Synthesis and characterization of Bi2S3 nanocrystals in glass matrix
This is the first evidence for the successful growth of Bi2S3 nanocrystals in glass matrix (SiO2-K2O-Na2O-B 2O3-ZnO-TiO2) using the fusion method. Different sizes of nanocrystals in glass matrix were grown by annealing the glass (dispersed with Bi2S3 nucleons) under two different conditions. The gla...
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| Veröffentlicht in: | Materials science & engineering. B, Solid-state materials for advanced technology Solid-state materials for advanced technology, 2010-04, Vol.168 (1-3), p.161-163 |
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| container_title | Materials science & engineering. B, Solid-state materials for advanced technology |
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| creator | Panmand, Rajendra P. Kawade, Ujjwala V. Kulkarni, Milind V. Apte, Sanjay K. Kale, Bharat B. Gosavi, Suresh W. |
| description | This is the first evidence for the successful growth of Bi2S3 nanocrystals in glass matrix (SiO2-K2O-Na2O-B 2O3-ZnO-TiO2) using the fusion method. Different sizes of nanocrystals in glass matrix were grown by annealing the glass (dispersed with Bi2S3 nucleons) under two different conditions. The glass was annealed between 6 and 48h at constant temperature 550A degree C. The glass was also annealed at the temperature between 550 and 600A degree C at constant annealing time 6h. The Bi2S3 nanocomposite obtained was characterized by optical transmission (OT) spectroscopy and transmission electron microscopy (TEM). OT spectroscopy revealed strong red shift in transmission cut off which indicates increase in particle size of nanocrystals under both the conditions. TEM analysis demonstrated the nanocrystal size in the range of 2-5nm. |
| doi_str_mv | 10.1016/j.mseb.2009.12.039 |
| format | Article |
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Different sizes of nanocrystals in glass matrix were grown by annealing the glass (dispersed with Bi2S3 nucleons) under two different conditions. The glass was annealed between 6 and 48h at constant temperature 550A degree C. The glass was also annealed at the temperature between 550 and 600A degree C at constant annealing time 6h. The Bi2S3 nanocomposite obtained was characterized by optical transmission (OT) spectroscopy and transmission electron microscopy (TEM). OT spectroscopy revealed strong red shift in transmission cut off which indicates increase in particle size of nanocrystals under both the conditions. 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TEM analysis demonstrated the nanocrystal size in the range of 2-5nm.</description><subject>Annealing</subject><subject>Doppler effect</subject><subject>Glass</subject><subject>Materials science</subject><subject>Nanocrystals</subject><subject>Nanostructure</subject><subject>Silicon dioxide</subject><subject>Spectroscopy</subject><subject>Transmission electron microscopy</subject><issn>0921-5107</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNotkL1OwzAYRT2ARCm8AJM3poTPP7HxCAUKUiWGwmw5jk1dJU6xXYny9KQq05Wuro6uDkI3BGoCRNxt6yG7tqYAqia0BqbO0AwUJVVDQF6gy5y3AEAopTP0tD7EsnE5ZGxih-3GJGOLS-HXlDBGPHr8GOia4WjiaNMhF9NnHCL-6k3OeDAlhZ8rdO6n2l3_5xx9vjx_LF6r1fvybfGwqiyVqlTcOT8d5ExyT1yrKPO8oyBZC1x1nbP3ovXENAI865QUnbCN5MKDFdYrbtgc3Z64uzR-710uegjZur430Y37rKUACs3EnZb0tLRpzDk5r3cpDCYdNAF9tKS3-mhJHy1pQvVkif0BxJZedw</recordid><startdate>20100415</startdate><enddate>20100415</enddate><creator>Panmand, Rajendra P.</creator><creator>Kawade, Ujjwala V.</creator><creator>Kulkarni, Milind V.</creator><creator>Apte, Sanjay K.</creator><creator>Kale, Bharat B.</creator><creator>Gosavi, Suresh W.</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20100415</creationdate><title>Synthesis and characterization of Bi2S3 nanocrystals in glass matrix</title><author>Panmand, Rajendra P. ; Kawade, Ujjwala V. ; Kulkarni, Milind V. ; Apte, Sanjay K. ; Kale, Bharat B. ; Gosavi, Suresh W.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c279t-4eef0164374f1eb923f4d2073b049ddec86bf1a560f3d976d6c5746f0c6cf94a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Annealing</topic><topic>Doppler effect</topic><topic>Glass</topic><topic>Materials science</topic><topic>Nanocrystals</topic><topic>Nanostructure</topic><topic>Silicon dioxide</topic><topic>Spectroscopy</topic><topic>Transmission electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Panmand, Rajendra P.</creatorcontrib><creatorcontrib>Kawade, Ujjwala V.</creatorcontrib><creatorcontrib>Kulkarni, Milind V.</creatorcontrib><creatorcontrib>Apte, Sanjay K.</creatorcontrib><creatorcontrib>Kale, Bharat B.</creatorcontrib><creatorcontrib>Gosavi, Suresh W.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science & engineering. 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| issn | 0921-5107 |
| language | eng |
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| source | ScienceDirect Journals (5 years ago - present) |
| subjects | Annealing Doppler effect Glass Materials science Nanocrystals Nanostructure Silicon dioxide Spectroscopy Transmission electron microscopy |
| title | Synthesis and characterization of Bi2S3 nanocrystals in glass matrix |
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