topic><topic>Carbon Isotopes - chemistry</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Chromatography, High Pressure Liquid - standards</topic><topic>ESI-MS/MS</topic><topic>Exact sciences and technology</topic><topic>Isotopic labeled</topic><topic>Other chromatographic methods</topic><topic>Reference Standards</topic><topic>Spectrometric and optical methods</topic><topic>Spectrometry, Mass, Electrospray Ionization - standards</topic><topic>Tandem Mass Spectrometry - standards</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lischka, S.</creatorcontrib><creatorcontrib>Körte, F.</creatorcontrib><creatorcontrib>Faust, R.</creatorcontrib><creatorcontrib>Nehls, I.</creatorcontrib><creatorcontrib>Piechotta, Ch</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Talanta (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lischka, S.</au><au>Körte, F.</au><au>Faust, R.</au><au>Nehls, I.</au><au>Piechotta, Ch</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis, characterization and application of a two-fold 13C-labeled calibration standard for the analysis of arsenobetaine using HPLC–ESI-MS/MS without high resolution mass spectrometry</atitle><jtitle>Talanta (Oxford)</jtitle><addtitle>Talanta</addtitle><date>2011-09-30</date><risdate>2011</risdate><volume>85</volume><issue>4</issue><spage>1996</spage><epage>1999</epage><pages>1996-1999</pages><issn>0039-9140</issn><eissn>1873-3573</eissn><coden>TLNTA2</coden><abstract>A procedure has been developed for the determination of arsenobetaine in fish matrix by HPLC–ESI-MS/MS. Hereby (trimethylarsonium)-1,2-13C-acetate (arsenobetaine) is used as internal calibration standard. Arsenobetaine was determined in a fish material (Sea Bass) with an expanded uncertainty of 3.8%.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>21872050</pmid><doi>10.1016/j.talanta.2011.07.047</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0039-9140 |
| ispartof | Talanta (Oxford), 2011-09, Vol.85 (4), p.1996-1999 |
| issn | 0039-9140 1873-3573 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_885906524 |
| source | MEDLINE; ScienceDirect Journals (5 years ago - present) |
| subjects | 13C Analytical chemistry Arsenicals - analysis Arsenicals - chemistry Arsenobetaine Calibration Carbon Isotopes - chemistry Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, High Pressure Liquid - standards ESI-MS/MS Exact sciences and technology Isotopic labeled Other chromatographic methods Reference Standards Spectrometric and optical methods Spectrometry, Mass, Electrospray Ionization - standards Tandem Mass Spectrometry - standards |
| title | Synthesis, characterization and application of a two-fold 13C-labeled calibration standard for the analysis of arsenobetaine using HPLC–ESI-MS/MS without high resolution mass spectrometry |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-09T02%3A54%3A07IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Synthesis,%20characterization%20and%20application%20of%20a%20two-fold%2013C-labeled%20calibration%20standard%20for%20the%20analysis%20of%20arsenobetaine%20using%20HPLC%E2%80%93ESI-MS/MS%20without%20high%20resolution%20mass%20spectrometry&rft.jtitle=Talanta%20(Oxford)&rft.au=Lischka,%20S.&rft.date=2011-09-30&rft.volume=85&rft.issue=4&rft.spage=1996&rft.epage=1999&rft.pages=1996-1999&rft.issn=0039-9140&rft.eissn=1873-3573&rft.coden=TLNTA2&rft_id=info:doi/10.1016/j.talanta.2011.07.047&rft_dat=%3Cproquest_cross%3E885906524%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=885906524&rft_id=info:pmid/21872050&rft_els_id=S0039914011006229&rfr_iscdi=true |