Calibration of GC-FID and IR spectrometric methods for determination of high boiling petroleum hydrocarbons in environmental samples
Calibration problems connected with the determination of C^sub 20^-C^sub 44^ petroleum hydrocarbons by gas chromatography - flame ionization detection (GC-FID) and IR spectrometric methods were studied in this paper. It has been found that the mass responses and mass response factors of FID determin...
Gespeichert in:
| Veröffentlicht in: | Water, air, and soil pollution air, and soil pollution, 2004-03, Vol.153 (1-4), p.329-341 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 341 |
|---|---|
| container_issue | 1-4 |
| container_start_page | 329 |
| container_title | Water, air, and soil pollution |
| container_volume | 153 |
| creator | KRUPCIK, Jan OSWALD, Peter OKTAVEC, Drahomir ARMSTRONG, Daniel W |
| description | Calibration problems connected with the determination of C^sub 20^-C^sub 44^ petroleum hydrocarbons by gas chromatography - flame ionization detection (GC-FID) and IR spectrometric methods were studied in this paper. It has been found that the mass responses and mass response factors of FID determined by capillary GC-FID as well as by IR spectrometry, at wave number 2959 and 2924 cm^sup -1^, of high boiling petroleum distillation fractions (in the range C^sub 20^-C^sub 46^) are not constant. Moreover, it was found that mass response factors for differentpetroleum oils that have the same boiling temperature interval might differ up to 1.5 fold both for FID and IRD methods, dependingon their hydrocarbon group composition. However, calibration of the IR spectrometric method using the empirical equations proposed in DIN 38 409, Part 18, norm (for the determination of total petroleumhydrocarbons in waters polluted with high boiled petroleum fractions)gave results which overlapped within ±10% of the expected values.[PUBLICATION ABSTRACT] |
| doi_str_mv | 10.1023/B:WATE.0000019957.61544.bb |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_869567646</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2136865921</sourcerecordid><originalsourceid>FETCH-LOGICAL-a373t-48e1dc16fa7badb6726990e2b1558a39558dc74a8d797a69d33878b5d47463e3</originalsourceid><addsrcrecordid>eNpdkUtr3DAUhUVpodNJ_4MIlKw8sSxLsrJLJo8OBAJloEtx9XBGQZYcyRPIPj88niQ00Lu4Z_Odcy8chI5JvSJ1Q08vzv6eb69W9WGIlEysOGFtu9L6C1oQJmjVSNp8RYu6bmXFpZDf0Y9SHg687MQCvawheJ1h8ini1OObdXW9ucQQLd78wWV0ZsppcFP2Bs-yS7bgPmVs3eTy4OM_487f77BOPvh4j8fZkILbD3j3bHMykHWKBfuIXXzyOcXBxQkCLjCMwZUj9K2HUNzPD12i7fXVdv27ur272azPbyuggk5V2zliDeE9CA1Wc9FwKWvXaMJYB1TO2xrRQmeFFMClpbQTnWa2FS2nji7RyXvsmNPj3pVJDb4YFwJEl_ZFdVwyLvjMLtHxf-RD2uc4_6YEq6loWNvN0Nk7ZHIqJbtejdkPkJ8VqdWhHXWhDu2oz3bUWztK69n86-MCFAOhzxCNL58JjJNGSkpfAYVdkso</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>750372548</pqid></control><display><type>article</type><title>Calibration of GC-FID and IR spectrometric methods for determination of high boiling petroleum hydrocarbons in environmental samples</title><source>SpringerNature Journals</source><creator>KRUPCIK, Jan ; OSWALD, Peter ; OKTAVEC, Drahomir ; ARMSTRONG, Daniel W</creator><creatorcontrib>KRUPCIK, Jan ; OSWALD, Peter ; OKTAVEC, Drahomir ; ARMSTRONG, Daniel W</creatorcontrib><description>Calibration problems connected with the determination of C^sub 20^-C^sub 44^ petroleum hydrocarbons by gas chromatography - flame ionization detection (GC-FID) and IR spectrometric methods were studied in this paper. It has been found that the mass responses and mass response factors of FID determined by capillary GC-FID as well as by IR spectrometry, at wave number 2959 and 2924 cm^sup -1^, of high boiling petroleum distillation fractions (in the range C^sub 20^-C^sub 46^) are not constant. Moreover, it was found that mass response factors for differentpetroleum oils that have the same boiling temperature interval might differ up to 1.5 fold both for FID and IRD methods, dependingon their hydrocarbon group composition. However, calibration of the IR spectrometric method using the empirical equations proposed in DIN 38 409, Part 18, norm (for the determination of total petroleumhydrocarbons in waters polluted with high boiled petroleum fractions)gave results which overlapped within ±10% of the expected values.