Facile solution synthesis and characterization of porous cubic-shaped superstructure of ZnAl2O4
Porous and cubic-shaped superstructure of ZnAl2O4 was successfully synthesized by a facile wet chemical solution-phase method. The structural properties of the samples were systematically investigated by X-ray powder diffraction (XRD), Brunauer-Emmet-Teller (BET), scanning electron microscopy (SEM),...
Gespeichert in:
| Veröffentlicht in: | Materials letters 2011-01, Vol.65 (2), p.194-197 |
|---|---|
| Hauptverfasser: | , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 197 |
|---|---|
| container_issue | 2 |
| container_start_page | 194 |
| container_title | Materials letters |
| container_volume | 65 |
| creator | Zhu, Zhengru Li, Xinyong Zhao, Qidong Liu, Shaomin Hu, Xijun Chen, Guohua |
| description | Porous and cubic-shaped superstructure of ZnAl2O4 was successfully synthesized by a facile wet chemical solution-phase method. The structural properties of the samples were systematically investigated by X-ray powder diffraction (XRD), Brunauer-Emmet-Teller (BET), scanning electron microscopy (SEM), energy-dispersive spectra (EDS), and Fourier transform infrared spectroscopy (FT-IR) techniques. The characterization results revealed that the structure of the cubic-shaped ZnAl2O4 was an inverse spinel structure. The sample prepared by a solution-phase chemical method has a higher surface area and monomodal pore size distributions. Furthermore, the valence states and the surface chemical compositions of ZnAl2O4 were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare cubic-shaped ZnAl2O4 in large scale, which broadens their practical applications. |
| doi_str_mv | 10.1016/j.matlet.2010.09.085 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_861534763</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>861534763</sourcerecordid><originalsourceid>FETCH-LOGICAL-c349t-d9149f5e372b6c169075735a31f79c217c2127d467c9400c57cb4a5287f6ef953</originalsourceid><addsrcrecordid>eNotkE1LAzEQhnNQsFb_gYfcPO2abL6aYylWhUIvCuIlpNmEpmx310xyqL_erfUwvDDvwzA8CD1QUlNC5dOhPtrc-Vw3ZFoRXZOFuEKzqVKVUOrzBt0CHAghXBM-Q2ZtXew8hqErOQ49hlOf9x4iYNu32O1tsi77FH_sXz0EPA5pKIBd2UVXwd6OvsVQRp8gp-JySf5MffXLrtnyO3QdbAf-_j_n6GP9_L56rTbbl7fVclM5xnWuWk25DsIz1eyko1ITJRQTltGgtGuomqZRLZfKaU6IE8rtuBXNQgXpgxZsjh4vd8c0fBcP2RwjON91tvfTt2YhqWBcSTaR_EK6NAAkH8yY4tGmk6HEnBWag7koNGeFhmgzKWS_URxp1w</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>861534763</pqid></control><display><type>article</type><title>Facile solution synthesis and characterization of porous cubic-shaped superstructure of ZnAl2O4</title><source>ScienceDirect Journals (5 years ago - present)</source><creator>Zhu, Zhengru ; Li, Xinyong ; Zhao, Qidong ; Liu, Shaomin ; Hu, Xijun ; Chen, Guohua</creator><creatorcontrib>Zhu, Zhengru ; Li, Xinyong ; Zhao, Qidong ; Liu, Shaomin ; Hu, Xijun ; Chen, Guohua</creatorcontrib><description>Porous and cubic-shaped superstructure of ZnAl2O4 was successfully synthesized by a facile wet chemical solution-phase method. The structural properties of the samples were systematically investigated by X-ray powder diffraction (XRD), Brunauer-Emmet-Teller (BET), scanning electron microscopy (SEM), energy-dispersive spectra (EDS), and Fourier transform infrared spectroscopy (FT-IR) techniques. The characterization results revealed that the structure of the cubic-shaped ZnAl2O4 was an inverse spinel structure. The sample prepared by a solution-phase chemical method has a higher surface area and monomodal pore size distributions. Furthermore, the valence states and the surface chemical compositions of ZnAl2O4 were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare cubic-shaped ZnAl2O4 in large scale, which broadens their practical applications.</description><identifier>ISSN: 0167-577X</identifier><identifier>DOI: 10.1016/j.matlet.2010.09.085</identifier><language>eng</language><subject>Diffraction ; Fourier transforms ; Infrared spectroscopy ; Inverse ; Scanning electron microscopy ; Spectra ; Superstructures ; X-ray photoelectron spectroscopy ; X-rays</subject><ispartof>Materials letters, 2011-01, Vol.65 (2), p.194-197</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c349t-d9149f5e372b6c169075735a31f79c217c2127d467c9400c57cb4a5287f6ef953</citedby><cites>FETCH-LOGICAL-c349t-d9149f5e372b6c169075735a31f79c217c2127d467c9400c57cb4a5287f6ef953</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>Zhu, Zhengru</creatorcontrib><creatorcontrib>Li, Xinyong</creatorcontrib><creatorcontrib>Zhao, Qidong</creatorcontrib><creatorcontrib>Liu, Shaomin</creatorcontrib><creatorcontrib>Hu, Xijun</creatorcontrib><creatorcontrib>Chen, Guohua</creatorcontrib><title>Facile solution synthesis and characterization of porous cubic-shaped superstructure of ZnAl2O4</title><title>Materials letters</title><description>Porous and cubic-shaped superstructure of ZnAl2O4 was successfully synthesized by a facile wet chemical solution-phase method. The structural properties of the samples were systematically investigated by X-ray powder diffraction (XRD), Brunauer-Emmet-Teller (BET), scanning electron microscopy (SEM), energy-dispersive spectra (EDS), and Fourier transform infrared spectroscopy (FT-IR) techniques. The characterization results revealed that the structure of the cubic-shaped ZnAl2O4 was an inverse spinel structure. The sample prepared by a solution-phase chemical method has a higher surface area and monomodal pore size distributions. Furthermore, the valence states and the surface chemical compositions of ZnAl2O4 were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare cubic-shaped ZnAl2O4 in large scale, which broadens their practical applications.