Development and validation of an HPLC-FLD method for rapid determination of histamine in skipjack tuna fish (Katsuwonus pelamis)
► This study compared and validated two HPLC methods. ► Recoveries greater than 55% could not be observed by HPLC-UV. ► Derivatization with pre-column o-phthalaldehyde was found efficient. ► Good recoveries were obtained at all spiking levels by HPLC-FLD. This study compared and validated two method...
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| Veröffentlicht in: | Food chemistry 2011-05, Vol.126 (2), p.756-761 |
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| creator | Tahmouzi, Saeed Khaksar, Ramin Ghasemlou, Mehran |
| description | ► This study compared and validated two HPLC methods. ► Recoveries greater than 55% could not be observed by HPLC-UV. ► Derivatization with pre-column o-phthalaldehyde was found efficient. ► Good recoveries were obtained at all spiking levels by HPLC-FLD.
This study compared and validated two methods of high-performance liquid chromatography: fluorescence detection (HPLC-FLD) and UV–Vis detection. Recoveries greater than 55% at all spiking levels using UV–Vis detection could not be obtained. However, derivatization with pre-column o-phthalaldehyde (OPA) was found to efficiently enhance the method sensitivity. The analytical method was validated based on the following criteria: linearity, sensitivity, accuracy, precision, repeatability, and recovery. For fluorescence detection, excellent linear correlation with R2=0.9977 was observed over the range of 5.0 to 100.0mg/L. The minimum detection limit was calculated to be 1.5mg/kg, while the limit of quantification (LOQ) value of the validated method was determined to be 4.5mg/kg. Good recoveries (RSD%=1.35) were obtained at all spiking levels ranging between 0 and 200mg/kg. The proposed method was found to be suitable, selective, and rapid for the determination of histamine. |
| doi_str_mv | 10.1016/j.foodchem.2010.11.060 |
| format | Article |
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This study compared and validated two methods of high-performance liquid chromatography: fluorescence detection (HPLC-FLD) and UV–Vis detection. Recoveries greater than 55% at all spiking levels using UV–Vis detection could not be obtained. However, derivatization with pre-column o-phthalaldehyde (OPA) was found to efficiently enhance the method sensitivity. The analytical method was validated based on the following criteria: linearity, sensitivity, accuracy, precision, repeatability, and recovery. For fluorescence detection, excellent linear correlation with R2=0.9977 was observed over the range of 5.0 to 100.0mg/L. The minimum detection limit was calculated to be 1.5mg/kg, while the limit of quantification (LOQ) value of the validated method was determined to be 4.5mg/kg. Good recoveries (RSD%=1.35) were obtained at all spiking levels ranging between 0 and 200mg/kg. The proposed method was found to be suitable, selective, and rapid for the determination of histamine.</description><identifier>ISSN: 0308-8146</identifier><identifier>EISSN: 1873-7072</identifier><identifier>DOI: 10.1016/j.foodchem.2010.11.060</identifier><identifier>CODEN: FOCHDJ</identifier><language>eng</language><publisher>Kidlington: Elsevier Ltd</publisher><subject>Biogenic amine ; Biological and medical sciences ; detection ; equipment performance ; Fish and seafood industries ; fluorescence ; food analysis ; food composition ; food contamination ; Food industries ; food quality ; Fundamental and applied biological sciences. Psychology ; High-performance liquid chromatography ; histamine ; Katsuwonus ; Katsuwonus pelamis ; Marine ; Pelamis ; rapid methods ; scombroid poisoning ; Thunnus ; tuna ; Tuna fish ; Validation ; validity</subject><ispartof>Food chemistry, 2011-05, Vol.126 (2), p.756-761</ispartof><rights>2010 Elsevier Ltd</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c398t-c91773e3099d762ba59baea586c786ff35ab555a289ef0ab43236ab42ec31c4b3</citedby><cites>FETCH-LOGICAL-c398t-c91773e3099d762ba59baea586c786ff35ab555a289ef0ab43236ab42ec31c4b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.foodchem.2010.11.060$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>315,781,785,3551,27926,27927,45997</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=23822935$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Tahmouzi, Saeed</creatorcontrib><creatorcontrib>Khaksar, Ramin</creatorcontrib><creatorcontrib>Ghasemlou, Mehran</creatorcontrib><title>Development and validation of an HPLC-FLD method for rapid determination of histamine in skipjack tuna fish (Katsuwonus pelamis)</title><title>Food chemistry</title><description>► This study compared and validated two HPLC methods. ► Recoveries greater than 55% could not be observed by HPLC-UV. ► Derivatization with pre-column o-phthalaldehyde was found efficient. ► Good recoveries were obtained at all spiking levels by HPLC-FLD.