[PUBLICATION ABSTRACT]</description><identifier>ISSN: 0049-6979</identifier><identifier>EISSN: 1573-2932</identifier><identifier>DOI: 10.1023/B:WATE.0000019957.61544.bb</identifier><identifier>CODEN: WAPLAC</identifier><language>eng</language><publisher>Dordrecht: Springer</publisher><subject>Analytical chemistry ; Applied sciences ; Boiling ; Calibration ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Distillation ; Environmental monitoring ; Exact sciences and technology ; Gas chromatographic methods ; Gas chromatography ; Global environmental pollution ; Hydrocarbons ; Ionization ; Methods ; Petroleum ; Petroleum hydrocarbons ; Pollution ; Spectrometric and optical methods ; Spectrometry</subject><ispartof>Water, air, and soil pollution, 2004-03, Vol.153 (1-4), p.329-341</ispartof><rights>2004 INIST-CNRS</rights><rights>Kluwer Academic Publishers 2004</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a373t-48e1dc16fa7badb6726990e2b1558a39558dc74a8d797a69d33878b5d47463e3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=15612993$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>KRUPCIK, Jan</creatorcontrib><creatorcontrib>OSWALD, Peter</creatorcontrib><creatorcontrib>OKTAVEC, Drahomir</creatorcontrib><creatorcontrib>ARMSTRONG, Daniel W</creatorcontrib><title>Calibration of GC-FID and IR spectrometric methods for determination of high boiling petroleum hydrocarbons in environmental samples</title><title>Water, air, and soil pollution</title><description>Calibration problems connected with the determination of C^sub 20^-C^sub 44^ petroleum hydrocarbons by gas chromatography - flame ionization detection (GC-FID) and IR spectrometric methods were studied in this paper. It has been found that the mass responses and mass response factors of FID determined by capillary GC-FID as well as by IR spectrometry, at wave number 2959 and 2924 cm^sup -1^, of high boiling petroleum distillation fractions (in the range C^sub 20^-C^sub 46^) are not constant. Moreover, it was found that mass response factors for differentpetroleum oils that have the same boiling temperature interval might differ up to 1.5 fold both for FID and IRD methods, dependingon their hydrocarbon group composition. However, calibration of the IR spectrometric method using the empirical equations proposed in DIN 38 409, Part 18, norm (for the determination of total petroleumhydrocarbons in waters polluted with high boiled petroleum fractions)gave results which overlapped within ±10% of the expected values.[PUBLICATION ABSTRACT]</description><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Boiling</subject><subject>Calibration</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Distillation</subject><subject>Environmental monitoring</subject><subject>Exact sciences and technology</subject><subject>Gas chromatographic methods</subject><subject>Gas chromatography</subject><subject>Global environmental pollution</subject><subject>Hydrocarbons</subject><subject>Ionization</subject><subject>Methods</subject><subject>Petroleum</subject><subject>Petroleum hydrocarbons</subject><subject>Pollution</subject><subject>Spectrometric and optical methods</subject><subject>Spectrometry</subject><issn>0049-6979</issn><issn>1573-2932</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2004</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNpdkUtr3DAUhUVpodNJ_4MIlKw8sSxLsrJLJo8OBAJloEtx9XBGQZYcyRPIPj88niQ00Lu4Z_Odcy8chI5JvSJ1Q08vzv6eb69W9WGIlEysOGFtu9L6C1oQJmjVSNp8RYu6bmXFpZDf0Y9SHg687MQCvawheJ1h8ini1OObdXW9ucQQLd78wWV0ZsppcFP2Bs-yS7bgPmVs3eTy4OM_487f77BOPvh4j8fZkILbD3j3bHMykHWKBfuIXXzyOcXBxQkCLjCMwZUj9K2HUNzPD12i7fXVdv27ur272azPbyuggk5V2zliDeE9CA1Wc9FwKWvXaMJYB1TO2xrRQmeFFMClpbQTnWa2FS2nji7RyXvsmNPj3pVJDb4YFwJEl_ZFdVwyLvjMLtHxf-RD2uc4_6YEq6loWNvN0Nk7ZHIqJbtejdkPkJ8VqdWhHXWhDu2oz3bUWztK69n86-MCFAOhzxCNL58JjJNGSkpfAYVdkso</recordid><startdate>20040301</startdate><enddate>20040301</enddate><creator>KRUPCIK, Jan</creator><creator>OSWALD, Peter</creator><creator>OKTAVEC, Drahomir</creator><creator>ARMSTRONG, Daniel