</description><subject>Diffraction</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Inverse</subject><subject>Scanning electron microscopy</subject><subject>Spectra</subject><subject>Superstructures</subject><subject>X-ray photoelectron spectroscopy</subject><subject>X-rays</subject><issn>0167-577X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNotkE1LAzEQhnNQsFb_gYfcPO2abL6aYylWhUIvCuIlpNmEpmx310xyqL_erfUwvDDvwzA8CD1QUlNC5dOhPtrc-Vw3ZFoRXZOFuEKzqVKVUOrzBt0CHAghXBM-Q2ZtXew8hqErOQ49hlOf9x4iYNu32O1tsi77FH_sXz0EPA5pKIBd2UVXwd6OvsVQRp8gp-JySf5MffXLrtnyO3QdbAf-_j_n6GP9_L56rTbbl7fVclM5xnWuWk25DsIz1eyko1ITJRQTltGgtGuomqZRLZfKaU6IE8rtuBXNQgXpgxZsjh4vd8c0fBcP2RwjON91tvfTt2YhqWBcSTaR_EK6NAAkH8yY4tGmk6HEnBWag7koNGeFhmgzKWS_URxp1w</recordid><startdate>20110131</startdate><enddate>20110131</enddate><creator>Zhu, Zhengru</creator><creator>Li, Xinyong</creator><creator>Zhao, Qidong</creator><creator>Liu, Shaomin</creator><creator>Hu, Xijun</creator><creator>Chen, Guohua</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20110131</creationdate><title>Facile solution synthesis and characterization of porous cubic-shaped superstructure of ZnAl2O4</title><author>Zhu, Zhengru ; Li, Xinyong ; Zhao, Qidong ; Liu, Shaomin ; Hu, Xijun ; Chen, Guohua</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c349t-d9149f5e372b6c169075735a31f79c217c2127d467c9400c57cb4a5287f6ef953</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Diffraction</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Inverse</topic><topic>Scanning electron microscopy</topic><topic>Spectra</topic><topic>Superstructures</topic><topic>X-ray photoelectron spectroscopy</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhu, Zhengru</creatorcontrib><creatorcontrib>Li, Xinyong</creatorcontrib><creatorcontrib>Zhao, Qidong</creatorcontrib><creatorcontrib>Liu, Shaomin</creatorcontrib><creatorcontrib>Hu, Xijun</creatorcontrib><creatorcontrib>Chen, Guohua</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhu, Zhengru</au><au>Li, Xinyong</au><au>Zhao, Qidong</au><au>Liu, Shaomin</au><au>Hu, Xijun</au><au>Chen, Guohua</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Facile solution synthesis and characterization of porous cubic-shaped superstructure of ZnAl2O4</atitle><jtitle>Materials letters</jtitle><date>2011-01-31</date><risdate>2011</risdate><volume>65</volume><issue>2</issue><spage>194</spage><epage>197</epage><pages>194-197</pages><issn>0167-577X</issn><abstract>Porous and cubic-shaped superstructure of ZnAl2O4 was successfully synthesized by a facile wet chemical solution-phase method. The structural properties of the samples were systematically investigated by X-ray powder diffraction (XRD), Brunauer-Emmet-Teller (BET), scanning electron microscopy (SEM), energy-dispersive spectra (EDS), and Fourier transform infrared spectroscopy (FT-IR) techniques. The characterization results revealed that the structure of the cubic-shaped ZnAl2O4 was an inverse spinel structure. The sample prepared by a solution-phase chemical method has a higher surface area and monomodal pore size distributions. Furthermore, the valence states and the surface chemical compositions of ZnAl2O4 were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare cubic-shaped ZnAl2O4 in large scale, which broadens their practical applications.</abstract><doi>10.1016/j.matlet.2010.09.085</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0167-577X |
| ispartof | Materials letters, 2011-01, Vol.65 (2), p.194-197 |
| issn | 0167-577X |
| language | eng |
| recordid | cdi_proquest_miscellaneous_861534763 |
| source | ScienceDirect Journals (5 years ago - present) |
| subjects | Diffraction Fourier transforms Infrared spectroscopy Inverse Scanning electron microscopy Spectra Superstructures X-ray photoelectron spectroscopy X-rays |
| title | Facile solution synthesis and characterization of porous cubic-shaped superstructure of ZnAl2O4 |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-12T22%3A31%3A50IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Facile%20solution%20synthesis%20and%20characterization%20of%20porous%20cubic-shaped%20superstructure%20of%20ZnAl2O4&rft.jtitle=Materials%20letters&rft.au=Zhu,%20Zhengru&rft.date=2011-01-31&rft.volume=65&rft.issue=2&rft.spage=194&rft.epage=197&rft.pages=194-197&rft.issn=0167-577X&rft_id=info:doi/10.1016/j.matlet.2010.09.085&rft_dat=%3Cproquest_cross%3E861534763%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=861534763&rft_id=info:pmid/&rfr_iscdi=true |