Mechanical alloying of biocompatible Co–28Cr–6Mo alloy
We report on an alternative route for the synthesis of crystalline Co–28Cr–6Mo alloy, which could be used for surgical implants. Co, Cr and Mo elemental powders, mixed in an adequate weight relation according to ISO Standard 58342-4 (ISO, 1996), were used for the mechanical alloying (MA) of nano-str...
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| Veröffentlicht in: | Journal of materials science. Materials in medicine 2010-07, Vol.21 (7), p.2021-2026 |
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| creator | Sánchez-De Jesús, F. Bolarín-Miró, A. M. Torres-Villaseñor, G. Cortés-Escobedo, C. A. Betancourt-Cantera, J. A. |
| description | We report on an alternative route for the synthesis of crystalline Co–28Cr–6Mo alloy, which could be used for surgical implants. Co, Cr and Mo elemental powders, mixed in an adequate weight relation according to ISO Standard 58342-4 (ISO, 1996), were used for the mechanical alloying (MA) of nano-structured Co-alloy. The process was carried out at room temperature in a shaker mixer mill using hardened steel balls and vials as milling media, with a 1:8 ball:powder weight ratio. Crystalline structure characterization of milled powders was carried out by X-ray diffraction in order to analyze the phase transformations as a function of milling time. The aim of this work was to evaluate the alloying mechanism involved in the mechanical alloying of Co–28Cr–6Mo alloy. The evolution of the phase transformations with milling time is reported for each mixture. Results showed that the resultant alloy is a Co-alpha solid solution, successfully obtained by mechanical alloying after a total of 10 h of milling time: first Cr and Mo are mechanically prealloyed for 7 h, and then Co is mixed in for 3 h. In addition, different methods of premixing were studied. The particle size of the powders is reduced with increasing milling time, reaching about 5 μm at 10 h; a longer time promotes the formation of aggregates. The morphology and crystal structure of milled powders as a function of milling time were analyzed by scanning electron microscopy and XR diffraction. |
| doi_str_mv | 10.1007/s10856-010-4066-9 |
| format | Article |
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M. ; Torres-Villaseñor, G. ; Cortés-Escobedo, C. A. ; Betancourt-Cantera, J. A.</creator><creatorcontrib>Sánchez-De Jesús, F. ; Bolarín-Miró, A. M. ; Torres-Villaseñor, G. ; Cortés-Escobedo, C. A. ; Betancourt-Cantera, J. A.</creatorcontrib><description>We report on an alternative route for the synthesis of crystalline Co–28Cr–6Mo alloy, which could be used for surgical implants. Co, Cr and Mo elemental powders, mixed in an adequate weight relation according to ISO Standard 58342-4 (ISO, 1996), were used for the mechanical alloying (MA) of nano-structured Co-alloy. The process was carried out at room temperature in a shaker mixer mill using hardened steel balls and vials as milling media, with a 1:8 ball:powder weight ratio. Crystalline structure characterization of milled powders was carried out by X-ray diffraction in order to analyze the phase transformations as a function of milling time. The aim of this work was to evaluate the alloying mechanism involved in the mechanical alloying of Co–28Cr–6Mo alloy. The evolution of the phase transformations with milling time is reported for each mixture. Results showed that the resultant alloy is a Co-alpha solid solution, successfully obtained by mechanical alloying after a total of 10 h of milling time: first Cr and Mo are mechanically prealloyed for 7 h, and then Co is mixed in for 3 h. In addition, different methods of premixing were studied. The particle size of the powders is reduced with increasing milling time, reaching about 5 μm at 10 h; a longer time promotes the formation of aggregates. The morphology and crystal structure of milled powders as a function of milling time were analyzed by scanning electron microscopy and XR diffraction.</description><identifier>ISSN: 0957-4530</identifier><identifier>EISSN: 1573-4838</identifier><identifier>DOI: 10.1007/s10856-010-4066-9</identifier><identifier>PMID: 20364362</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Alloys ; Applied sciences ; Biological and medical sciences ; Biomaterials ; Biomedical Engineering and Bioengineering ; Biomedical materials ; Ceramics ; Chemistry and Materials Science ; Chromium Alloys - chemical synthesis ; Chromium Alloys - chemistry ; Composites ; Crystallography ; Dental research ; Exact sciences and technology ; Glass ; Materials Science ; Medical sciences ; Metals. Metallurgy ; Microscopy, Electron, Scanning ; Molybdenum - chemistry ; Natural Materials ; Particle Size ; Polymer Sciences ; Powders ; Regenerative Medicine/Tissue Engineering ; Surfaces and Interfaces ; Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases ; Technology. Biomaterials. Equipments ; Thin Films ; Transplants & implants ; X-Ray Diffraction</subject><ispartof>Journal of materials science. 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M.</creatorcontrib><creatorcontrib>Torres-Villaseñor, G.</creatorcontrib><creatorcontrib>Cortés-Escobedo, C. A.</creatorcontrib><creatorcontrib>Betancourt-Cantera, J. A.