Validation of Selective Ion Flow Tube Mass Spectrometry for Fast Quantification of Volatile Bases Produced on Atlantic Cod (Gadus morhua)
Selective ion flow tube mass spectrometry (SIFT-MS) is a direct mass spectrometric technique that allows qualitative and quantitative analysis of a large number of volatile organic compounds. Because of its speed and ease of use, this nondestructive technique could be considered as a practical tool...
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Veröffentlicht in: | Journal of agricultural and food chemistry 2010-05, Vol.58 (9), p.5213-5219 |
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creator | Noseda, Bert Ragaert, Peter Pauwels, Danny Anthierens, Tom Van Langenhove, Herman Dewulf, Jo Devlieghere, Frank |
description | Selective ion flow tube mass spectrometry (SIFT-MS) is a direct mass spectrometric technique that allows qualitative and quantitative analysis of a large number of volatile organic compounds. Because of its speed and ease of use, this nondestructive technique could be considered as a practical tool for quality control. This research focuses on the possibilities of direct headspace sampling by SIFT-MS for the quantification of the volatile basic nitrogen content (TVB-N) of fish fillets. These volatile bases [trimethylamine (TMA), dimethylamine (DMA), and ammonia] give additional information in conjunction with the sensory scoring and microbiological analysis about the quality of the fish fillets. This research validates in a first part the SIFT-MS method for the quantification of the volatile bases in mixed cod samples. With regard to the investigated linearity, repeatability, reproducibility, recovery, limit of detection, and limit of quantification, SIFT-MS appeared to be an adequate technique for measuring volatile bases spiked on cod. In the second part of this research, the technique was validated for the analysis of volatile bases on cod fillets during a storage experiment under ice. A good correlation was obtained between the proposed direct headspace sampling and traditional methods. The sensitivity of the SIFT-MS method can be improved when cod fillets are made more alkaline (pH >11) during sampling. |
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Because of its speed and ease of use, this nondestructive technique could be considered as a practical tool for quality control. This research focuses on the possibilities of direct headspace sampling by SIFT-MS for the quantification of the volatile basic nitrogen content (TVB-N) of fish fillets. These volatile bases [trimethylamine (TMA), dimethylamine (DMA), and ammonia] give additional information in conjunction with the sensory scoring and microbiological analysis about the quality of the fish fillets. This research validates in a first part the SIFT-MS method for the quantification of the volatile bases in mixed cod samples. With regard to the investigated linearity, repeatability, reproducibility, recovery, limit of detection, and limit of quantification, SIFT-MS appeared to be an adequate technique for measuring volatile bases spiked on cod. In the second part of this research, the technique was validated for the analysis of volatile bases on cod fillets during a storage experiment under ice. A good correlation was obtained between the proposed direct headspace sampling and traditional methods. The sensitivity of the SIFT-MS method can be improved when cod fillets are made more alkaline (pH >11) during sampling.</description><identifier>ISSN: 0021-8561</identifier><identifier>EISSN: 1520-5118</identifier><identifier>DOI: 10.1021/jf904129j</identifier><identifier>PMID: 20387831</identifier><identifier>CODEN: JAFCAU</identifier><language>eng</language><publisher>Washington, DC: American Chemical Society</publisher><subject>ammonia ; Analytical Methods ; Animals ; Biological and medical sciences ; dimethylamine ; equipment performance ; Fish and seafood industries ; fish fillets ; Fishes ; food analysis ; food composition ; Food industries ; Fundamental and applied biological sciences. Psychology ; Gadus morhua ; Ion Flow Tube Mass Spectrometry ; mass spectrometry ; Mass Spectrometry - methods ; Nitrogen - analysis ; quantitative analysis ; rapid methods ; trimethylamine ; validity ; volatile compounds ; Volatilization</subject><ispartof>Journal of agricultural and food chemistry, 2010-05, Vol.58 (9), p.5213-5219</ispartof><rights>Copyright © 2010 American Chemical