Extraction of second phases from magnesium and aluminum alloys for analytical electron microscopy

Techniques are described for the extraction onto carbon replicas of precipitates and inclusions from Mg and Al‐based alloys for analytical transmission electron microscopy. EDX analysis of Mn precipitates from a MG‐Mn alloy illustrates the problems that can arise from spurious X‐rays, caused by the...

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Veröffentlicht in:Microscopy research and technique 1994-08, Vol.28 (5), p.422-426
Hauptverfasser: Carpenter, G. J. C., Ng-Yelim, J., Phaneuf, M. W.
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container_title Microscopy research and technique
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creator Carpenter, G. J. C.
Ng-Yelim, J.
Phaneuf, M. W.
description Techniques are described for the extraction onto carbon replicas of precipitates and inclusions from Mg and Al‐based alloys for analytical transmission electron microscopy. EDX analysis of Mn precipitates from a MG‐Mn alloy illustrates the problems that can arise from spurious X‐rays, caused by the use of a 3mm disc specimen. Published 1994 Wiley‐Liss, Inc.
doi_str_mv 10.1002/jemt.1070280508
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source MEDLINE; Wiley Online Library All Journals
subjects Alloys - chemistry
Aluminum - analysis
Aluminum - isolation & purification
Alummum alloys
Applied sciences
Carbon extraction replicas
Convergent beam electron diffraction
Cross-disciplinary physics: materials science
rheology
EDX analysis
Electron Probe Microanalysis
Exact sciences and technology
Magnesium - analysis
Magnesium - isolation & purification
Magnesium alloys
Materials science
Metals. Metallurgy
Microscopy, Electron - methods
Phase diagrams and microstructures developed by solidification and solid-solid phase transformations
Physics
Precipitation
Solid-phase precipitation
Spurious X-rays
Transmission electron microscopy
title Extraction of second phases from magnesium and aluminum alloys for analytical electron microscopy
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