</creatorcontrib><title>Mechanical alloying of biocompatible Co–28Cr–6Mo alloy</title><title>Journal of materials science. Materials in medicine</title><addtitle>J Mater Sci: Mater Med</addtitle><addtitle>J Mater Sci Mater Med</addtitle><description>We report on an alternative route for the synthesis of crystalline Co–28Cr–6Mo alloy, which could be used for surgical implants. Co, Cr and Mo elemental powders, mixed in an adequate weight relation according to ISO Standard 58342-4 (ISO, 1996), were used for the mechanical alloying (MA) of nano-structured Co-alloy. The process was carried out at room temperature in a shaker mixer mill using hardened steel balls and vials as milling media, with a 1:8 ball:powder weight ratio. Crystalline structure characterization of milled powders was carried out by X-ray diffraction in order to analyze the phase transformations as a function of milling time. The aim of this work was to evaluate the alloying mechanism involved in the mechanical alloying of Co–28Cr–6Mo alloy. The evolution of the phase transformations with milling time is reported for each mixture. Results showed that the resultant alloy is a Co-alpha solid solution, successfully obtained by mechanical alloying after a total of 10 h of milling time: first Cr and Mo are mechanically prealloyed for 7 h, and then Co is mixed in for 3 h. In addition, different methods of premixing were studied. The particle size of the powders is reduced with increasing milling time, reaching about 5 μm at 10 h; a longer time promotes the formation of aggregates. The morphology and crystal structure of milled powders as a function of milling time were analyzed by scanning electron microscopy and XR diffraction.</description><subject>Alloys</subject><subject>Applied sciences</subject><subject>Biological and medical sciences</subject><subject>Biomaterials</subject><subject>Biomedical Engineering and Bioengineering</subject><subject>Biomedical materials</subject><subject>Ceramics</subject><subject>Chemistry and Materials Science</subject><subject>Chromium Alloys - chemical synthesis</subject><subject>Chromium Alloys - chemistry</subject><subject>Composites</subject><subject>Crystallography</subject><subject>Dental research</subject><subject>Exact sciences and technology</subject><subject>Glass</subject><subject>Materials Science</subject><subject>Medical sciences</subject><subject>Metals. Metallurgy</subject><subject>Microscopy, Electron, Scanning</subject><subject>Molybdenum - chemistry</subject><subject>Natural Materials</subject><subject>Particle Size</subject><subject>Polymer Sciences</subject><subject>Powders</subject><subject>Regenerative Medicine/Tissue Engineering</subject><subject>Surfaces and Interfaces</subject><subject>Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases</subject><subject>Technology. Biomaterials. 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Metallurgy</topic><topic>Microscopy, Electron, Scanning</topic><topic>Molybdenum - chemistry</topic><topic>Natural Materials</topic><topic>Particle Size</topic><topic>Polymer Sciences</topic><topic>Powders</topic><topic>Regenerative Medicine/Tissue Engineering</topic><topic>Surfaces and Interfaces</topic><topic>Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases</topic><topic>Technology. Biomaterials. Equipments</topic><topic>Thin Films</topic><topic>Transplants & implants</topic><topic>X-Ray Diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sánchez-De Jesús, F.</creatorcontrib><creatorcontrib>Bolarín-Miró, A. M.</creatorcontrib><creatorcontrib>Torres-Villaseñor, G.</creatorcontrib><creatorcontrib>Cortés-Escobedo, C. A.</creatorcontrib><creatorcontrib>Betancourt-Cantera, J. 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Materials in medicine</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sánchez-De Jesús, F.</au><au>Bolarín-Miró, A. M.</au><au>Torres-Villaseñor, G.</au><au>Cortés-Escobedo, C. A.</au><au>Betancourt-Cantera, J. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Mechanical alloying of biocompatible Co–28Cr–6Mo alloy</atitle><jtitle>Journal of materials science. Materials in medicine</jtitle><stitle>J Mater Sci: Mater Med</stitle><addtitle>J Mater Sci Mater Med</addtitle><date>2010-07-01</date><risdate>2010</risdate><volume>21</volume><issue>7</issue><spage>2021</spage><epage>2026</epage><pages>2021-2026</pages><issn>0957-4530</issn><eissn>1573-4838</eissn><abstract>We report on an alternative route for the synthesis of crystalline Co–28Cr–6Mo alloy, which could be used for surgical implants. Co, Cr and Mo elemental powders, mixed in an adequate weight relation according to ISO Standard 58342-4 (ISO, 1996), were used for the mechanical alloying (MA) of nano-structured Co-alloy. The process was carried out at room temperature in a shaker mixer mill using hardened steel balls and vials as milling media, with a 1:8 ball:powder weight ratio. Crystalline structure characterization of milled powders was carried out by X-ray diffraction in order to analyze the phase transformations as a function of milling time. The aim of this work was to evaluate the alloying mechanism involved in the mechanical alloying of Co–28Cr–6Mo alloy. The evolution of the phase transformations with milling time is reported for each mixture. Results showed that the resultant alloy is a Co-alpha solid solution, successfully obtained by mechanical alloying after a total of 10 h of milling time: first Cr and Mo are mechanically prealloyed for 7 h, and then Co is mixed in for 3 h. In addition, different methods of premixing were studied. The particle size of the powders is reduced with increasing milling time, reaching about 5 μm at 10 h; a longer time promotes the formation of aggregates. The morphology and crystal structure of milled powders as a function of milling time were analyzed by scanning electron microscopy and XR diffraction.</abstract><cop>Boston</cop><pub>Springer US</pub><pmid>20364362</pmid><doi>10.1007/s10856-010-4066-9</doi><tpages>6</tpages></addata></record> |
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| subjects | Alloys Applied sciences Biological and medical sciences Biomaterials Biomedical Engineering and Bioengineering Biomedical materials Ceramics Chemistry and Materials Science Chromium Alloys - chemical synthesis Chromium Alloys - chemistry Composites Crystallography Dental research Exact sciences and technology Glass Materials Science Medical sciences Metals. Metallurgy Microscopy, Electron, Scanning Molybdenum - chemistry Natural Materials Particle Size Polymer Sciences Powders Regenerative Medicine/Tissue Engineering Surfaces and Interfaces Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases Technology. Biomaterials. Equipments Thin Films Transplants & implants X-Ray Diffraction |
| title | Mechanical alloying of biocompatible Co–28Cr–6Mo alloy |
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