A highly selective and sensitive disposable carbon composite PVC-based membrane for determination of lead ion in environmental samples
A Pt wire coated with phenyl hydrazone derivative–carbon composite in a poly(vinyl chloride) membrane was used for detection of lead. The sensor had a Nernstian slope of 29.46 ± 0.41 mV/decade over a wide linear concentration range of 7.7 × 10 −7 to 1.0 × 10 −1 mol L −1 for Pb(NO 3) 2. The detection...
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| Veröffentlicht in: | Journal of hazardous materials 2010-02, Vol.174 (1), p.656-661 |
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| container_title | Journal of hazardous materials |
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| creator | Abbaspour, A. Mirahmadi, E. Khalafi-nejad, A. Babamohammadi, S. |
| description | A Pt wire coated with phenyl hydrazone derivative–carbon composite in a poly(vinyl chloride) membrane was used for detection of lead. The sensor had a Nernstian slope of 29.46
±
0.41
mV/decade over a wide linear concentration range of 7.7
×
10
−7 to 1.0
×
10
−1
mol
L
−1 for Pb(NO
3)
2. The detection limit was 3.2
×
10
−7
mol
L
−1 and the electrode was applicable in the pH range of 3.7–6.3. It had a short response time of approximately 6
s and was used at least for 70 days. The electrode has exhibited good selectivity for Pb(II) relative to 19 other metal ions. The functionality of the proposed sensor was also investigated in binary water–alcohol mixture and it concluded that 23% water–methanol and 20% water–ethanol content could not bring out any changes in its potential. The practical analytical utility of the electrode was demonstrated by measurement of Pb(II) in mineral rock and potentiometric titration of sulfate anion. |
| doi_str_mv | 10.1016/j.jhazmat.2009.09.101 |
| format | Article |
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±
0.41
mV/decade over a wide linear concentration range of 7.7
×
10
−7 to 1.0
×
10
−1
mol
L
−1 for Pb(NO
3)
2. The detection limit was 3.2
×
10
−7
mol
L
−1 and the electrode was applicable in the pH range of 3.7–6.3. It had a short response time of approximately 6
s and was used at least for 70 days. The electrode has exhibited good selectivity for Pb(II) relative to 19 other metal ions. The functionality of the proposed sensor was also investigated in binary water–alcohol mixture and it concluded that 23% water–methanol and 20% water–ethanol content could not bring out any changes in its potential. The practical analytical utility of the electrode was demonstrated by measurement of Pb(II) in mineral rock and potentiometric titration of sulfate anion.</description><identifier>ISSN: 0304-3894</identifier><identifier>EISSN: 1873-3336</identifier><identifier>DOI: 10.1016/j.jhazmat.2009.09.101</identifier><identifier>PMID: 19828247</identifier><identifier>CODEN: JHMAD9</identifier><language>eng</language><publisher>Kidlington: Elsevier B.V</publisher><subject>Applied sciences ; Butyl-3-(2-phenylhydrazono)indolin-2-one ; Carbon ; Carbon composite ; Coated wire electrode ; Environmental Pollutants - analysis ; Exact sciences and technology ; Ion-Selective Electrodes ; Lead ; Lead - analysis ; Magnetic Resonance Spectroscopy ; Membranes, Artificial ; Pollution ; Polyvinyl Chloride ; PVC ; Spectrophotometry, Infrared</subject><ispartof>Journal of hazardous materials, 2010-02, Vol.174 (1), p.656-661</ispartof><rights>2009 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c394t-f036779b999340133f82ec855de9c86e23b5472ac9768ea5aae8c51f1a63abc03</citedby><cites>FETCH-LOGICAL-c394t-f036779b999340133f82ec855de9c86e23b5472ac9768ea5aae8c51f1a63abc03</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jhazmat.2009.09.101$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22341655$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/19828247$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Abbaspour, A.</creatorcontrib><creatorcontrib>Mirahmadi, E.</creatorcontrib><creatorcontrib>Khalafi-nejad, A.</creatorcontrib><creatorcontrib>Babamohammadi, S.</creatorcontrib><title>A highly selective and sensitive disposable carbon composite PVC-based membrane for determination of lead ion in environmental samples</title><title>Journal of hazardous materials</title><addtitle>J Hazard Mater</addtitle><description>A Pt wire coated with phenyl hydrazone derivative–carbon composite in a poly(vinyl chloride) membrane was used for detection of lead. The sensor had a Nernstian slope of 29.46
±
0.41
mV/decade over a wide linear concentration range of 7.7
×
10
−7 to 1.0
×
10
−1
mol
L
−1 for Pb(NO
3)
2. The detection limit was 3.2
×
10
−7
mol
L
−1 and the electrode was applicable in the pH range of 3.7–6.3. It had a short response time of approximately 6
