Scanning transmission electron microscopy using selective high-order laue zones: three-dimensional atomic ordering in sodium cobaltate

Scanning transmission electron microscopy using selective high-order laue zones: three-dimensional atomic ordering in sodium cobaltate

A new scanning transmission electron microscopy (STEM) imaging technique using high-order Laue zones (named HOLZ-STEM), a diffraction contrast which has been strenuously avoided or minimized in traditional STEM imaging, can be used to obtain the additional 1D periodic information along the electron...

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Veröffentlicht in:Physical review letters 2010-09, Vol.105 (12), p.125502-125502, Article 125502
Hauptverfasser: Huang, F-T, Gloter, A, Chu, M-W, Chou, F C, Shu, G J, Liu, L-K, Chen, C H, Colliex, C
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container_end_page 125502
container_issue 12
container_start_page 125502
container_title Physical review letters
container_volume 105
creator Huang, F-T
Gloter, A
Chu, M-W
Chou, F C
Shu, G J
Liu, L-K
Chen, C H
Colliex, C
description A new scanning transmission electron microscopy (STEM) imaging technique using high-order Laue zones (named HOLZ-STEM), a diffraction contrast which has been strenuously avoided or minimized in traditional STEM imaging, can be used to obtain the additional 1D periodic information along the electron propagation axis without sacrificing atomic resolution in the lateral (2D) dimension. HOLZ-STEM has been demonstrated to resolve the 3D long-range Na ordering of Na0.71CoO2. Direct evidence of spiral-like Na-trimer chains twisting along the c axis is unambiguously established in real space.
doi_str_mv 10.1103/PhysRevLett.105.125502
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title Scanning transmission electron microscopy using selective high-order laue zones: three-dimensional atomic ordering in sodium cobaltate
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