Proton induced x-ray emission analysis of Pima Indian autopsy tissues
Proton particle-induced X-ray emission (PIXE) analysis has been used to determine the concentrations of K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Se, Br, Rb, Sr, Cd, Cs, and Pb in liver, spleen, aorta, kidney medulla, kidney cortex, abdominal fat, pancreas, and hair taken at autopsy from Southwest Indians,...
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| Veröffentlicht in: | Anal. Chem.; (United States) 1979-07, Vol.51 (8), p.1187-1194 |
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| creator | Mangelson, N. F Hill, M. W Nielson, K. K Eatough, D. J Christensen, J. J Izatt, R. M Richards, D. O |
| description | Proton particle-induced X-ray emission (PIXE) analysis has been used to determine the concentrations of K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Se, Br, Rb, Sr, Cd, Cs, and Pb in liver, spleen, aorta, kidney medulla, kidney cortex, abdominal fat, pancreas, and hair taken at autopsy from Southwest Indians, primarily of the Pima tribe. Samples were prepared by a low-temperature ashing procedure which is compared to other preparation methods. Data were analyzed by a computer program, ANALEX. The accuracy is tested with NBS standard reference materials and with flame atomic absorption spectrophotometric results. The precision allowed observation of element concentration differences between replicate, half-gram samples of the same tissue. The differences appeared to arise from tissue inhomogeneities. 5 figures, 4 tables. |
| doi_str_mv | 10.1021/ac50044a021 |
| format | Article |
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F ; Hill, M. W ; Nielson, K. K ; Eatough, D. J ; Christensen, J. J ; Izatt, R. M ; Richards, D. O</creator><creatorcontrib>Mangelson, N. F ; Hill, M. W ; Nielson, K. K ; Eatough, D. J ; Christensen, J. J ; Izatt, R. M ; Richards, D. O ; Brigham Young Univ., Provo, UT</creatorcontrib><description>Proton particle-induced X-ray emission (PIXE) analysis has been used to determine the concentrations of K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Se, Br, Rb, Sr, Cd, Cs, and Pb in liver, spleen, aorta, kidney medulla, kidney cortex, abdominal fat, pancreas, and hair taken at autopsy from Southwest Indians, primarily of the Pima tribe. Samples were prepared by a low-temperature ashing procedure which is compared to other preparation methods. Data were analyzed by a computer program, ANALEX. The accuracy is tested with NBS standard reference materials and with flame atomic absorption spectrophotometric results. The precision allowed observation of element concentration differences between replicate, half-gram samples of the same tissue. The differences appeared to arise from tissue inhomogeneities. 5 figures, 4 tables.</description><identifier>ISSN: 0003-2700</identifier><identifier>EISSN: 1520-6882</identifier><identifier>DOI: 10.1021/ac50044a021</identifier><identifier>PMID: 484856</identifier><language>eng</language><publisher>United States: American Chemical Society</publisher><subject>400104 - Spectral Procedures- (-1987) ; ABSORPTION SPECTROSCOPY ; ALKALI METALS ; ALKALINE EARTH METALS ; AORTA ; ARTERIES ; AUTOPSY ; Autopsy - methods ; BARYONS ; BLOOD VESSELS ; BODY ; BROMINE ; CADMIUM ; CALCIUM ; CARDIOVASCULAR SYSTEM ; CESIUM ; CHEMICAL ANALYSIS ; COBALT ; COPPER ; DIAGNOSTIC TECHNIQUES ; DIGESTIVE SYSTEM ; DRY ASHING ; Electron Probe Microanalysis ; ELEMENTARY PARTICLES ; ELEMENTS ; ENDOCRINE GLANDS ; FERMIONS ; GLANDS ; HADRONS ; HAIR ; HALOGENS ; Humans ; Indians, North American ; INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ; IRON ; KIDNEYS ; LEAD ; LIVER ; MANGANESE ; METALS ; NICKEL ; NONDESTRUCTIVE ANALYSIS ; NONMETALS ; NUCLEONS ; ORGANS ; PANCREAS ; POTASSIUM ; PROTONS ; QUALITATIVE CHEMICAL ANALYSIS ; RUBIDIUM ; SELENIUM ; SEMIMETALS ; SKIN ; SPECTROSCOPY ; SPLEEN ; STRONTIUM ; TISSUES ; TITANIUM ; Trace Elements - analysis ; TRANSITION ELEMENTS ; X-RAY EMISSION ANALYSIS ; ZINC</subject><ispartof>Anal. 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F</creatorcontrib><creatorcontrib>Hill, M. W</creatorcontrib><creatorcontrib>Nielson, K. K</creatorcontrib><creatorcontrib>Eatough, D. J</creatorcontrib><creatorcontrib>Christensen, J. J</creatorcontrib><creatorcontrib>Izatt, R. M</creatorcontrib><creatorcontrib>Richards, D. O</creatorcontrib><creatorcontrib>Brigham Young Univ., Provo, UT</creatorcontrib><title>Proton induced x-ray emission analysis of Pima Indian autopsy tissues</title><title>Anal. Chem.; (United States)</title><addtitle>Anal. Chem</addtitle><description>Proton particle-induced X-ray emission (PIXE) analysis has been used to determine the concentrations of K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Se, Br, Rb, Sr, Cd, Cs, and Pb in liver, spleen, aorta, kidney medulla, kidney cortex, abdominal fat, pancreas, and hair taken at autopsy from Southwest Indians, primarily of the Pima tribe. Samples were prepared by a low-temperature ashing procedure which is compared to other preparation methods. Data were analyzed by a computer program, ANALEX. The accuracy is tested with NBS standard reference materials and with flame atomic absorption spectrophotometric results. The precision allowed observation of element concentration differences between replicate, half-gram samples of the same tissue. The differences appeared to arise from tissue inhomogeneities. 5 figures, 4 tables.</description><subject>400104 - Spectral Procedures- (-1987)</subject><subject>ABSORPTION SPECTROSCOPY</subject><subject>ALKALI METALS</subject><subject>ALKALINE EARTH METALS</subject><subject>AORTA</subject><subject>ARTERIES</subject><subject>AUTOPSY</subject><subject>Autopsy - methods</subject><subject>BARYONS</subject><subject>BLOOD VESSELS</subject><subject>BODY</subject><subject>BROMINE</subject><subject>CADMIUM</subject><subject>CALCIUM</subject><subject>CARDIOVASCULAR SYSTEM</subject><subject>CESIUM</subject><subject>CHEMICAL ANALYSIS</subject><subject>COBALT</subject><subject>COPPER</subject><subject>DIAGNOSTIC TECHNIQUES</subject><subject>DIGESTIVE SYSTEM</subject><subject>DRY ASHING</subject><subject>Electron Probe Microanalysis</subject><subject>ELEMENTARY PARTICLES</subject><subject>ELEMENTS</subject><subject>ENDOCRINE GLANDS</subject><subject>FERMIONS</subject><subject>GLANDS</subject><subject>HADRONS</subject><subject>HAIR</subject><subject>HALOGENS</subject><subject>Humans</subject><subject>Indians, North American</subject><subject>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</subject><subject>IRON</subject><subject>KIDNEYS</subject><subject>LEAD</subject><subject>LIVER</subject><subject>MANGANESE</subject><subject>METALS</subject><subject>NICKEL</subject><subject>NONDESTRUCTIVE ANALYSIS</subject><subject>NONMETALS</subject><subject>NUCLEONS</subject><subject>ORGANS</subject><subject>PANCREAS</subject><subject>POTASSIUM</subject><subject>PROTONS</subject><subject>QUALITATIVE