Comparison of Fermented Soybean Paste (Doenjang) Prepared by Different Methods Based on Profiling of Volatile Compounds

:  In this study, 2 different extraction methods, namely solvent‐assisted flavor evaporation (SAFE) and solid‐phase microextraction (SPME), were employed to investigate the comprehensive volatile profile of Doenjang (one of Korean fermented soybean pastes) efficiently. Quantitatively, major volatile...

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Veröffentlicht in:Journal of food science 2011-04, Vol.76 (3), p.C368-C379
Hauptverfasser: Jo, Ye-Jin, Cho, In Hee, Song, Chi Kwang, Shin, Hye Won, Kim, Young-Suk
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container_issue 3
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container_title Journal of food science
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creator Jo, Ye-Jin
Cho, In Hee
Song, Chi Kwang
Shin, Hye Won
Kim, Young-Suk
description :  In this study, 2 different extraction methods, namely solvent‐assisted flavor evaporation (SAFE) and solid‐phase microextraction (SPME), were employed to investigate the comprehensive volatile profile of Doenjang (one of Korean fermented soybean pastes) efficiently. Quantitatively, major volatiles of Doenjang isolated by SAFE were 3‐methylbutanoic acid, butanoic acid, 3‐hydroxy‐2‐methyl‐4H‐pyran‐4‐one (maltol), ethyl 2‐methylbutanoate, 2‐methylpropanoic acid, tetramethylpyrazine, and 4‐ethyl‐2‐methoxyphenol, while ethanol, ethenylbenzene, ethyl benzoate, ethyl linoleate, ethyl acetate, ethyl butanoate, tetramethylpyrazine, and ethyl 2‐methylpropanoate extracted by SPME. In addition, volatile profiling that applied principal component analysis to gas chromatography‐mass spectrometry datasets allowed Doenjang samples that had been prepared using different traditional and commercial methods to be discriminated, and the volatile compounds that contributed to their discrimination were assigned. The major volatiles that were related to differentiation of traditional and commercial Doenjang samples were 2‐pentylfuran, 4‐ethylphenol, dihydro‐5‐methyl‐2(3H)‐furanone, butanoic acid, pyrazines (for example, 2‐ethyl‐5‐methylpyrazine and 2,3‐dimethylpyrazine), esters (for example, ethyl 4‐methylpentanoate and diethyl succinate), maltol, dimethyl disulfide, 2‐ and 3‐methylbutanal, hexanal, 4‐vinylphenol, and ethanol.
doi_str_mv 10.1111/j.1750-3841.2011.02068.x
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The major volatiles that were related to differentiation of traditional and commercial Doenjang samples were 2‐pentylfuran, 4‐ethylphenol, dihydro‐5‐methyl‐2(3H)‐furanone, butanoic acid, pyrazines (for example, 2‐ethyl‐5‐methylpyrazine and 2,3‐dimethylpyrazine), esters (for example, ethyl 4‐methylpentanoate and diethyl succinate), maltol, dimethyl disulfide, 2‐ and 3‐methylbutanal, hexanal, 4‐vinylphenol, and ethanol.</description><identifier>ISSN: 0022-1147</identifier><identifier>EISSN: 1750-3841</identifier><identifier>DOI: 10.1111/j.1750-3841.2011.02068.x</identifier><identifier>PMID: 21535802</identifier><identifier>CODEN: JFDSAZ</identifier><language>eng</language><publisher>Malden, USA: Blackwell Publishing Inc</publisher><subject>Aspergillus - metabolism ; Bacillus subtilis - metabolism ; Biological and medical sciences ; Chromatography ; Condiments - analysis ; Condiments - microbiology ; Evaporation ; Extraction processes ; Fermentation ; fermented soybean paste (Doenjang) ; Food Analysis - methods ; Food Handling - methods ; Food industries ; Food science ; Fruit and vegetable industries ; Fundamental and applied biological sciences. 