Determination of 2-Propanol in Surface Cleaning Solutions Used for Copper Continuous Casting Process by Flow Injection-Spectrophotometric Detection with On-line Column Separation
A flow-injection system has been developed for the determination of 2-propanol in the surface cleaning solutions used in the copper continuous cast rod making system. Adsorption chromatography in nitric acid medium was used for the on-line separation of oily substances in the sample solution. Cerium...
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| Veröffentlicht in: | Analytical Sciences 2003, Vol.19(9), pp.1335-1338 |
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| container_title | Analytical Sciences |
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| creator | HAYASHIBE, Yutaka TOKUDA, Masahiro TAKEYA, Minoru |
| description | A flow-injection system has been developed for the determination of 2-propanol in the surface cleaning solutions used in the copper continuous cast rod making system. Adsorption chromatography in nitric acid medium was used for the on-line separation of oily substances in the sample solution. Cerium(IV) diammonium nitrate was utilized as the chromogenic reagent for the spectrophotometric detection of 2-propanol. The system permits a throughput of one sample per hour for the oily sample, and of 12 samples per hour for the none-oily sample. The reproducibility has been proven to be satisfactory with a relative standard deviation of less than 6.0% (2.2%(V/V) 2-propanol level, n = 23). The detection limit is 0.01%(V/V). |
| doi_str_mv | 10.2116/analsci.19.1335 |
| format | Article |
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Adsorption chromatography in nitric acid medium was used for the on-line separation of oily substances in the sample solution. Cerium(IV) diammonium nitrate was utilized as the chromogenic reagent for the spectrophotometric detection of 2-propanol. The system permits a throughput of one sample per hour for the oily sample, and of 12 samples per hour for the none-oily sample. The reproducibility has been proven to be satisfactory with a relative standard deviation of less than 6.0% (2.2%(V/V) 2-propanol level, n = 23). 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Adsorption chromatography in nitric acid medium was used for the on-line separation of oily substances in the sample solution. Cerium(IV) diammonium nitrate was utilized as the chromogenic reagent for the spectrophotometric detection of 2-propanol. The system permits a throughput of one sample per hour for the oily sample, and of 12 samples per hour for the none-oily sample. The reproducibility has been proven to be satisfactory with a relative standard deviation of less than 6.0% (2.2%(V/V) 2-propanol level, n = 23). The detection limit is 0.01%(V/V).</description><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Chemical industry and chemicals</subject><subject>Chemistry</subject><subject>Exact sciences and technology</subject><subject>Industrial chemicals</subject><subject>Organic industry</subject><subject>Spectrometric and optical methods</subject><issn>0910-6340</issn><issn>1348-2246</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNpdkU9r3DAQxU1pabZpz70VQUlvTjyy_EfHsmnaQCCFbc5mLI-zWmzJlWRCvlY_YeWsSUovGsH85r0ZXpJ8hOycA5QXaHDwSp-DPIc8L14lG8hFnXIuytfJJpOQpWUuspPknfeHLANec_42OQFRQBm7m-TPJQVyozYYtDXM9oynP52d0NiBacN2s-tREdsOhEabe7azw7ygnt156lhvHdvaaaKlmKDNbGfPtujDAkclRd6z9pFdDfaBXZsDqWU63U3xE332NtiRgtOKLZs8NdmDDnt2a9JBm-gcDce4CE3onpZ8n7zp49X0Ya2nyd3Vt1_bH-nN7ffr7debVImqDmldZ22NvJOlRAmlgKICLosqB8qo6ATvSCK0vMWy6jpsey6ga5FXPOclEOWnyZej7uTs75l8aEbtFQ0DGopHNlUULLIaIvj5P_BgZ7ck04AQdSHKMl-oiyOlnPXeUd9MTo_oHhvImiXMZg2zAdksYcaJT6vu3I7UvfBrehE4WwH0CofeoVHav3AFVFKKRejyyB18wHt6BtAFrQb611iuT_R_bqs9uoZM_hc0usTj</recordid><startdate>20030901</startdate><enddate>20030901</enddate><creator>HAYASHIBE, Yutaka</creator><creator>TOKUDA, Masahiro</creator><creator>TAKEYA, Minoru</creator><general>The Japan Society for Analytical Chemistry</general><general>Japan Society for Analytical Chemistry</general><general>Japan Science and Technology Agency</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SE</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>H8G</scope><scope>JG9</scope><scope>L7M</scope><scope>P64</scope><scope>7X8</scope></search><sort><creationdate>20030901</creationdate><title>Determination of 2-Propanol in Surface Cleaning Solutions Used for Copper Continuous Casting Process by Flow Injection-Spectrophotometric Detection with On-line Column Separation</title><author>HAYASHIBE, Yutaka ; TOKUDA, Masahiro ; TAKEYA, Minoru</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c478t-880b8a2d969a91641571295731e0e5d42de9a1b2ba67ddabf241dba2723261ee3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Chemical industry and chemicals</topic><topic>Chemistry</topic><topic>Exact sciences and technology</topic><topic>Industrial chemicals</topic><topic>Organic industry</topic><topic>Spectrometric and optical methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>HAYASHIBE, Yutaka</creatorcontrib><creatorcontrib>TOKUDA, Masahiro</creatorcontrib><creatorcontrib>TAKEYA, Minoru</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Biotechnology Research Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Analytical Sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>HAYASHIBE, Yutaka</au><au>TOKUDA, Masahiro</au><au>TAKEYA, Minoru</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of 2-Propanol in Surface Cleaning Solutions Used for Copper Continuous Casting Process by Flow Injection-Spectrophotometric Detection with On-line Column Separation</atitle><jtitle>Analytical Sciences</jtitle><addtitle>Anal Sci</addtitle><date>2003-09-01</date><risdate>2003</risdate><volume>19</volume><issue>9</issue><spage>1335</spage><epage>1338</epage><pages>1335-1338</pages><issn>0910-6340</issn><eissn>1348-2246</eissn><coden>ANSCEN</coden><abstract>A flow-injection system has been developed for the determination of 2-propanol in the surface cleaning solutions used in the copper continuous cast rod making system. 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| language | eng |
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| source | J-STAGE Free; SpringerNature Journals; Freely Accessible Japanese Titles; EZB-FREE-00999 freely available EZB journals; Free Full-Text Journals in Chemistry |
| subjects | Analytical chemistry Applied sciences Chemical industry and chemicals Chemistry Exact sciences and technology Industrial chemicals Organic industry Spectrometric and optical methods |
| title | Determination of 2-Propanol in Surface Cleaning Solutions Used for Copper Continuous Casting Process by Flow Injection-Spectrophotometric Detection with On-line Column Separation |
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