Subnanometer-Diameter Wires Isolated in a Polymer Matrix by Fast Polymerization
The preparation and analysis of inorganic-organic polymer nanocomposites consisting of inorganic nanowires and multiwire "cables" in a random-coil organic polymer host is reported. Dissolution of inorganic (LiMo$_3$Se$_3$)$_n$ wires in a strongly coordinating monomer, vinylene carbonate, a...
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| Veröffentlicht in: | Science (American Association for the Advancement of Science) 1996-08, Vol.273 (5276), p.782-784 |
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| container_issue | 5276 |
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| container_title | Science (American Association for the Advancement of Science) |
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| creator | Golden, Josh H. DiSalvo, Francis J. Jean M. J. Fréchet Silcox, John Thomas, Malcolm Elman, Jim |
| description | The preparation and analysis of inorganic-organic polymer nanocomposites consisting of inorganic nanowires and multiwire "cables" in a random-coil organic polymer host is reported. Dissolution of inorganic (LiMo$_3$Se$_3$)$_n$ wires in a strongly coordinating monomer, vinylene carbonate, and the use of a rapid polymerization in the presence of a cross-linking agent produce nanocomposites without phase separation. Polymerization of dilute solutions yields a material containing mostly (Mo$_3$Se$_{3^-}$)$_n$ mono- and biwires, 6 to 20 angstroms in diameter and 50 to 100 nanometers long. Polymerization of more concentrated liquid crystalline solutions yields a nanocomposite containing oriented multiwire cables, 20 to 40 angstroms in diameter and up to 1500 nanometers long, that display optical anisotropy and electrical conductivity. |
| doi_str_mv | 10.1126/science.273.5276.782 |
| format | Article |
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J. Fréchet ; Silcox, John ; Thomas, Malcolm ; Elman, Jim</creator><creatorcontrib>Golden, Josh H. ; DiSalvo, Francis J. ; Jean M. J. Fréchet ; Silcox, John ; Thomas, Malcolm ; Elman, Jim</creatorcontrib><description>The preparation and analysis of inorganic-organic polymer nanocomposites consisting of inorganic nanowires and multiwire "cables" in a random-coil organic polymer host is reported. Dissolution of inorganic (LiMo$_3$Se$_3$)$_n$ wires in a strongly coordinating monomer, vinylene carbonate, and the use of a rapid polymerization in the presence of a cross-linking agent produce nanocomposites without phase separation. Polymerization of dilute solutions yields a material containing mostly (Mo$_3$Se$_{3^-}$)$_n$ mono- and biwires, 6 to 20 angstroms in diameter and 50 to 100 nanometers long. 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Polymerization of dilute solutions yields a material containing mostly (Mo$_3$Se$_{3^-}$)$_n$ mono- and biwires, 6 to 20 angstroms in diameter and 50 to 100 nanometers long. Polymerization of more concentrated liquid crystalline solutions yields a nanocomposite containing oriented multiwire cables, 20 to 40 angstroms in diameter and up to 1500 nanometers long, that display optical anisotropy and electrical conductivity.</abstract><cop>Washington, DC</cop><pub>American Society for the Advancement of Science</pub><pmid>8670415</pmid><doi>10.1126/science.273.5276.782</doi><tpages>3</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0036-8075 |
| ispartof | Science (American Association for the Advancement of Science), 1996-08, Vol.273 (5276), p.782-784 |
| issn | 0036-8075 1095-9203 |
| language | eng |
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| source | JSTOR Archive Collection A-Z Listing; American Association for the Advancement of Science |
| subjects | Applied sciences Change Agents Chemical bonding Composites Conductivity Exact sciences and technology Forms of application and semi-finished materials Inhalants Innovations Molecular weight Monomers Nanocomposites Nanotechnology Nanowires Organic chemistry Polymer industry, paints, wood Polymerization Polymers Solvents Technology of polymers Thin films Wire |
| title | Subnanometer-Diameter Wires Isolated in a Polymer Matrix by Fast Polymerization |
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