On-line coupling of solid-phase extraction with mass spectrometry for the analysis of biological samples: III. Determination of prednisolone in serum

Solid-phase extraction (SPE) was directly coupled to mass spectrometry (MS) to assess the feasibility of the system for the rapid determination of prednisolone in serum. A C 18 stationary phase allowed washing of the cartridge with 25% methanol. Elution was performed by switching the methanol percen...

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Veröffentlicht in:	Journal of chromatography. B, Analytical technologies in the biomedical and life sciences Analytical technologies in the biomedical and life sciences, 2003-08, Vol.794 (1), p.185-192
Hauptverfasser:	van Hout, M.W.J, Hofland, C.M, Niederländer, H.A.G, Bruins, A.P, de Zeeuw, R.A, de Jong, G.J
Format:	Artikel
Sprache:	eng
Schlagworte:	Analysis Biological and medical sciences General pharmacology Glucocorticoids - blood Humans Mass Spectrometry - methods Medical sciences Pharmacology. Drug treatments Prednisolone Prednisolone - blood Sensitivity and Specificity
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