First Synthesis of Dodecasubstituted Porphycenes

The synthesis of dodecasubstituted porphycenes has not been reported, to date. Herein, the preparation of tetramethyloctaethylporphycene by a McMurry‐type coupling of 3,3′,4,4′‐tetraethyl‐5,5′‐diformyl‐2,2′‐bipyrrole was attempted at first, but dodecasubstituted porphycene was not successfully obtai...

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Veröffentlicht in:	Chemistry : a European journal 2011-03, Vol.17 (12), p.3376-3383
Hauptverfasser:	Kuzuhara, Daiki, Yamada, Hiroko, Yano, Keiko, Okujima, Tetsuo, Mori, Shigeki, Uno, Hidemitsu
Format:	Artikel
Sprache:	eng
Schlagworte:	Chemistry Crystal structure Hydrogen bonding Joining NMR Nuclear magnetic resonance porphyrinoids Spectra Spectroscopy Spectrum analysis structure elucidation substituent effects Synthesis synthesis design X-rays
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