Identification of Urinary Benzodiazepines and their Metabolites: Comparison of Automated HPLC and GC-MS after Immunoassay Screening of Clinical Specimens

An automated high-performance liquid chromatographic method, benzodiazepines by REMEDi HS, was used to analyze benzodiazepines and their metabolites after β-glucuronidase hydrolysis of 1-mL urine specimens from the following: 924 clinic and hospital patients whose specimens had previously been found...

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Veröffentlicht in:	Journal of analytical toxicology 1996-10, Vol.20 (6), p.416-424
Hauptverfasser:	Valentine, Jimmie L., Middleton, Rosalyn, Sparks, Carolyn
Format:	Artikel
Sprache:	eng
Schlagworte:	1-Propanol - chemistry Acetamides - chemistry Analysis Anti-Anxiety Agents - urine Biological and medical sciences Chloroform - chemistry Chromatography, High Pressure Liquid Clonazepam - urine Flunitrazepam - urine Gas Chromatography-Mass Spectrometry General pharmacology Glucuronidase - chemistry Humans Hydrolysis Inpatients Medical sciences Pharmacology. Drug treatments Reference Standards Trimethylsilyl Compounds - chemistry
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