Statistical mixture design development of digestion methods for Oyster tissue using inductively coupled plasma optical emission spectrometry for the determination of metallic ions
The quantitative determination of chemical elements in organic or biological samples is an important analytical problem. Normally the elements to be determined in the organic matrix must be transformed into a simple inorganic form. A digestion method by heating on a block digestor has been developed...
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| Veröffentlicht in: | Talanta (Oxford) 2009-12, Vol.80 (2), p.559-564 |
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| creator | Nano, R.M.W. Bruns, R.E. Ferreira, S.L.C. Baccan, N. Cadore, S. |
| description | The quantitative determination of chemical elements in organic or biological samples is an important analytical problem. Normally the elements to be determined in the organic matrix must be transformed into a simple inorganic form. A digestion method by heating on a block digestor has been developed for the determination of Al, As, Ba, Ca, Cd, Co, Cu, Fe, Mg, Mn, V and Zn in Oyster tissue by ICP OES. A simplex centroid statistical mixture design has been used to study the effects of changing HNO
3, HCl and H
2O
2 reagent proportions on the digestion of these samples. Response surface and principal component analyses show that the species Ca, Cd, Cu, Fe, Mg, Mn and Zn have very similar analytical tendencies under this experiment. By means of mixture modeling maximum recoveries for these ions were predicted using 19%, 18% and 63% of the HCl, HNO
3 and H
2O
2 pseudocomponent mixtures, respectively. This corresponds to 21.4%, 30.8% and 47.8% of the HCl, HNO
3 and H
2O
2 commercial solutions. Furthermore the As, Co and V ions present large recoveries for these mixtures as well. The Al and Ba ion recoveries are seen to be independent of the mixture proportions. The analysis of Oyster tissue reference material (SRM 1566b – NIST) under optimized conditions at the selected wavelengths resulted in ion recoveries between 90% and 100%. |
| doi_str_mv | 10.1016/j.talanta.2009.07.025 |
| format | Article |
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3, HCl and H
2O
2 reagent proportions on the digestion of these samples. Response surface and principal component analyses show that the species Ca, Cd, Cu, Fe, Mg, Mn and Zn have very similar analytical tendencies under this experiment. By means of mixture modeling maximum recoveries for these ions were predicted using 19%, 18% and 63% of the HCl, HNO
3 and H
2O
2 pseudocomponent mixtures, respectively. This corresponds to 21.4%, 30.8% and 47.8% of the HCl, HNO
3 and H
2O
2 commercial solutions. Furthermore the As, Co and V ions present large recoveries for these mixtures as well. The Al and Ba ion recoveries are seen to be independent of the mixture proportions. The analysis of Oyster tissue reference material (SRM 1566b – NIST) under optimized conditions at the selected wavelengths resulted in ion recoveries between 90% and 100%.</description><identifier>ISSN: 0039-9140</identifier><identifier>EISSN: 1873-3573</identifier><identifier>DOI: 10.1016/j.talanta.2009.07.025</identifier><identifier>PMID: 19836520</identifier><identifier>CODEN: TLNTA2</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Aluminum - analysis ; Aluminum - chemistry ; Analysis of Variance ; Analytical chemistry ; Animals ; Arsenic - analysis ; Arsenic - chemistry ; Atomic emission spectrometry ; Barium - analysis ; Barium - chemistry ; Biological samples ; Cadmium - analysis ; Cadmium - chemistry ; Calcium - analysis ; Calcium - chemistry ; Chemistry ; Chemistry Techniques, Analytical - methods ; Cobalt - analysis ; Cobalt - chemistry ; Copper - analysis ; Copper - chemistry ; Exact sciences and technology ; Hydrochloric Acid - chemistry ; Hydrogen Peroxide - chemistry ; Ions - analysis ; Ions - chemistry ; Iron - analysis ; Iron - chemistry ; Magnesium - analysis ; Magnesium - chemistry ; Manganese - analysis ; Manganese - chemistry ; Metallic ions ; Metals - analysis ; Metals - chemistry ; Nitric Acid - chemistry ; Ostreidae - chemistry ; Reproducibility of Results ; Simplex centroid design ; Spectrometric and optical methods ; Spectrum Analysis - methods ; Statistical mixture design ; Vanadium - analysis ; Vanadium - chemistry ; Zinc - analysis ; Zinc - chemistry</subject><ispartof>Talanta (Oxford), 2009-12, Vol.80 (2), p.559-564</ispartof><rights>2009 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c472t-4a75f0b5a60b873b3336e1a40b7835e2f5f4479b59c3fa26d0d0ae0efc4fd6f03</citedby><cites>FETCH-LOGICAL-c472t-4a75f0b5a60b873b3336e1a40b7835e2f5f4479b59c3fa26d0d0ae0efc4fd6f03</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0039914009005840$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22537056$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/19836520$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Nano, R.M.W.</creatorcontrib><creatorcontrib>Bruns, R.E.</creatorcontrib><creatorcontrib>Ferreira, S.L.C.</creatorcontrib><creatorcontrib>Baccan, N.</creatorcontrib><creatorcontrib>Cadore, S.</creatorcontrib><title>Statistical mixture design development of digestion methods for Oyster tissue using inductively coupled plasma optical emission spectrometry for the determination of metallic ions</title><title>Talanta (Oxford)</title><addtitle>Talanta</addtitle><description>The quantitative determination of chemical elements in organic or biological samples is an important analytical problem. Normally the elements to be determined in the organic matrix must be transformed into a simple inorganic form. A digestion method by heating on a block digestor has been developed for the determination of Al, As, Ba, Ca, Cd, Co, Cu, Fe, Mg, Mn, V and Zn in Oyster tissue by ICP OES. A simplex centroid statistical mixture design has been used to study the effects of changing HNO
3, HCl and H
2O
2 reagent proportions on the digestion of these samples. Response surface and principal component analyses show that the species Ca, Cd, Cu, Fe, Mg, Mn and Zn have very similar analytical tendencies under this experiment. By means of mixture modeling maximum recoveries for these ions were predicted using 19%, 18% and 63% of the HCl, HNO
3 and H
2O
2 pseudocomponent mixtures, respectively. This corresponds to 21.4%, 30.8% and 47.8% of the HCl, HNO
3 and H
2O
2 commercial solutions. Furthermore the As, Co and V ions present large recoveries for these mixtures as well. The Al and Ba ion recoveries are seen to be independent of the mixture proportions. The analysis of Oyster tissue reference material (SRM 1566b – NIST) under optimized conditions at the selected wavelengths resulted in ion recoveries between 90% and 100%.</description><subject>Aluminum - analysis</subject><subject>Aluminum - chemistry</subject><subject>Analysis of Variance</subject><subject>Analytical chemistry</subject><subject>Animals</subject><subject>Arsenic - analysis</subject><subject>Arsenic - chemistry</subject><subject>Atomic emission spectrometry</subject><subject>Barium - analysis</subject><subject>Barium - chemistry</subject><subject>Biological samples</subject><subject>Cadmium - analysis</subject><subject>Cadmium - chemistry</subject><subject>Calcium - analysis</subject><subject>Calcium - chemistry</subject><subject>Chemistry</subject><subject>Chemistry Techniques, Analytical - methods</subject><subject>Cobalt - analysis</subject><subject>Cobalt - chemistry</subject><subject>Copper - analysis</subject><subject>Copper - chemistry</subject><subject>Exact sciences and technology</subject><subject>Hydrochloric Acid - chemistry</subject><subject>Hydrogen Peroxide - chemistry</subject><subject>Ions - analysis</subject><subject>Ions - chemistry</subject><subject>Iron - analysis</subject><subject>Iron - chemistry</subject><subject>Magnesium - analysis</subject><subject>Magnesium - chemistry</subject><subject>Manganese - analysis</subject><subject>Manganese - chemistry</subject><subject>Metallic ions</subject><subject>Metals - analysis</subject><subject>Metals - chemistry</subject><subject>Nitric Acid - chemistry</subject><subject>Ostreidae - chemistry</subject><subject>Reproducibility of Results</subject><subject>Simplex centroid design</subject><subject>Spectrometric and optical methods</subject><subject>Spectrum Analysis - methods</subject><subject>Statistical mixture design</subject><subject>Vanadium - analysis</subject><subject>Vanadium - chemistry</subject><subject>Zinc - analysis</subject><subject>Zinc - chemistry</subject><issn>0039-9140</issn><issn>1873-3573</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkc2O1DAQhCMEYoeFRwD5ApwydOw4Pye0WvEnrbQH4Gw5dnvWoyQOtrNinosXpGdnBDc4WZa_rmpXFcXLCrYVVM27_TbrUc9ZbzlAv4V2C1w-KjZV14pSyFY8LjYAoi_7qoaL4llKewDgAsTT4qLqO9FIDpvi19ess0_ZGz2yyf_Ma0RmMfndTMc9jmGZcM4sOGb9DgkMM5sw3wWbmAuR3R5SxshII63I1uTnHfOzXU32NH1gJqzLiJYto06TZmE5WeFEA0ettKDJMZBkPDwI5rvjAqQ5-Vk_2JE3Petx9IbRPT0vnjg9JnxxPi-L7x8_fLv-XN7cfvpyfXVTmrrluax1Kx0MUjcwUCiDEKLBStcwtJ2QyJ10dd32g-yNcJo3FixoBHSmdrZxIC6LtyfdJYYfK_1d0dIGR4odw5pUK2roRccbIt_8k-QV9LLiHYHyBJoYUoro1BL9pONBVaCOvaq9Oveqjr0qaBX1SnOvzgbrMKH9O3UukoDXZ0AnytdFPRuf_nCcNFqQx03fnzik4O49RpWMx9mg9ZGKUDb4_6zyGxtcyfs</recordid><startdate>20091215</startdate><enddate>20091215</enddate><creator>Nano, R.M.W.</creator><creator>Bruns, R.E.</creator><creator>Ferreira, S.L.C.</creator><creator>Baccan, N.</creator><creator>Cadore, S.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U7</scope><scope>C1K</scope><scope>F1W</scope><scope>H95</scope><scope>L.G</scope><scope>7X8</scope></search><sort><creationdate>20091215</creationdate><title>Statistical mixture design development of digestion methods for Oyster tissue using inductively coupled plasma optical emission spectrometry for the determination of metallic ions</title><author>Nano, R.M.W. ; Bruns, R.E. ; Ferreira, S.L.C. ; Baccan, N. ; Cadore, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c472t-4a75f0b5a60b873b3336e1a40b7835e2f5f4479b59c3fa26d0d0ae0efc4fd6f03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>Aluminum - analysis</topic><topic>Aluminum - chemistry</topic><topic>Analysis of Variance</topic><topic>Analytical chemistry</topic><topic>Animals</topic><topic>Arsenic - analysis</topic><topic>Arsenic - chemistry</topic><topic>Atomic emission spectrometry</topic><topic>Barium - analysis</topic><topic>Barium - chemistry</topic><topic>Biological samples</topic><topic>Cadmium - analysis</topic><topic>Cadmium - chemistry</topic><topic>Calcium - analysis</topic><topic>Calcium - chemistry</topic><topic>Chemistry</topic><topic>Chemistry Techniques, Analytical - methods</topic><topic>Cobalt - analysis</topic><topic>Cobalt - chemistry</topic><topic>Copper - analysis</topic><topic>Copper - chemistry</topic><topic>Exact sciences and technology</topic><topic>Hydrochloric Acid - chemistry</topic><topic>Hydrogen Peroxide - chemistry</topic><topic>Ions - analysis</topic><topic>Ions - chemistry</topic><topic>Iron - analysis</topic><topic>Iron - chemistry</topic><topic>Magnesium - analysis</topic><topic>Magnesium - chemistry</topic><topic>Manganese - analysis</topic><topic>Manganese - chemistry</topic><topic>Metallic ions</topic><topic>Metals - analysis</topic><topic>Metals - chemistry</topic><topic>Nitric Acid - chemistry</topic><topic>Ostreidae - chemistry</topic><topic>Reproducibility of Results</topic><topic>Simplex centroid design</topic><topic>Spectrometric and optical methods</topic><topic>Spectrum Analysis - methods</topic><topic>Statistical mixture design</topic><topic>Vanadium - analysis</topic><topic>Vanadium - chemistry</topic><topic>Zinc - analysis</topic><topic>Zinc - chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nano, R.M.W.