Society</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a403t-d938f503877ede222af76c26b90683ea508d5d66cb2015cf48d896b018155ecf3</citedby><cites>FETCH-LOGICAL-a403t-d938f503877ede222af76c26b90683ea508d5d66cb2015cf48d896b018155ecf3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/jf904129j$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/jf904129j$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,2765,27076,27924,27925,56738,56788</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22764386$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/20387831$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Noseda, Bert</creatorcontrib><creatorcontrib>Ragaert, Peter</creatorcontrib><creatorcontrib>Pauwels, Danny</creatorcontrib><creatorcontrib>Anthierens, Tom</creatorcontrib><creatorcontrib>Van Langenhove, Herman</creatorcontrib><creatorcontrib>Dewulf, Jo</creatorcontrib><creatorcontrib>Devlieghere, Frank</creatorcontrib><title>Validation of Selective Ion Flow Tube Mass Spectrometry for Fast Quantification of Volatile Bases Produced on Atlantic Cod (Gadus morhua)</title><title>Journal of agricultural and food chemistry</title><addtitle>J. Agric. Food Chem</addtitle><description>Selective ion flow tube mass spectrometry (SIFT-MS) is a direct mass spectrometric technique that allows qualitative and quantitative analysis of a large number of volatile organic compounds. Because of its speed and ease of use, this nondestructive technique could be considered as a practical tool for quality control. This research focuses on the possibilities of direct headspace sampling by SIFT-MS for the quantification of the volatile basic nitrogen content (TVB-N) of fish fillets. These volatile bases [trimethylamine (TMA), dimethylamine (DMA), and ammonia] give additional information in conjunction with the sensory scoring and microbiological analysis about the quality of the fish fillets. This research validates in a first part the SIFT-MS method for the quantification of the volatile bases in mixed cod samples. With regard to the investigated linearity, repeatability, reproducibility, recovery, limit of detection, and limit of quantification, SIFT-MS appeared to be an adequate technique for measuring volatile bases spiked on cod. In the second part of this research, the technique was validated for the analysis of volatile bases on cod fillets during a storage experiment under ice. A good correlation was obtained between the proposed direct headspace sampling and traditional methods. The sensitivity of the SIFT-MS method can be improved when cod fillets are made more alkaline (pH >11) during sampling.</description><subject>ammonia</subject><subject>Analytical Methods</subject><subject>Animals</subject><subject>Biological and medical sciences</subject><subject>dimethylamine</subject><subject>equipment performance</subject><subject>Fish and seafood industries</subject><subject>fish fillets</subject><subject>Fishes</subject><subject>food analysis</subject><subject>food composition</subject><subject>Food industries</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Gadus morhua</subject><subject>Ion Flow Tube Mass Spectrometry</subject><subject>mass spectrometry</subject><subject>Mass Spectrometry - methods</subject><subject>Nitrogen - analysis</subject><subject>quantitative analysis</subject><subject>rapid methods</subject><subject>trimethylamine</subject><subject>validity</subject><subject>volatile compounds</subject><subject>Volatilization</subject><issn>0021-8561</issn><issn>1520-5118</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNptkM1uEzEUhS0EoqGw4AXAG0S7GPDP2ONZloiUSkWA0nY7uuMfmMgTp_YY1Efgresoabrp6l7d8-no3IPQW0o-UcLo55VrSU1Zu3qGZlQwUglK1XM0I0WslJD0CL1KaUUIUaIhL9ERI1w1itMZ-n8DfjAwDWGNg8NL662ehr8WX5TDwod_-Cr3Fn-HlPByU7QYRjvFO-xCxAtIE_6VYT0NbtAHk5vgy-4t_gLJJvwzBpO1NbioZ5Pf0hrPg8En52BywmOIfzKcvkYvHPhk3-znMbpefL2af6suf5xfzM8uK6gJnyrTcuXENn9jjWWMgWukZrJviVTcgiDKCCOl7hmhQrtaGdXKnlBFhbDa8WP0cee7ieE22zR145C09SWYDTl1Dedt3ZReC3m6I3UMKUXruk0cRoh3HSXdtvjuUHxh3-1dcz9acyAfmi7Ahz0ASYN3EdZ6SI8ca2TNlSzc-x3nIHTwOxbmelle4eWDmknVPDqBTt0q5LgudT0R6R5N05_1</recordid><startdate>20100512</startdate><enddate>20100512</enddate><creator>Noseda, Bert</creator><creator>Ragaert, Peter</creator><creator>Pauwels, Danny</creator><creator>Anthierens, Tom</creator><creator>Van Langenhove, Herman</creator><creator>Dewulf, Jo</creator><creator>Devlieghere, Frank</creator><general>American Chemical Society</general><scope>FBQ</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20100512</creationdate><title>Validation of Selective Ion Flow Tube Mass Spectrometry for Fast Quantification of Volatile Bases Produced on Atlantic