X-ray diffraction and scanning electron microscopy of galvannealed coatings on steel
The formation of Fe-Zn intermetallic compounds, as relevant in the commercial product galvannealed steel sheet, was investigated by scanning electron microscopy and different methods of X-ray diffraction. A scanning electron microscope with high resolution was applied to investigate the layers of th...
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| Veröffentlicht in: | Analytical & bioanalytical chemistry (Print) 2009-04, Vol.393 (8), p.1863-1870 |
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| container_title | Analytical & bioanalytical chemistry (Print) |
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| creator | Schmid, P Uran, K Macherey, F Ebert, M Ullrich, H.-J Sommer, D Friedel, F |
| description | The formation of Fe-Zn intermetallic compounds, as relevant in the commercial product galvannealed steel sheet, was investigated by scanning electron microscopy and different methods of X-ray diffraction. A scanning electron microscope with high resolution was applied to investigate the layers of the galvannealed coating and its topography. Grazing incidence X-ray diffraction (GID) was preferred over conventional Bragg-Brentano geometry for analysing thin crystalline layers because of its lower incidence angle α and its lower depth of information. Furthermore, in situ experiments at an environmental scanning electron microscope (ESEM) with an internal heating plate and at an X-ray diffractometer equipped with a high-temperature chamber were carried out. Thus, it was possible to investigate the phase evolution during heat treatment by X-ray diffraction and to display the growth of the ζ crystals in the ESEM. |
| doi_str_mv | 10.1007/s00216-008-2581-z |
| format | Article |
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A scanning electron microscope with high resolution was applied to investigate the layers of the galvannealed coating and its topography. Grazing incidence X-ray diffraction (GID) was preferred over conventional Bragg-Brentano geometry for analysing thin crystalline layers because of its lower incidence angle α and its lower depth of information. Furthermore, in situ experiments at an environmental scanning electron microscope (ESEM) with an internal heating plate and at an X-ray diffractometer equipped with a high-temperature chamber were carried out. 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A scanning electron microscope with high resolution was applied to investigate the layers of the galvannealed coating and its topography. Grazing incidence X-ray diffraction (GID) was preferred over conventional Bragg-Brentano geometry for analysing thin crystalline layers because of its lower incidence angle α and its lower depth of information. Furthermore, in situ experiments at an environmental scanning electron microscope (ESEM) with an internal heating plate and at an X-ray diffractometer equipped with a high-temperature chamber were carried out. 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| subjects | Analytical Chemistry Annealing Applied sciences Biochemistry Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Coatings Diffraction Environmental scanning electron microscopy Exact sciences and technology Fe-Zn phase formation Food Science Global environmental pollution Grazing incidence X-ray diffraction Heat treatment High-temperature in situ observation Laboratory Medicine Monitoring/Environmental Analysis Original Paper Pollution Scanning electron microscopy Sheet metal Steels X-ray diffraction X-rays |
| title | X-ray diffraction and scanning electron microscopy of galvannealed coatings on steel |
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