</creatorcontrib><creatorcontrib>Bruns, R.E.</creatorcontrib><creatorcontrib>Ferreira, S.L.C.</creatorcontrib><creatorcontrib>Baccan, N.</creatorcontrib><creatorcontrib>Cadore, S.</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Toxicology Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 1: Biological Sciences & Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><collection>MEDLINE - Academic</collection><jtitle>Talanta (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nano, R.M.W.</au><au>Bruns, R.E.</au><au>Ferreira, S.L.C.</au><au>Baccan, N.</au><au>Cadore, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Statistical mixture design development of digestion methods for Oyster tissue using inductively coupled plasma optical emission spectrometry for the determination of metallic ions</atitle><jtitle>Talanta (Oxford)</jtitle><addtitle>Talanta</addtitle><date>2009-12-15</date><risdate>2009</risdate><volume>80</volume><issue>2</issue><spage>559</spage><epage>564</epage><pages>559-564</pages><issn>0039-9140</issn><eissn>1873-3573</eissn><coden>TLNTA2</coden><abstract>The quantitative determination of chemical elements in organic or biological samples is an important analytical problem. Normally the elements to be determined in the organic matrix must be transformed into a simple inorganic form. A digestion method by heating on a block digestor has been developed for the determination of Al, As, Ba, Ca, Cd, Co, Cu, Fe, Mg, Mn, V and Zn in Oyster tissue by ICP OES. A simplex centroid statistical mixture design has been used to study the effects of changing HNO
3, HCl and H
2O
2 reagent proportions on the digestion of these samples. Response surface and principal component analyses show that the species Ca, Cd, Cu, Fe, Mg, Mn and Zn have very similar analytical tendencies under this experiment. By means of mixture modeling maximum recoveries for these ions were predicted using 19%, 18% and 63% of the HCl, HNO
3 and H
2O
2 pseudocomponent mixtures, respectively. This corresponds to 21.4%, 30.8% and 47.8% of the HCl, HNO
3 and H
2O
2 commercial solutions. Furthermore the As, Co and V ions present large recoveries for these mixtures as well. The Al and Ba ion recoveries are seen to be independent of the mixture proportions. The analysis of Oyster tissue reference material (SRM 1566b – NIST) under optimized conditions at the selected wavelengths resulted in ion recoveries between 90% and 100%.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>19836520</pmid><doi>10.1016/j.talanta.2009.07.025</doi><tpages>6</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | Talanta (Oxford), 2009-12, Vol.80 (2), p.559-564 |
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| subjects | Aluminum - analysis Aluminum - chemistry Analysis of Variance Analytical chemistry Animals Arsenic - analysis Arsenic - chemistry Atomic emission spectrometry Barium - analysis Barium - chemistry Biological samples Cadmium - analysis Cadmium - chemistry Calcium - analysis Calcium - chemistry Chemistry Chemistry Techniques, Analytical - methods Cobalt - analysis Cobalt - chemistry Copper - analysis Copper - chemistry Exact sciences and technology Hydrochloric Acid - chemistry Hydrogen Peroxide - chemistry Ions - analysis Ions - chemistry Iron - analysis Iron - chemistry Magnesium - analysis Magnesium - chemistry Manganese - analysis Manganese - chemistry Metallic ions Metals - analysis Metals - chemistry Nitric Acid - chemistry Ostreidae - chemistry Reproducibility of Results Simplex centroid design Spectrometric and optical methods Spectrum Analysis - methods Statistical mixture design Vanadium - analysis Vanadium - chemistry Zinc - analysis Zinc - chemistry |
| title | Statistical mixture design development of digestion methods for Oyster tissue using inductively coupled plasma optical emission spectrometry for the determination of metallic ions |
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