Novel pulsed switched power supply for a fast field cycling NMR spectrometer

In this paper, we outline the operating principles of a pulsed switched power supply for a fast field-cycling nuclear magnetic resonance spectrometer. The power supply uses a variant of a four-quadrant chopper with a duty cycle that defines the average output current. With this topology only two sem...

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Veröffentlicht in:Solid state nuclear magnetic resonance 2004, Vol.25 (1), p.160-166
Hauptverfasser: Sousa, D.M., Fernandes, P.A.L., Marques, G.D., Ribeiro, A.C., Sebastião, P.J.
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Sprache:eng
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Zusammenfassung:In this paper, we outline the operating principles of a pulsed switched power supply for a fast field-cycling nuclear magnetic resonance spectrometer. The power supply uses a variant of a four-quadrant chopper with a duty cycle that defines the average output current. With this topology only two semiconductors are necessary to drive hundreds of amperes with an output power of several kilowatts. The output current ripple has a well-defined shape that can be reduced to acceptable values by a careful design of the semiconductors’ controlling circuits and drivers. A power supply prototype was tested with a home build air-core magnet operating with fields between 0 and 0.21 T. The system is computer controlled using pulse generator and data acquisition PC cards, and specific user-friendly home-developed software. A comparative proton relaxometry study in two well-known liquid crystal compounds 5CB and MBBA was performed to check the reproducibility of the T 1 measurements.
ISSN:0926-2040
1527-3326
DOI:10.1016/j.ssnmr.2003.03.026