Cod (Gadus morhua)</title><author>Noseda, Bert ; Ragaert, Peter ; Pauwels, Danny ; Anthierens, Tom ; Van Langenhove, Herman ; Dewulf, Jo ; Devlieghere, Frank</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a403t-d938f503877ede222af76c26b90683ea508d5d66cb2015cf48d896b018155ecf3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>ammonia</topic><topic>Analytical Methods</topic><topic>Animals</topic><topic>Biological and medical sciences</topic><topic>dimethylamine</topic><topic>equipment performance</topic><topic>Fish and seafood industries</topic><topic>fish fillets</topic><topic>Fishes</topic><topic>food analysis</topic><topic>food composition</topic><topic>Food industries</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Gadus morhua</topic><topic>Ion Flow Tube Mass Spectrometry</topic><topic>mass spectrometry</topic><topic>Mass Spectrometry - methods</topic><topic>Nitrogen - analysis</topic><topic>quantitative analysis</topic><topic>rapid methods</topic><topic>trimethylamine</topic><topic>validity</topic><topic>volatile compounds</topic><topic>Volatilization</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Noseda, Bert</creatorcontrib><creatorcontrib>Ragaert, Peter</creatorcontrib><creatorcontrib>Pauwels, Danny</creatorcontrib><creatorcontrib>Anthierens, Tom</creatorcontrib><creatorcontrib>Van Langenhove, Herman</creatorcontrib><creatorcontrib>Dewulf, Jo</creatorcontrib><creatorcontrib>Devlieghere, Frank</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of agricultural and food chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Noseda, Bert</au><au>Ragaert, Peter</au><au>Pauwels, Danny</au><au>Anthierens, Tom</au><au>Van Langenhove, Herman</au><au>Dewulf, Jo</au><au>Devlieghere, Frank</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Validation of Selective Ion Flow Tube Mass Spectrometry for Fast Quantification of Volatile Bases Produced on Atlantic Cod (Gadus morhua)</atitle><jtitle>Journal of agricultural and food chemistry</jtitle><addtitle>J. Agric. Food Chem</addtitle><date>2010-05-12</date><risdate>2010</risdate><volume>58</volume><issue>9</issue><spage>5213</spage><epage>5219</epage><pages>5213-5219</pages><issn>0021-8561</issn><eissn>1520-5118</eissn><coden>JAFCAU</coden><abstract>Selective ion flow tube mass spectrometry (SIFT-MS) is a direct mass spectrometric technique that allows qualitative and quantitative analysis of a large number of volatile organic compounds. Because of its speed and ease of use, this nondestructive technique could be considered as a practical tool for quality control. This research focuses on the possibilities of direct headspace sampling by SIFT-MS for the quantification of the volatile basic nitrogen content (TVB-N) of fish fillets. These volatile bases [trimethylamine (TMA), dimethylamine (DMA), and ammonia] give additional information in conjunction with the sensory scoring and microbiological analysis about the quality of the fish fillets. This research validates in a first part the SIFT-MS method for the quantification of the volatile bases in mixed cod samples. With regard to the investigated linearity, repeatability, reproducibility, recovery, limit of detection, and limit of quantification, SIFT-MS appeared to be an adequate technique for measuring volatile bases spiked on cod. In the second part of this research, the technique was validated for the analysis of volatile bases on cod fillets during a storage experiment under ice. A good correlation was obtained between the proposed direct headspace sampling and traditional methods. The sensitivity of the SIFT-MS method can be improved when cod fillets are made more alkaline (pH >11) during sampling.</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><pmid>20387831</pmid><doi>10.1021/jf904129j</doi><tpages>7</tpages><oa>free_for_read</oa></addata></record> |
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subjects | ammonia Analytical Methods Animals Biological and medical sciences dimethylamine equipment performance Fish and seafood industries fish fillets Fishes food analysis food composition Food industries Fundamental and applied biological sciences. Psychology Gadus morhua Ion Flow Tube Mass Spectrometry mass spectrometry Mass Spectrometry - methods Nitrogen - analysis quantitative analysis rapid methods trimethylamine validity volatile compounds Volatilization |
title | Validation of Selective Ion Flow Tube Mass Spectrometry for Fast Quantification of Volatile Bases Produced on Atlantic Cod (Gadus morhua) |
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