A replica technique for extracting precipitates from zirconium alloys for transmission electron microscopy analysis
A reliable two‐stage carbon replica technique has been developed to extract precipitates from zirconium alloys. Using this technique, all precipitating phases can be extracted from Zircaloy‐2, Zr‐Cr‐Fe, and Zr‐Nb‐Fe alloys. Precipitate identification using EDS X‐ray analysis and convergent beam elec...
Gespeichert in:
| Veröffentlicht in: | Journal of electron microscopy technique 1990-08, Vol.15 (4), p.400-405 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 405 |
|---|---|
| container_issue | 4 |
| container_start_page | 400 |
| container_title | Journal of electron microscopy technique |
| container_volume | 15 |
| creator | Ng-Yelim, J. Woo, O. T. Carpenter, G. J. C. |
| description | A reliable two‐stage carbon replica technique has been developed to extract precipitates from zirconium alloys. Using this technique, all precipitating phases can be extracted from Zircaloy‐2, Zr‐Cr‐Fe, and Zr‐Nb‐Fe alloys. Precipitate identification using EDS X‐ray analysis and convergent beam electron diffraction was greatly facilitated in comparison to thin foils. In addition, the sensitivity for the detection of trace elements in particles was increased using extraction replicas. The chemical compositions of the precipitates as determined from both replica and thin foils were in excellent agreement. |
| doi_str_mv | 10.1002/jemt.1060150410 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_79964823</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>79964823</sourcerecordid><originalsourceid>FETCH-LOGICAL-c4120-cce08289ea1ca211846f3763706f8d8681e29efa616dbe5766c279705d6264ac3</originalsourceid><addsrcrecordid>eNqFkM1PFTEUxRsjwSe6dmXSje5G2s70Y-KKEAQMaExQEjdN6bujxc4HvX2R4a-3j_cCYeWqN7m_c3ruIeQNZx84Y2L_GvpcJsW4ZA1nz8iCS1lXzHD9nCyYbnjFpOEvyEvEa8YaLbXYJbuibrlUakHwgCaYYvCOZvC_h3CzAtqNicJtTs7nMPyiUwIfppBdBqRdGnt6F5Ifh7DqqYtxnPFeUfgB-4AYxoFCBJ9TGfrg04h-nGbqBhdnDPiK7HQuIrzevnvk-6eji8OT6uzr8enhwVnlGy5Y5T0wI0wLjnsnODeN6mqtas1UZ5ZGGQ6ihc4prpZXILVSXuhWM7lUQjXO13vk_cZ3SmM5C7Mt6TzE6AYYV2h126rGiLqA-xtwHRUTdHZKoXdptpzZdc12XbN9rLko3m6tV1c9LB_4ba9l_267d-hd7Eo1PuCjbdtope-5jxvub4gw_-9b-_no_OJJimqjDpjh9kHt0h-rdK2lvfxybL_9MNroS2V_1v8A8reowA</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>79964823</pqid></control><display><type>article</type><title>A replica technique for extracting precipitates from zirconium alloys for transmission electron microscopy analysis</title><source>MEDLINE</source><source>Access via Wiley Online Library</source><creator>Ng-Yelim, J. ; Woo, O. T. ; Carpenter, G. J. C.</creator><creatorcontrib>Ng-Yelim, J. ; Woo, O. T. ; Carpenter, G. J. C.</creatorcontrib><description>A reliable two‐stage carbon replica technique has been developed to extract precipitates from zirconium alloys. Using this technique, all precipitating phases can be extracted from Zircaloy‐2, Zr‐Cr‐Fe, and Zr‐Nb‐Fe alloys. Precipitate identification using EDS X‐ray analysis and convergent beam electron diffraction was greatly facilitated in comparison to thin foils. In addition, the sensitivity for the detection of trace elements in particles was increased using extraction replicas. The chemical compositions of the precipitates as determined from both replica and thin foils were in excellent agreement.</description><identifier>ISSN: 0741-0581</identifier><identifier>EISSN: 1553-0817</identifier><identifier>DOI: 10.1002/jemt.1060150410</identifier><identifier>PMID: 2391566</identifier><identifier>CODEN: JEMTEC</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc., A Wiley Company</publisher><subject>Alloys - analysis ; Analytical electron microscopy ; Applied sciences ; Chemical Precipitation ; Cross-disciplinary physics: materials science; rheology ; Electron Probe Microanalysis ; Exact sciences and technology ; Extraction replica ; Materials science ; Metals. Metallurgy ; Microscopy, Electron ; Phase diagrams and microstructures developed by solidification and solid-solid phase transformations ; Physics ; Zirconium - analysis ; Zr alloys</subject><ispartof>Journal of electron microscopy technique, 1990-08, Vol.15 (4), p.400-405</ispartof><rights>Copyright © 1990 Wiley‐Liss, Inc.