The use of inductively coupled plasma mass spectrometry (ICP-MS) for the determination of toxic and essential elements in different types of food samples
This paper describes a simple method for the determination of sixteen elements in food samples by using inductively coupled plasma spectrometry (ICP-MS). Prior to analysis, 100–250 mg of powdered food samples were accurately weighed into a Teflon digestion vessel. Then, 4 ml of 20% v/v concentrated...
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| Veröffentlicht in: | Food chemistry 2009-02, Vol.112 (3), p.727-732 |
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| container_title | Food chemistry |
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| creator | Nardi, Elene P. Evangelista, Fábio S. Tormen, Luciano Saint´Pierre, Tatiana D. Curtius, Adilson J. Souza, Samuel S. de Barbosa, Fernando |
| description | This paper describes a simple method for the determination of sixteen elements in food samples by using inductively coupled plasma spectrometry (ICP-MS). Prior to analysis, 100–250
mg of powdered food samples were accurately weighed into a Teflon digestion vessel. Then, 4
ml of 20% v/v concentrated nitric acid and 2
ml of hydrogen peroxide were added. Decomposition of samples was carried out in a microwave digestion system. In order to verify the accuracy and precision of the proposed method, five Standard Reference Materials from the National Institute of Standards and Technology (NIST) (Whole Egg Powder RM 8415, Rice Flour SRM 1568a, Typical Diet SRM 1548a, Wheat Flour SRM 1567a and Bovine Muscle Powder RM 8414) were analyzed. Additional validation data are provided based on the analysis of 18 different types of food samples by the proposed method and using comparative methods with AAS as the detector. |
| doi_str_mv | 10.1016/j.foodchem.2008.06.010 |
| format | Article |
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mg of powdered food samples were accurately weighed into a Teflon digestion vessel. Then, 4
ml of 20% v/v concentrated nitric acid and 2
ml of hydrogen peroxide were added. Decomposition of samples was carried out in a microwave digestion system. In order to verify the accuracy and precision of the proposed method, five Standard Reference Materials from the National Institute of Standards and Technology (NIST) (Whole Egg Powder RM 8415, Rice Flour SRM 1568a, Typical Diet SRM 1548a, Wheat Flour SRM 1567a and Bovine Muscle Powder RM 8414) were analyzed. Additional validation data are provided based on the analysis of 18 different types of food samples by the proposed method and using comparative methods with AAS as the detector.</description><identifier>ISSN: 0308-8146</identifier><identifier>EISSN: 1873-7072</identifier><identifier>DOI: 10.1016/j.foodchem.2008.06.010</identifier><identifier>CODEN: FOCHDJ</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Biological and medical sciences ; Data processing ; detection ; food analysis ; food contamination ; Food industries ; food safety ; Food samples ; foods ; Fundamental and applied biological sciences. Psychology ; ICP-MS ; in vitro digestion ; inductively coupled plasma mass spectrometry ; mass spectrometry ; Oryza sativa ; Rapid determination ; toxic substances ; Trace elements</subject><ispartof>Food chemistry, 2009-02, Vol.112 (3), p.727-732</ispartof><rights>2008 Elsevier Ltd</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c464t-4cd07ae947df60ccee21367c5394f441faab8b7101a174406ae8642dbd18c6e63</citedby><cites>FETCH-LOGICAL-c464t-4cd07ae947df60ccee21367c5394f441faab8b7101a174406ae8642dbd18c6e63</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.foodchem.2008.06.010$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20686334$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Nardi, Elene P.</creatorcontrib><creatorcontrib>Evangelista, Fábio S.</creatorcontrib><creatorcontrib>Tormen, Luciano</creatorcontrib><creatorcontrib>Saint´Pierre, Tatiana D.</creatorcontrib><creatorcontrib>Curtius, Adilson J.</creatorcontrib><creatorcontrib>Souza, Samuel S. de</creatorcontrib><creatorcontrib>Barbosa, Fernando</creatorcontrib><title>The use of inductively coupled plasma mass spectrometry (ICP-MS) for the determination of toxic and essential elements in different types of food samples</title><title>Food chemistry</title><description>This paper describes a simple method for the determination of sixteen elements in food samples by using inductively coupled plasma spectrometry (ICP-MS). Prior to analysis, 100–250
mg of powdered food samples were accurately weighed into a Teflon digestion vessel. Then, 4
ml of 20% v/v concentrated nitric acid and 2
ml of hydrogen peroxide were added. Decomposition of samples was carried out in a microwave digestion system. In order to verify the accuracy and precision of the proposed method, five Standard Reference Materials from the National Institute of Standards and Technology (NIST) (Whole Egg Powder RM 8415, Rice Flour SRM 1568a, Typical Diet SRM 1548a, Wheat Flour SRM 1567a and Bovine Muscle Powder RM 8414) were analyzed. Additional validation data are provided based on the analysis of 18 different types of food samples by the proposed method and using comparative methods with AAS as the detector.