s and was used at least for 70 days. The electrode has exhibited good selectivity for Pb(II) relative to 19 other metal ions. The functionality of the proposed sensor was also investigated in binary water–alcohol mixture and it concluded that 23% water–methanol and 20% water–ethanol content could not bring out any changes in its potential. The practical analytical utility of the electrode was demonstrated by measurement of Pb(II) in mineral rock and potentiometric titration of sulfate anion.</description><subject>Applied sciences</subject><subject>Butyl-3-(2-phenylhydrazono)indolin-2-one</subject><subject>Carbon</subject><subject>Carbon composite</subject><subject>Coated wire electrode</subject><subject>Environmental Pollutants - analysis</subject><subject>Exact sciences and technology</subject><subject>Ion-Selective Electrodes</subject><subject>Lead</subject><subject>Lead - analysis</subject><subject>Magnetic Resonance Spectroscopy</subject><subject>Membranes, Artificial</subject><subject>Pollution</subject><subject>Polyvinyl Chloride</subject><subject>PVC</subject><subject>Spectrophotometry, Infrared</subject><issn>0304-3894</issn><issn>1873-3336</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkduKFDEQhoMo7jj6CEpuxKsek04fkitZBk-wsF7sehuq09VOhhzGpGdgfQCf24zT6OVCQVI_XyXF_xPymrMNZ7x7v9_sd_DLw7ypGVObUkV-QlZc9qISQnRPyYoJ1lRCquaKvMh5zxjjfds8J1dcyVrWTb8iv6_pzv7YuQea0aGZ7QkphLF0Idu_3WjzIWYYHFIDaYiBmuiLYmek375vqwEyjtSjHxIEpFNMdMQZk7cBZlvwOFGHMNLz3QaK4WRTDB7DDI5m8AeH-SV5NoHL-Go51-T-08e77Zfq5vbz1-31TWWEauZqYqLrezUopUTDuBCTrNHIth1RGdlhLYa26Wswqu8kQguA0rR84tAJGAwTa_Lu8u4hxZ9HzLP2Nht0rqwej1n3ouF9LYt_a9JeSJNizgknfUjWQ3rQnOlzAnqvlwT0OQFdqshl7s3yw3HwOP6fWiwvwNsFgGzATcU1Y_M_rq7LCl3bFu7DhcPix8li0tlYDAZHm0pQeoz2kVX-APGzqXU</recordid><startdate>20100215</startdate><enddate>20100215</enddate><creator>Abbaspour, A.</creator><creator>Mirahmadi, E.</creator><creator>Khalafi-nejad, A.</creator><creator>Babamohammadi, S.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20100215</creationdate><title>A highly selective and sensitive disposable carbon composite PVC-based membrane for determination of lead ion in environmental samples</title><author>Abbaspour, A. ; Mirahmadi, E. ; Khalafi-nejad, A. ; Babamohammadi, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c394t-f036779b999340133f82ec855de9c86e23b5472ac9768ea5aae8c51f1a63abc03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Applied sciences</topic><topic>Butyl-3-(2-phenylhydrazono)indolin-2-one</topic><topic>Carbon</topic><topic>Carbon composite</topic><topic>Coated wire electrode</topic><topic>Environmental Pollutants - analysis</topic><topic>Exact sciences and technology</topic><topic>Ion-Selective Electrodes</topic><topic>Lead</topic><topic>Lead - analysis</topic><topic>Magnetic Resonance Spectroscopy</topic><topic>Membranes, Artificial</topic><topic>Pollution</topic><topic>Polyvinyl Chloride</topic><topic>PVC</topic><topic>Spectrophotometry, Infrared</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Abbaspour, A.</creatorcontrib><creatorcontrib>Mirahmadi, E.</creatorcontrib><creatorcontrib>Khalafi-nejad, A.</creatorcontrib><creatorcontrib>Babamohammadi, S.</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of hazardous materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Abbaspour, A.</au><au>Mirahmadi, E.</au><au>Khalafi-nejad, A.</au><au>Babamohammadi, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A highly selective and sensitive disposable carbon composite PVC-based membrane for determination of lead ion in environmental samples</atitle><jtitle>Journal of hazardous materials</jtitle><addtitle>J Hazard Mater</addtitle><date>2010-02-15</date><risdate>2010</risdate><volume>174</volume><issue>1</issue><spage>656</spage><epage>661</epage><pages>656-661</pages><issn>0304-3894</issn><eissn>1873-3336</eissn><coden>JHMAD9</coden><abstract>A Pt wire coated with phenyl hydrazone derivative–carbon composite in a poly(vinyl chloride) membrane was used for detection of lead. The sensor had a Nernstian slope of 29.46
±
0.41
mV/decade over a wide linear concentration range of 7.7
×
10
−7 to 1.0
×
10
−1
mol
L
−1 for Pb(NO
3)
2. The detection limit was 3.2
×
10
−7
mol
L
−1 and the electrode was applicable in the pH range of 3.7–6.3. It had a short response time of approximately 6
s and was used at least for 70 days. The electrode has exhibited good selectivity for Pb(II) relative to 19 other metal ions. The functionality of the proposed sensor was also investigated in binary water–alcohol mixture and it concluded that 23% water–methanol and 20% water–ethanol content could not bring out any changes in its potential. The practical analytical utility of the electrode was demonstrated by measurement of Pb(II) in mineral rock and potentiometric titration of sulfate anion.</abstract><cop>Kidlington</cop><pub>Elsevier B.V</pub><pmid>19828247</pmid><doi>10.1016/j.jhazmat.2009.09.101</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0304-3894 |
| ispartof | Journal of hazardous materials, 2010-02, Vol.174 (1), p.656-661 |
| issn | 0304-3894 1873-3336 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_734172833 |
| source | MEDLINE; Access via ScienceDirect (Elsevier) |
| subjects | Applied sciences Butyl-3-(2-phenylhydrazono)indolin-2-one Carbon Carbon composite Coated wire electrode Environmental Pollutants - analysis Exact sciences and technology Ion-Selective Electrodes Lead Lead - analysis Magnetic Resonance Spectroscopy Membranes, Artificial Pollution Polyvinyl Chloride PVC Spectrophotometry, Infrared |
| title | A highly selective and sensitive disposable carbon composite PVC-based membrane for determination of lead ion in environmental samples |
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