W</creator><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QH</scope><scope>7T7</scope><scope>7TV</scope><scope>7U7</scope><scope>7UA</scope><scope>7WY</scope><scope>7WZ</scope><scope>7X2</scope><scope>7X7</scope><scope>7XB</scope><scope>87Z</scope><scope>88E</scope><scope>88I</scope><scope>8C1</scope><scope>8FD</scope><scope>8FE</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>8FL</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>C1K</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>F1W</scope><scope>FR3</scope><scope>FRNLG</scope><scope>FYUFA</scope><scope>F~G</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>H96</scope><scope>H97</scope><scope>HCIFZ</scope><scope>K60</scope><scope>K6~</scope><scope>K9.</scope><scope>L.-</scope><scope>L.G</scope><scope>M0C</scope><scope>M0K</scope><scope>M0S</scope><scope>M1P</scope><scope>M2P</scope><scope>P64</scope><scope>PATMY</scope><scope>PCBAR</scope><scope>PQBIZ</scope><scope>PQBZA</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PYCSY</scope><scope>Q9U</scope><scope>7ST</scope><scope>7TN</scope><scope>SOI</scope></search><sort><creationdate>20040301</creationdate><title>Calibration of GC-FID and IR spectrometric methods for determination of high boiling petroleum hydrocarbons in environmental samples</title><author>KRUPCIK, Jan ; OSWALD, Peter ; OKTAVEC, Drahomir ; ARMSTRONG, Daniel W</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a373t-48e1dc16fa7badb6726990e2b1558a39558dc74a8d797a69d33878b5d47463e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2004</creationdate><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Boiling</topic><topic>Calibration</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Distillation</topic><topic>Environmental monitoring</topic><topic>Exact sciences and technology</topic><topic>Gas chromatographic methods</topic><topic>Gas chromatography</topic><topic>Global environmental pollution</topic><topic>Hydrocarbons</topic><topic>Ionization</topic><topic>Methods</topic><topic>Petroleum</topic><topic>Petroleum hydrocarbons</topic><topic>Pollution</topic><topic>Spectrometric and optical methods</topic><topic>Spectrometry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>KRUPCIK, Jan</creatorcontrib><creatorcontrib>OSWALD, Peter</creatorcontrib><creatorcontrib>OKTAVEC, Drahomir</creatorcontrib><creatorcontrib>ARMSTRONG, Daniel W</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Aqualine</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Pollution Abstracts</collection><collection>Toxicology Abstracts</collection><collection>Water Resources Abstracts</collection><collection>Access via ABI/INFORM (ProQuest)</collection><collection>ABI/INFORM Global (PDF only)</collection><collection>Agricultural Science Collection</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ABI/INFORM Global (Alumni Edition)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>Public Health Database</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ABI/INFORM Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Business Premium Collection</collection><collection>Natural Science Collection</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Engineering Research Database</collection><collection>Business Premium Collection (Alumni)</collection><collection>Health Research Premium Collection</collection><collection>ABI/INFORM Global (Corporate)</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 2: Ocean Technology, Policy & Non-Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 3: Aquatic Pollution & Environmental Quality</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Business Collection (Alumni Edition)</collection><collection>ProQuest Business Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>ABI/INFORM Professional