</rights><rights>1991 INIST-CNRS</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4120-cce08289ea1ca211846f3763706f8d8681e29efa616dbe5766c279705d6264ac3</citedby><cites>FETCH-LOGICAL-c4120-cce08289ea1ca211846f3763706f8d8681e29efa616dbe5766c279705d6264ac3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fjemt.1060150410$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fjemt.1060150410$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=19476766$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/2391566$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Ng-Yelim, J.</creatorcontrib><creatorcontrib>Woo, O. T.</creatorcontrib><creatorcontrib>Carpenter, G. J. C.</creatorcontrib><title>A replica technique for extracting precipitates from zirconium alloys for transmission electron microscopy analysis</title><title>Journal of electron microscopy technique</title><addtitle>J. Elec. Microsc. Tech</addtitle><description>A reliable two‐stage carbon replica technique has been developed to extract precipitates from zirconium alloys. Using this technique, all precipitating phases can be extracted from Zircaloy‐2, Zr‐Cr‐Fe, and Zr‐Nb‐Fe alloys. Precipitate identification using EDS X‐ray analysis and convergent beam electron diffraction was greatly facilitated in comparison to thin foils. In addition, the sensitivity for the detection of trace elements in particles was increased using extraction replicas. The chemical compositions of the precipitates as determined from both replica and thin foils were in excellent agreement.</description><subject>Alloys - analysis</subject><subject>Analytical electron microscopy</subject><subject>Applied sciences</subject><subject>Chemical Precipitation</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Electron Probe Microanalysis</subject><subject>Exact sciences and technology</subject><subject>Extraction replica</subject><subject>Materials science</subject><subject>Metals. Metallurgy</subject><subject>Microscopy, Electron</subject><subject>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</subject><subject>Physics</subject><subject>Zirconium - analysis</subject><subject>Zr alloys</subject><issn>0741-0581</issn><issn>1553-0817</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1990</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkM1PFTEUxRsjwSe6dmXSje5G2s70Y-KKEAQMaExQEjdN6bujxc4HvX2R4a-3j_cCYeWqN7m_c3ruIeQNZx84Y2L_GvpcJsW4ZA1nz8iCS1lXzHD9nCyYbnjFpOEvyEvEa8YaLbXYJbuibrlUakHwgCaYYvCOZvC_h3CzAtqNicJtTs7nMPyiUwIfppBdBqRdGnt6F5Ifh7DqqYtxnPFeUfgB-4AYxoFCBJ9TGfrg04h-nGbqBhdnDPiK7HQuIrzevnvk-6eji8OT6uzr8enhwVnlGy5Y5T0wI0wLjnsnODeN6mqtas1UZ5ZGGQ6ihc4prpZXILVSXuhWM7lUQjXO13vk_cZ3SmM5C7Mt6TzE6AYYV2h126rGiLqA-xtwHRUTdHZKoXdptpzZdc12XbN9rLko3m6tV1c9LB_4ba9l_267d-hd7Eo1PuCjbdtope-5jxvub4gw_-9b-_no_OJJimqjDpjh9kHt0h-rdK2lvfxybL_9MNroS2V_1v8A8reowA</recordid><startdate>199008</startdate><enddate>199008</enddate><creator>Ng-Yelim, J.</creator><creator>Woo, O. T.</creator><creator>Carpenter, G. J. C.</creator><general>Wiley Subscription Services, Inc., A Wiley Company</general><general>Liss</general><scope>BSCLL</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>199008</creationdate><title>A replica technique for extracting precipitates from zirconium alloys for transmission electron microscopy analysis</title><author>Ng-Yelim, J. ; Woo, O. T. ; Carpenter, G. J. C.