Structural analysis of leech galactocerebrosides using 1D and 2D NMR spectroscopy, gas chromatography-mass spectrometry, and FAB mass spectrometry

Cerebrosides were isolated from the leech species, Hirudo medicinalis, and purified to homogeneity by silicic acid chromatography, followed by preparative thin-layer chromatography. Their structure was determined by spectroscopic and chemical methods. 1D and 2D 1H NMR spectroscopy, DQF-COSY and HMQC...

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Veröffentlicht in:	Carbohydrate research 1998-03, Vol.308 (1-2), p.47-55
Hauptverfasser:	Zipser, B, Bradford, J J, Hollingsworth, R I
Format:	Artikel
Sprache:	eng
Schlagworte:	Animals Cattle Chromatography, Thin Layer Galactosylceramides - blood Galactosylceramides - chemistry Galactosylceramides - isolation & purification Gas Chromatography-Mass Spectrometry Leeches - chemistry Mass Spectrometry Nuclear Magnetic Resonance, Biomolecular
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