Advanced</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><collection>ABI/INFORM Global</collection><collection>Agricultural Science Database</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Science Database</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Environmental Science Database</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>ProQuest One Business</collection><collection>ProQuest One Business (Alumni)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Environmental Science Collection</collection><collection>ProQuest Central Basic</collection><collection>Environment Abstracts</collection><collection>Oceanic Abstracts</collection><collection>Environment Abstracts</collection><jtitle>Water, air, and soil pollution</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>KRUPCIK, Jan</au><au>OSWALD, Peter</au><au>OKTAVEC, Drahomir</au><au>ARMSTRONG, Daniel W</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Calibration of GC-FID and IR spectrometric methods for determination of high boiling petroleum hydrocarbons in environmental samples</atitle><jtitle>Water, air, and soil pollution</jtitle><date>2004-03-01</date><risdate>2004</risdate><volume>153</volume><issue>1-4</issue><spage>329</spage><epage>341</epage><pages>329-341</pages><issn>0049-6979</issn><eissn>1573-2932</eissn><coden>WAPLAC</coden><abstract>Calibration problems connected with the determination of C^sub 20^-C^sub 44^ petroleum hydrocarbons by gas chromatography - flame ionization detection (GC-FID) and IR spectrometric methods were studied in this paper. It has been found that the mass responses and mass response factors of FID determined by capillary GC-FID as well as by IR spectrometry, at wave number 2959 and 2924 cm^sup -1^, of high boiling petroleum distillation fractions (in the range C^sub 20^-C^sub 46^) are not constant. Moreover, it was found that mass response factors for differentpetroleum oils that have the same boiling temperature interval might differ up to 1.5 fold both for FID and IRD methods, dependingon their hydrocarbon group composition. However, calibration of the IR spectrometric method using the empirical equations proposed in DIN 38 409, Part 18, norm (for the determination of total petroleumhydrocarbons in waters polluted with high boiled petroleum fractions)gave results which overlapped within ±10% of the expected values.[PUBLICATION ABSTRACT]</abstract><cop>Dordrecht</cop><pub>Springer</pub><doi>10.1023/B:WATE.0000019957.61544.bb</doi><tpages>13</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0049-6979 |
| ispartof | Water, air, and soil pollution, 2004-03, Vol.153 (1-4), p.329-341 |
| issn | 0049-6979 1573-2932 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_869567646 |
| source | SpringerNature Journals |
| subjects | Analytical chemistry Applied sciences Boiling Calibration Chemistry Chromatographic methods and physical methods associated with chromatography Distillation Environmental monitoring Exact sciences and technology Gas chromatographic methods Gas chromatography Global environmental pollution Hydrocarbons Ionization Methods Petroleum Petroleum hydrocarbons Pollution Spectrometric and optical methods Spectrometry |
| title | Calibration of GC-FID and IR spectrometric methods for determination of high boiling petroleum hydrocarbons in environmental samples |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-23T20%3A57%3A40IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Calibration%20of%20GC-FID%20and%20IR%20spectrometric%20methods%20for%20determination%20of%20high%20boiling%20petroleum%20hydrocarbons%20in%20environmental%20samples&rft.jtitle=Water,%20air,%20and%20soil%20pollution&rft.au=KRUPCIK,%20Jan&rft.date=2004-03-01&rft.volume=153&rft.issue=1-4&rft.spage=329&rft.epage=341&rft.pages=329-341&rft.issn=0049-6979&rft.eissn=1573-2932&rft.coden=WAPLAC&rft_id=info:doi/10.1023/B:WATE.0000019957.61544.bb&rft_dat=%3Cproquest_cross%3E2136865921%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=750372548&rft_id=info:pmid/&rfr_iscdi=true |