CHEMICAL ANALYSIS</subject><subject>RUBIDIUM</subject><subject>SELENIUM</subject><subject>SEMIMETALS</subject><subject>SKIN</subject><subject>SPECTROSCOPY</subject><subject>SPLEEN</subject><subject>STRONTIUM</subject><subject>TISSUES</subject><subject>TITANIUM</subject><subject>Trace Elements - analysis</subject><subject>TRANSITION ELEMENTS</subject><subject>X-RAY EMISSION ANALYSIS</subject><subject>ZINC</subject><issn>0003-2700</issn><issn>1520-6882</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1979</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNptkMtP3DAQxq2qQJfHiWsPEQd6QAE_Esc5Ih4tD4mVoELqxXJsR5juxovHkdj_vlMFIQ6cZjTfTzPzfYTsM3rMKGcnxtaUVpXB_guZsZrTUirFv5IZpVSUvKH0G9kGeKaUMcrkFtmsVKVqOSMX8xRzHIowuNF6V7yWyawLvwwAAcdmMIs1BChiX8zD0hRXgwsG52OOK1gXGbnRwy7Z6M0C_N5b3SG_Ly8ezn6Vt3c_r85Ob0sjFM2lrU3rZCVV1XVWcSd43bKqc70XvfBO8RpNCNkr2zLHVWM7LLI3okfeGSd2yMG0N0IOGmzI3j7ZOAzeZi05b1TLEDqcoFWKL_hc1ujG-sXCDD6OoJtKtgzzQfBoAm2KAMn3epXQY1prRvX_YPWHYJH-_rZ27JbevbNTkiiXkxwg-9d31aS_WjaiqfXD_F7_OX-8ZpeP1_oG-R8Tbyzo5zgmTBo-PfwP5i2OsA</recordid><startdate>197907</startdate><enddate>197907</enddate><creator>Mangelson, N. F</creator><creator>Hill, M. W</creator><creator>Nielson, K. K</creator><creator>Eatough, D. J</creator><creator>Christensen, J. J</creator><creator>Izatt, R. M</creator><creator>Richards, D. O</creator><general>American Chemical Society</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>OTOTI</scope></search><sort><creationdate>197907</creationdate><title>Proton induced x-ray emission analysis of Pima Indian autopsy tissues</title><author>Mangelson, N. F ; Hill, M. W ; Nielson, K. K ; Eatough, D. J ; Christensen, J. J ; Izatt, R. M ; Richards, D. O</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a380t-c5a9d64684bbc82d325914bdfe3f3ed82544a36f8c91d287cb1d26fa3fbbcdad3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1979</creationdate><topic>400104 - Spectral Procedures- (-1987)</topic><topic>ABSORPTION SPECTROSCOPY</topic><topic>ALKALI METALS</topic><topic>ALKALINE EARTH METALS</topic><topic>AORTA</topic><topic>ARTERIES</topic><topic>AUTOPSY</topic><topic>Autopsy - methods</topic><topic>BARYONS</topic><topic>BLOOD VESSELS</topic><topic>BODY</topic><topic>BROMINE</topic><topic>CADMIUM</topic><topic>CALCIUM</topic><topic>CARDIOVASCULAR SYSTEM</topic><topic>CESIUM</topic><topic>CHEMICAL ANALYSIS</topic><topic>COBALT</topic><topic>COPPER</topic><topic>DIAGNOSTIC TECHNIQUES</topic><topic>DIGESTIVE SYSTEM</topic><topic>DRY ASHING</topic><topic>Electron Probe Microanalysis</topic><topic>ELEMENTARY PARTICLES</topic><topic>ELEMENTS</topic><topic>ENDOCRINE GLANDS</topic><topic>FERMIONS</topic><topic>GLANDS</topic><topic>HADRONS</topic><topic>HAIR</topic><topic>HALOGENS</topic><topic>Humans</topic><topic>Indians, North American</topic><topic>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</topic><topic>IRON</topic><topic>KIDNEYS</topic><topic>LEAD</topic><topic>LIVER</topic><topic>MANGANESE</topic><topic>METALS</topic><topic>NICKEL</topic><topic>NONDESTRUCTIVE ANALYSIS</topic><topic>NONMETALS</topic><topic>NUCLEONS</topic><topic>ORGANS</topic><topic>PANCREAS</topic><topic>POTASSIUM</topic><topic>PROTONS</topic><topic>QUALITATIVE CHEMICAL ANALYSIS</topic><topic>RUBIDIUM</topic><topic>SELENIUM</topic><topic>SEMIMETALS</topic><topic>SKIN</topic><topic>SPECTROSCOPY</topic><topic>SPLEEN</topic><topic>STRONTIUM</topic><topic>TISSUES</topic><topic>TITANIUM</topic><topic>Trace Elements - analysis</topic><topic>TRANSITION