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4120-cce08289ea1ca211846f3763706f8d8681e29efa616dbe5766c279705d6264ac3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1990</creationdate><topic>Alloys - analysis</topic><topic>Analytical electron microscopy</topic><topic>Applied sciences</topic><topic>Chemical Precipitation</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Electron Probe Microanalysis</topic><topic>Exact sciences and technology</topic><topic>Extraction replica</topic><topic>Materials science</topic><topic>Metals. Metallurgy</topic><topic>Microscopy, Electron</topic><topic>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</topic><topic>Physics</topic><topic>Zirconium - analysis</topic><topic>Zr alloys</topic><toplevel>online_resources</toplevel><creatorcontrib>Ng-Yelim, J.</creatorcontrib><creatorcontrib>Woo, O. T.</creatorcontrib><creatorcontrib>Carpenter, G. J. C.</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of electron microscopy technique</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ng-Yelim, J.</au><au>Woo, O. T.</au><au>Carpenter, G. J. C.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A replica technique for extracting precipitates from zirconium alloys for transmission electron microscopy analysis</atitle><jtitle>Journal of electron microscopy technique</jtitle><addtitle>J. Elec. Microsc. Tech</addtitle><date>1990-08</date><risdate>1990</risdate><volume>15</volume><issue>4</issue><spage>400</spage><epage>405</epage><pages>400-405</pages><issn>0741-0581</issn><eissn>1553-0817</eissn><coden>JEMTEC</coden><abstract>A reliable two‐stage carbon replica technique has been developed to extract precipitates from zirconium alloys. Using this technique, all precipitating phases can be extracted from Zircaloy‐2, Zr‐Cr‐Fe, and Zr‐Nb‐Fe alloys. Precipitate identification using EDS X‐ray analysis and convergent beam electron diffraction was greatly facilitated in comparison to thin foils. In addition, the sensitivity for the detection of trace elements in particles was increased using extraction replicas. The chemical compositions of the precipitates as determined from both replica and thin foils were in excellent agreement.</abstract><cop>Hoboken</cop><pub>Wiley Subscription Services, Inc., A Wiley Company</pub><pmid>2391566</pmid><doi>10.1002/jemt.1060150410</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0741-0581 |
| ispartof | Journal of electron microscopy technique, 1990-08, Vol.15 (4), p.400-405 |
| issn | 0741-0581 1553-0817 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_79964823 |
| source | MEDLINE; Access via Wiley Online Library |
| subjects | Alloys - analysis Analytical electron microscopy Applied sciences Chemical Precipitation Cross-disciplinary physics: materials science rheology Electron Probe Microanalysis Exact sciences and technology Extraction replica Materials science Metals. Metallurgy Microscopy, Electron Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics Zirconium - analysis Zr alloys |
| title | A replica technique for extracting precipitates from zirconium alloys for transmission electron microscopy analysis |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-23T00%3A32%3A08IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=A%20replica%20technique%20for%20extracting%20precipitates%20from%20zirconium%20alloys%20for%20transmission%20electron%20microscopy%20analysis&rft.jtitle=Journal%20of%20electron%20microscopy%20technique&rft.au=Ng-Yelim,%20J.&rft.date=1990-08&rft.volume=15&rft.issue=4&rft.spage=400&rft.epage=405&rft.pages=400-405&rft.issn=0741-0581&rft.eissn=1553-0817&rft.coden=JEMTEC&rft_id=info:doi/10.1002/jemt.1060150410&rft_dat=%3Cproquest_cross%3E79964823%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=79964823&rft_id=info:pmid/2391566&rfr_iscdi=true |