Rapid separation and characterization of active flavonolignans of Silybum marianum by ultra-performance liquid chromatography coupled with electrospray tandem mass spectrometry

Ultra-performance liquid chromatography (UPLC) interfaced with the electrospray ionization (ESI) tandem mass spectrometer (MS n ) was developed for the simultaneous determination of silychristins A ( 1) and B ( 2), silydianin ( 3), silybins A ( 4) and B ( 5), and isosilybins A ( 6) and B ( 7), major...

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Veröffentlicht in:	Journal of pharmaceutical and biomedical analysis 2010-12, Vol.53 (4), p.1053-1057
Hauptverfasser:	Wang, Kuiwu, Zhang, Hong, Shen, Lianqing, Du, Qizhen, Li, Jianrong
Format:	Artikel
Sprache:	eng
Schlagworte:	Analysis Analytical, structural and metabolic biochemistry Biological and medical sciences Chromatography, Liquid - methods ESI-MS n Flavonolignan Flavonolignans - analysis Fundamental and applied biological sciences. Psychology General pharmacology Medical sciences Pharmacology. Drug treatments Silybum marianum (L.) Gaertn Silybum marianum - chemistry Silymarin Silymarin - analysis Spectrometry, Mass, Electrospray Ionization - methods UPLC separation
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