ELEMENTS</topic><topic>X-RAY EMISSION ANALYSIS</topic><topic>ZINC</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mangelson, N. F</creatorcontrib><creatorcontrib>Hill, M. W</creatorcontrib><creatorcontrib>Nielson, K. K</creatorcontrib><creatorcontrib>Eatough, D. J</creatorcontrib><creatorcontrib>Christensen, J. J</creatorcontrib><creatorcontrib>Izatt, R. M</creatorcontrib><creatorcontrib>Richards, D. O</creatorcontrib><creatorcontrib>Brigham Young Univ., Provo, UT</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>OSTI.GOV</collection><jtitle>Anal. Chem.; (United States)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mangelson, N. F</au><au>Hill, M. W</au><au>Nielson, K. K</au><au>Eatough, D. J</au><au>Christensen, J. J</au><au>Izatt, R. M</au><au>Richards, D. O</au><aucorp>Brigham Young Univ., Provo, UT</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Proton induced x-ray emission analysis of Pima Indian autopsy tissues</atitle><jtitle>Anal. Chem.; (United States)</jtitle><addtitle>Anal. Chem</addtitle><date>1979-07</date><risdate>1979</risdate><volume>51</volume><issue>8</issue><spage>1187</spage><epage>1194</epage><pages>1187-1194</pages><issn>0003-2700</issn><eissn>1520-6882</eissn><abstract>Proton particle-induced X-ray emission (PIXE) analysis has been used to determine the concentrations of K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Se, Br, Rb, Sr, Cd, Cs, and Pb in liver, spleen, aorta, kidney medulla, kidney cortex, abdominal fat, pancreas, and hair taken at autopsy from Southwest Indians, primarily of the Pima tribe. Samples were prepared by a low-temperature ashing procedure which is compared to other preparation methods. Data were analyzed by a computer program, ANALEX. The accuracy is tested with NBS standard reference materials and with flame atomic absorption spectrophotometric results. The precision allowed observation of element concentration differences between replicate, half-gram samples of the same tissue. The differences appeared to arise from tissue inhomogeneities. 5 figures, 4 tables.</abstract><cop>United States</cop><pub>American Chemical Society</pub><pmid>484856</pmid><doi>10.1021/ac50044a021</doi><tpages>8</tpages></addata></record> |
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| ispartof | Anal. Chem.; (United States), 1979-07, Vol.51 (8), p.1187-1194 |
| issn | 0003-2700 1520-6882 |
| language | eng |
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| source | ACS Publications; MEDLINE |
| subjects | 400104 - Spectral Procedures- (-1987) ABSORPTION SPECTROSCOPY ALKALI METALS ALKALINE EARTH METALS AORTA ARTERIES AUTOPSY Autopsy - methods BARYONS BLOOD VESSELS BODY BROMINE CADMIUM CALCIUM CARDIOVASCULAR SYSTEM CESIUM CHEMICAL ANALYSIS COBALT COPPER DIAGNOSTIC TECHNIQUES DIGESTIVE SYSTEM DRY ASHING Electron Probe Microanalysis ELEMENTARY PARTICLES ELEMENTS ENDOCRINE GLANDS FERMIONS GLANDS HADRONS HAIR HALOGENS Humans Indians, North American INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY IRON KIDNEYS LEAD LIVER MANGANESE METALS NICKEL NONDESTRUCTIVE ANALYSIS NONMETALS NUCLEONS ORGANS PANCREAS POTASSIUM PROTONS QUALITATIVE CHEMICAL ANALYSIS RUBIDIUM SELENIUM SEMIMETALS SKIN SPECTROSCOPY SPLEEN STRONTIUM TISSUES TITANIUM Trace Elements - analysis TRANSITION ELEMENTS X-RAY EMISSION ANALYSIS ZINC |
| title | Proton induced x-ray emission analysis of Pima Indian autopsy tissues |
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