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Psychology</subject><subject>Gas Chromatography-Mass Spectrometry</subject><subject>Mass spectrometry</subject><subject>Mucorales - metabolism</subject><subject>Principal Component Analysis</subject><subject>Principal components analysis</subject><subject>Republic of Korea</subject><subject>Solid Phase Microextraction</subject><subject>Soy Foods - analysis</subject><subject>Soy Foods - microbiology</subject><subject>Soybeans</subject><subject>volatile compounds</subject><subject>Volatile Organic Compounds - analysis</subject><subject>volatile profiling</subject><issn>0022-1147</issn><issn>1750-3841</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqNkl1v0zAYhS0EYt3gLyALCTEuEmzHX7lBgpaOjzEqrYxLy0nskZDExU609t_j0FIkbsA3tvU-57y2jwGAGKU4jpdNigVDSSYpTgnCOEUEcZlu74HZsXAfzBAiJMGYihNwGkKDpn3GH4ITglnGJCIzcDd33Ub7OrgeOguXxnemH0wFr92uMLqHKx0GA88XzvSN7m9fwJU3URCJYgcXtbXGRwH8ZIZvrgrwjQ6xFM1W3tm6rfvbyfbGtXqoWwOnbm7sq_AIPLC6DebxYT4DX5Zv1_N3yeXni_fz15dJyTGRCUM0rwTXLDeSiSzjyCBWyFxgQbUWKLNFZajUmhGRW8RiOSdEYsQIp8bm2Rl4vvfdePdjNGFQXR1K07a6N24MSsbnYjll-N8kp0JyIWUkn_5FNm70fbxGhDjjsTeLkNxDpXcheGPVxted9juFkZpCVI2aslJTVmoKUf0KUW2j9MnBfyw6Ux2Fv1OLwLMDoEOpW-t1X9bhD0eR5CijkXu15-7i2-_--wDqw3JxPS2jQbI3qOMn2B4NtP-uuMgEU1-vLtTV6ma-xouPap39BM6ExN0</recordid><startdate>201104</startdate><enddate>201104</enddate><creator>Jo, Ye-Jin</creator><creator>Cho, In Hee</creator><creator>Song, Chi Kwang</creator><creator>Shin, Hye Won</creator><creator>Kim, Young-Suk</creator><general>Blackwell Publishing Inc</general><general>Wiley</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QO</scope><scope>7QR</scope><scope>7ST</scope><scope>7T7</scope><scope>7U7</scope><scope>8FD</scope><scope>C1K</scope><scope>F28</scope><scope>FR3</scope><scope>P64</scope><scope>RC3</scope><scope>SOI</scope><scope>7X8</scope></search><sort><creationdate>201104</creationdate><title>Comparison of Fermented Soybean Paste (Doenjang) Prepared by Different Methods Based on Profiling of Volatile Compounds</title><author>Jo, Ye-Jin ; Cho, In Hee ; Song, Chi Kwang ; Shin, Hye Won ; Kim, Young-Suk</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c6128-5049d76a59e8573360e05b897174aa703fbde48aa5279f050e09228105264ef93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Aspergillus - metabolism</topic><topic>Bacillus subtilis - metabolism</topic><topic>Biological and medical sciences</topic><topic>Chromatography</topic><topic>Condiments - analysis</topic><topic>Condiments - microbiology</topic><topic>Evaporation</topic><topic>Extraction processes</topic><topic>Fermentation</topic><topic>fermented soybean paste (Doenjang)</topic><topic>Food Analysis - methods</topic><topic>Food Handling - methods</topic><topic>Food industries</topic><topic>Food science</topic><topic>Fruit and vegetable industries</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Gas Chromatography-Mass Spectrometry</topic><topic>Mass spectrometry</topic><topic>Mucorales - metabolism</topic><topic>Principal Component Analysis</topic><topic>Principal components analysis</topic><topic>Republic of Korea</topic><topic>Solid Phase Microextraction</topic><topic>Soy Foods - analysis</topic><topic>Soy Foods - microbiology</topic><topic>Soybeans</topic><topic>volatile compounds</topic><topic>Volatile Organic Compounds - analysis</topic><topic>volatile profiling</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jo, Ye-Jin</creatorcontrib><creatorcontrib>Cho, In Hee</creatorcontrib><creatorcontrib>Song, Chi Kwang</creatorcontrib><creatorcontrib>Shin, Hye Won</creatorcontrib><creatorcontrib>Kim, Young-Suk</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Biotechnology Research Abstracts</collection><collection>Chemoreception