This study compared and validated two methods of high-performance liquid chromatography: fluorescence detection (HPLC-FLD) and UV–Vis detection. Recoveries greater than 55% at all spiking levels using UV–Vis detection could not be obtained. However, derivatization with pre-column o-phthalaldehyde (OPA) was found to efficiently enhance the method sensitivity. The analytical method was validated based on the following criteria: linearity, sensitivity, accuracy, precision, repeatability, and recovery. For fluorescence detection, excellent linear correlation with R2=0.9977 was observed over the range of 5.0 to 100.0mg/L. The minimum detection limit was calculated to be 1.5mg/kg, while the limit of quantification (LOQ) value of the validated method was determined to be 4.5mg/kg. Good recoveries (RSD%=1.35) were obtained at all spiking levels ranging between 0 and 200mg/kg. The proposed method was found to be suitable, selective, and rapid for the determination of histamine.</description><subject>Biogenic amine</subject><subject>Biological and medical sciences</subject><subject>detection</subject><subject>equipment performance</subject><subject>Fish and seafood industries</subject><subject>fluorescence</subject><subject>food analysis</subject><subject>food composition</subject><subject>food contamination</subject><subject>Food industries</subject><subject>food quality</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>High-performance liquid chromatography</subject><subject>histamine</subject><subject>Katsuwonus</subject><subject>Katsuwonus pelamis</subject><subject>Marine</subject><subject>Pelamis</subject><subject>rapid methods</subject><subject>scombroid poisoning</subject><subject>Thunnus</subject><subject>tuna</subject><subject>Tuna fish</subject><subject>Validation</subject><subject>validity</subject><issn>0308-8146</issn><issn>1873-7072</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkMuOEzEQRVsIJMLAL4A3CFh08KMf9g6UYRhEJJBg1la1u0yc6diN7Q5ix6fjKMNsWZV0dW5V6VTVc0bXjLLu7X5tQxjNDg9rTk8hW9OOPqhWTPai7mnPH1YrKqisJWu6x9WTlPaU0sLKVfXnEo84hfmAPhPwIznC5EbILngSbEnI9dftpr7aXpID5l0YiQ2RRJjdSEbMGA_O39M7lzKUAInzJN26eQ_mluTFA7Eu7cjrz5DT8iv4JZEZp4KmN0-rRxamhM_u5kV1c_Xh--a63n75-GnzflsboWSujWJ9L1BQpca-4wO0agCEVnaml521ooWhbVvgUqGlMDSCi64MjkYw0wzionp13jvH8HPBlHW5bnCawGNYkpataGSrZFPI7kyaGFKKaPUc3QHib82oPhnXe_3PuD4Z14zpYrwUX96dgGRgshG8cem-zYXkXIm2cC_OnIWg4UcszM23skhQprhgqivEuzOBxcjRYdTJOPQGRxfRZD0G979n_gJNCqSv</recordid><startdate>20110515</startdate><enddate>20110515</enddate><creator>Tahmouzi, Saeed</creator><creator>Khaksar, Ramin</creator><creator>Ghasemlou, Mehran</creator><general>Elsevier Ltd</general><general>[Amsterdam]: Elsevier Science</general><general>Elsevier</general><scope>FBQ</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7TN</scope><scope>F1W</scope><scope>H95</scope><scope>L.G</scope></search><sort><creationdate>20110515</creationdate><title>Development and validation of an HPLC-FLD method for rapid determination of histamine in skipjack tuna fish (Katsuwonus pelamis)</title><author>Tahmouzi, Saeed ; Khaksar, Ramin ; Ghasemlou, Mehran</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c398t-c91773e3099d762ba59baea586c786ff35ab555a289ef0ab43236ab42ec31c4b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Biogenic amine</topic><topic>Biological and medical sciences</topic><topic>detection</topic><topic>equipment performance</topic><topic>Fish and seafood industries</topic><topic>fluorescence</topic><topic>food analysis</topic><topic>food