Polymorphic and coherency transition of Y–Al complex oxide particles with extrusion temperature in an Al-alloyed high-Cr oxide dispersion strengthened ferritic steel

The phase and metal/oxide interface structure of the nanometer-scale particles in an Al-alloyed high-Cr oxide dispersion strengthened ferritic steel extruded at 1150 °C and 1050 °C were characterized by high-resolution transmission electron microscopy and diffraction contrast techniques, including w...

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Veröffentlicht in:Acta materialia 2011-02, Vol.59 (3), p.992-1002
Hauptverfasser: Dou, P., Kimura, A., Okuda, T., Inoue, M., Ukai, S., Ohnuki, S., Fujisawa, T., Abe, F.
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container_end_page 1002
container_issue 3
container_start_page 992
container_title Acta materialia
container_volume 59
creator Dou, P.
Kimura, A.
Okuda, T.
Inoue, M.
Ukai, S.
Ohnuki, S.
Fujisawa, T.
Abe, F.
description The phase and metal/oxide interface structure of the nanometer-scale particles in an Al-alloyed high-Cr oxide dispersion strengthened ferritic steel extruded at 1150 °C and 1050 °C were characterized by high-resolution transmission electron microscopy and diffraction contrast techniques, including weak beam electron microscopy. After extrusion at 1150 °C, yttrium–aluminum–hexagonal (YAH, YAlO 3) and yttrium–aluminum–perovskite (YAP, YAlO 3) oxides (diameter ⩽10 nm) constitute ∼55% and 38% of the particles, respectively; ∼78% of the particles (4.5–10 nm in diameter), which include 40% YAH oxide and 38% YAP phase with misfit (translational) moiré fringe spacing of 2.15 nm and 1.65 nm, respectively, are semi-coherent with the matrix. After extrusion at 1050 °C, almost all the particles are YAH phase, and ∼86.5% (diameter
doi_str_mv 10.1016/j.actamat.2010.10.026
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After extrusion at 1150 °C, yttrium–aluminum–hexagonal (YAH, YAlO 3) and yttrium–aluminum–perovskite (YAP, YAlO 3) oxides (diameter ⩽10 nm) constitute ∼55% and 38% of the particles, respectively; ∼78% of the particles (4.5–10 nm in diameter), which include 40% YAH oxide and 38% YAP phase with misfit (translational) moiré fringe spacing of 2.15 nm and 1.65 nm, respectively, are semi-coherent with the matrix. After extrusion at 1050 °C, almost all the particles are YAH phase, and ∼86.5% (diameter &lt;4.5 nm) are coherent with the matrix. The coherency of the oxides is size dependent. 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After extrusion at 1150 °C, yttrium–aluminum–hexagonal (YAH, YAlO 3) and yttrium–aluminum–perovskite (YAP, YAlO 3) oxides (diameter ⩽10 nm) constitute ∼55% and 38% of the particles, respectively; ∼78% of the particles (4.5–10 nm in diameter), which include 40% YAH oxide and 38% YAP phase with misfit (translational) moiré fringe spacing of 2.15 nm and 1.65 nm, respectively, are semi-coherent with the matrix. After extrusion at 1050 °C, almost all the particles are YAH phase, and ∼86.5% (diameter &lt;4.5 nm) are coherent with the matrix. The coherency of the oxides is size dependent. 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After extrusion at 1150 °C, yttrium–aluminum–hexagonal (YAH, YAlO 3) and yttrium–aluminum–perovskite (YAP, YAlO 3) oxides (diameter ⩽10 nm) constitute ∼55% and 38% of the particles, respectively; ∼78% of the particles (4.5–10 nm in diameter), which include 40% YAH oxide and 38% YAP phase with misfit (translational) moiré fringe spacing of 2.15 nm and 1.65 nm, respectively, are semi-coherent with the matrix. After extrusion at 1050 °C, almost all the particles are YAH phase, and ∼86.5% (diameter &lt;4.5 nm) are coherent with the matrix. The coherency of the oxides is size dependent. The crystallographic orientation correlations of the oxides and matrix were found.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.actamat.2010.10.026</doi><tpages>11</tpages></addata></record>
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subjects Aluminum
Coherence
Coherency
Dispersions
Electron microscopy
Extrusion
Ferritic stainless steels
Interface structure
Misfit moiré fringe
Oxide dispersion strengthened steel
Oxides
Structural steels
Transmission electron microscopy
title Polymorphic and coherency transition of Y–Al complex oxide particles with extrusion temperature in an Al-alloyed high-Cr oxide dispersion strengthened ferritic steel
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