</description><subject>Biological and medical sciences</subject><subject>Data processing</subject><subject>detection</subject><subject>food analysis</subject><subject>food contamination</subject><subject>Food industries</subject><subject>food safety</subject><subject>Food samples</subject><subject>foods</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>ICP-MS</subject><subject>in vitro digestion</subject><subject>inductively coupled plasma mass spectrometry</subject><subject>mass spectrometry</subject><subject>Oryza sativa</subject><subject>Rapid determination</subject><subject>toxic substances</subject><subject>Trace elements</subject><issn>0308-8146</issn><issn>1873-7072</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNqFkc1u1DAQxyMEEsvCK4AvCDgkjBPjeG-gFR-VikBqe7a89ph6lcTB41Tso_C2ONrClZNt6f_hmV9VPefQcODy7bHxMTp7i2PTAqgGZAMcHlQbrvqu7qFvH1Yb6EDVigv5uHpCdASAFrjaVL-vb5EthCx6Fia32BzucDgxG5d5QMfmwdBo2GiIGM1oc4oj5nRiry_23-uvV2-Yj4nlEuIwYxrDZHKI0xqX469gmZkcQyKccjADwwHHcqXSxVzwHlN5sXyakVbLOggjM5Zqelo98mYgfHZ_bqubTx-v91_qy2-fL_YfLmsrpMi1sA56gzvROy_BWsSWd7K377qd8EJwb8xBHfqyKcN7IUAaVFK07uC4shJlt61enXPnFH8uSFmPgSwOg5kwLqSLSSou1aqUZ6VNkSih13MKo0knzUGvKPRR_0WhVxQapC4oivHlfYUhawafzGQD_XO3sKZ3ouhenHXeRG1-pKK5uSqcOoBd26sy2LZ6f1Zg2chdwKTJBpwsupAKHO1i-N9n_gBTW66F</recordid><startdate>20090201</startdate><enddate>20090201</enddate><creator>Nardi, Elene P.</creator><creator>Evangelista, Fábio S.</creator><creator>Tormen, Luciano</creator><creator>Saint´Pierre, Tatiana D.</creator><creator>Curtius, Adilson J.</creator><creator>Souza, Samuel S. de</creator><creator>Barbosa, Fernando</creator><general>Elsevier Ltd</general><general>[Amsterdam]: Elsevier Science</general><general>Elsevier</general><scope>FBQ</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U7</scope><scope>C1K</scope></search><sort><creationdate>20090201</creationdate><title>The use of inductively coupled plasma mass spectrometry (ICP-MS) for the determination of toxic and essential elements in different types of food samples</title><author>Nardi, Elene P. ; Evangelista, Fábio S. ; Tormen, Luciano ; Saint´Pierre, Tatiana D. ; Curtius, Adilson J. ; Souza, Samuel S. de ; Barbosa, Fernando</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c464t-4cd07ae947df60ccee21367c5394f441faab8b7101a174406ae8642dbd18c6e63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>Biological and medical sciences</topic><topic>Data processing</topic><topic>detection</topic><topic>food analysis</topic><topic>food contamination</topic><topic>Food industries</topic><topic>food safety</topic><topic>Food samples</topic><topic>foods</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>ICP-MS</topic><topic>in vitro digestion</topic><topic>inductively coupled plasma mass spectrometry</topic><topic>mass spectrometry</topic><topic>Oryza sativa</topic><topic>Rapid determination</topic><topic>toxic substances</topic><topic>Trace elements</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nardi, Elene P.</creatorcontrib><creatorcontrib>Evangelista, Fábio S.</creatorcontrib><creatorcontrib>Tormen, Luciano</creatorcontrib><creatorcontrib>Saint´Pierre, Tatiana D.</creatorcontrib><creatorcontrib>Curtius, Adilson J.</creatorcontrib><creatorcontrib>Souza, Samuel S. de</creatorcontrib><creatorcontrib>Barbosa, Fernando</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Toxicology Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><jtitle>Food chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nardi, Elene P.</au><au>Evangelista, Fábio S.</au><au>Tormen, Luciano</au><au>Saint´Pierre, Tatiana D.</au><au>Curtius, Adilson J.</au><au>Souza, Samuel S. de</au><au>Barbosa, Fernando</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The use of inductively coupled plasma mass spectrometry (ICP-MS) for the determination of toxic and essential elements in different types of food samples</atitle><jtitle>Food chemistry</jtitle><date>2009-02-01</date><risdate>2009</risdate><volume>112</volume><issue>3</issue><spage>727</spage><epage>732</epage><pages>727-732</pages><issn>0308-8146</issn><eissn>1873-7072</eissn><coden>FOCHDJ</coden><abstract>This paper describes a simple method for the determination of sixteen elements in food samples by using inductively coupled plasma spectrometry (ICP-MS). Prior to analysis, 100–250
mg of powdered food samples were accurately weighed into a Teflon digestion vessel. Then, 4
ml of 20% v/v concentrated nitric acid and 2
ml of hydrogen peroxide were added. Decomposition of samples was carried out in a microwave digestion system. In order to verify the accuracy and precision of the proposed method, five Standard Reference Materials from the National Institute of Standards and Technology (NIST) (Whole Egg Powder RM 8415, Rice Flour SRM 1568a, Typical Diet SRM 1548a, Wheat Flour SRM 1567a and Bovine Muscle Powder RM 8414) were analyzed. Additional validation data are provided based on the analysis of 18 different types of food samples by the proposed method and using comparative methods with AAS as the detector.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.foodchem.2008.06.010</doi><tpages>6</tpages></addata></record> |
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| identifier | ISSN: 0308-8146 |
| ispartof | Food chemistry, 2009-02, Vol.112 (3), p.727-732 |
| issn | 0308-8146 1873-7072 |
| language | eng |
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| source | Access via ScienceDirect (Elsevier) |
| subjects | Biological and medical sciences Data processing detection food analysis food contamination Food industries food safety Food samples foods Fundamental and applied biological sciences. Psychology ICP-MS in vitro digestion inductively coupled plasma mass spectrometry mass spectrometry Oryza sativa Rapid determination toxic substances Trace elements |
| title | The use of inductively coupled plasma mass spectrometry (ICP-MS) for the determination of toxic and essential elements in different types of food samples |
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