composition</topic><topic>food contamination</topic><topic>Food industries</topic><topic>food quality</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>High-performance liquid chromatography</topic><topic>histamine</topic><topic>Katsuwonus</topic><topic>Katsuwonus pelamis</topic><topic>Marine</topic><topic>Pelamis</topic><topic>rapid methods</topic><topic>scombroid poisoning</topic><topic>Thunnus</topic><topic>tuna</topic><topic>Tuna fish</topic><topic>Validation</topic><topic>validity</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tahmouzi, Saeed</creatorcontrib><creatorcontrib>Khaksar, Ramin</creatorcontrib><creatorcontrib>Ghasemlou, Mehran</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Oceanic Abstracts</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 1: Biological Sciences & Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><jtitle>Food chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tahmouzi, Saeed</au><au>Khaksar, Ramin</au><au>Ghasemlou, Mehran</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development and validation of an HPLC-FLD method for rapid determination of histamine in skipjack tuna fish (Katsuwonus pelamis)</atitle><jtitle>Food chemistry</jtitle><date>2011-05-15</date><risdate>2011</risdate><volume>126</volume><issue>2</issue><spage>756</spage><epage>761</epage><pages>756-761</pages><issn>0308-8146</issn><eissn>1873-7072</eissn><coden>FOCHDJ</coden><abstract>► This study compared and validated two HPLC methods. ► Recoveries greater than 55% could not be observed by HPLC-UV. ► Derivatization with pre-column o-phthalaldehyde was found efficient. ► Good recoveries were obtained at all spiking levels by HPLC-FLD.
This study compared and validated two methods of high-performance liquid chromatography: fluorescence detection (HPLC-FLD) and UV–Vis detection. Recoveries greater than 55% at all spiking levels using UV–Vis detection could not be obtained. However, derivatization with pre-column o-phthalaldehyde (OPA) was found to efficiently enhance the method sensitivity. The analytical method was validated based on the following criteria: linearity, sensitivity, accuracy, precision, repeatability, and recovery. For fluorescence detection, excellent linear correlation with R2=0.9977 was observed over the range of 5.0 to 100.0mg/L. The minimum detection limit was calculated to be 1.5mg/kg, while the limit of quantification (LOQ) value of the validated method was determined to be 4.5mg/kg. Good recoveries (RSD%=1.35) were obtained at all spiking levels ranging between 0 and 200mg/kg. The proposed method was found to be suitable, selective, and rapid for the determination of histamine.</abstract><cop>Kidlington</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.foodchem.2010.11.060</doi><tpages>6</tpages></addata></record> |
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| subjects | Biogenic amine Biological and medical sciences detection equipment performance Fish and seafood industries fluorescence food analysis food composition food contamination Food industries food quality Fundamental and applied biological sciences. Psychology High-performance liquid chromatography histamine Katsuwonus Katsuwonus pelamis Marine Pelamis rapid methods scombroid poisoning Thunnus tuna Tuna fish Validation validity |
| title | Development and validation of an HPLC-FLD method for rapid determination of histamine in skipjack tuna fish (Katsuwonus pelamis) |
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