Abstracts</collection><collection>Environment Abstracts</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Toxicology Abstracts</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ANTE: Abstracts in New Technology &amp; Engineering</collection><collection>Engineering Research Database</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Genetics Abstracts</collection><collection>Environment Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of food science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Jo, Ye-Jin</au><au>Cho, In Hee</au><au>Song, Chi Kwang</au><au>Shin, Hye Won</au><au>Kim, Young-Suk</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Comparison of Fermented Soybean Paste (Doenjang) Prepared by Different Methods Based on Profiling of Volatile Compounds</atitle><jtitle>Journal of food science</jtitle><addtitle>J Food Sci</addtitle><date>2011-04</date><risdate>2011</risdate><volume>76</volume><issue>3</issue><spage>C368</spage><epage>C379</epage><pages>C368-C379</pages><issn>0022-1147</issn><eissn>1750-3841</eissn><coden>JFDSAZ</coden><abstract>:  In this study, 2 different extraction methods, namely solvent‐assisted flavor evaporation (SAFE) and solid‐phase microextraction (SPME), were employed to investigate the comprehensive volatile profile of Doenjang (one of Korean fermented soybean pastes) efficiently. Quantitatively, major volatiles of Doenjang isolated by SAFE were 3‐methylbutanoic acid, butanoic acid, 3‐hydroxy‐2‐methyl‐4H‐pyran‐4‐one (maltol), ethyl 2‐methylbutanoate, 2‐methylpropanoic acid, tetramethylpyrazine, and 4‐ethyl‐2‐methoxyphenol, while ethanol, ethenylbenzene, ethyl benzoate, ethyl linoleate, ethyl acetate, ethyl butanoate, tetramethylpyrazine, and ethyl 2‐methylpropanoate extracted by SPME. In addition, volatile profiling that applied principal component analysis to gas chromatography‐mass spectrometry datasets allowed Doenjang samples that had been prepared using different traditional and commercial methods to be discriminated, and the volatile compounds that contributed to their discrimination were assigned. The major volatiles that were related to differentiation of traditional and commercial Doenjang samples were 2‐pentylfuran, 4‐ethylphenol, dihydro‐5‐methyl‐2(3H)‐furanone, butanoic acid, pyrazines (for example, 2‐ethyl‐5‐methylpyrazine and 2,3‐dimethylpyrazine), esters (for example, ethyl 4‐methylpentanoate and diethyl succinate), maltol, dimethyl disulfide, 2‐ and 3‐methylbutanal, hexanal, 4‐vinylphenol, and ethanol.</abstract><cop>Malden, USA</cop><pub>Blackwell Publishing Inc</pub><pmid>21535802</pmid><doi>10.1111/j.1750-3841.2011.02068.x</doi><tpages>12</tpages><oa>free_for_read</oa></addata></record>
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subjects Aspergillus - metabolism
Bacillus subtilis - metabolism
Biological and medical sciences
Chromatography
Condiments - analysis
Condiments - microbiology
Evaporation
Extraction processes
Fermentation
fermented soybean paste (Doenjang)
Food Analysis - methods
Food Handling - methods
Food industries
Food science
Fruit and vegetable industries
Fundamental and applied biological sciences. Psychology
Gas Chromatography-Mass Spectrometry
Mass spectrometry
Mucorales - metabolism
Principal Component Analysis
Principal components analysis
Republic of Korea
Solid Phase Microextraction
Soy Foods - analysis
Soy Foods - microbiology
Soybeans
volatile compounds
Volatile Organic Compounds - analysis
volatile profiling
title Comparison of Fermented Soybean Paste (Doenjang) Prepared by Different Methods Based on Profiling of Volatile Compounds
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