Ion chromatographic determination of organic acids in food samples using a permanent coating graphite carbon column
From the viewpoint of a graphite carbon column with excellent durability, it was applied to the ion chromatography (IC) of several organic acids. The carbon column was permanently coated with the cetyltrimethylammonium (CTMA) ion, and the elution behaviors of several organic acids (acetic acid, lact...
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| Veröffentlicht in: | Talanta (Oxford) 2007-04, Vol.72 (1), p.305-309 |
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| creator | Yoshikawa, Kenji Okamura, Miho Inokuchi, Miki Sakuragawa, Akio |
| description | From the viewpoint of a graphite carbon column with excellent durability, it was applied to the ion chromatography (IC) of several organic acids. The carbon column was permanently coated with the cetyltrimethylammonium (CTMA) ion, and the elution behaviors of several organic acids (acetic acid, lactic acid, succinic acid, malic acid, tartaric acid, citric acid) and inorganic anions (Cl
−, NO
2
−, NO
3
−, SO
4
2−) were examined according to a non-suppressed IC coupled with conductivity detector, when an ion-exchange ability was given to the graphite carbon column. When salicylic acid and sodium salicylate were used as a mobile phase, each organic acid are analyzed approximately 10
min. But the separation of malic acid, chloride and nitrite was difficult. When benzoic acid and 2-amino-2-hydroxymethyl-1,3-puropanediol (tris aminomethane) were used as a mobile phase, tartaric acid and citric acid, etc. with large valency showed tendency to which the width of each peaks extended and retention time increased. However, it was possible to separate excellently for the analytes detected within 10
min. The developed method was then applied to the determination of organic acids in several food samples. |
| doi_str_mv | 10.1016/j.talanta.2006.10.020 |
| format | Article |
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−, NO
2
−, NO
3
−, SO
4
2−) were examined according to a non-suppressed IC coupled with conductivity detector, when an ion-exchange ability was given to the graphite carbon column. When salicylic acid and sodium salicylate were used as a mobile phase, each organic acid are analyzed approximately 10
min. But the separation of malic acid, chloride and nitrite was difficult. When benzoic acid and 2-amino-2-hydroxymethyl-1,3-puropanediol (tris aminomethane) were used as a mobile phase, tartaric acid and citric acid, etc. with large valency showed tendency to which the width of each peaks extended and retention time increased. However, it was possible to separate excellently for the analytes detected within 10
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−, NO
2
−, NO
3
−, SO
4
2−) were examined according to a non-suppressed IC coupled with conductivity detector, when an ion-exchange ability was given to the graphite carbon column. When salicylic acid and sodium salicylate were used as a mobile phase, each organic acid are analyzed approximately 10
min. But the separation of malic acid, chloride and nitrite was difficult. When benzoic acid and 2-amino-2-hydroxymethyl-1,3-puropanediol (tris aminomethane) were used as a mobile phase, tartaric acid and citric acid, etc. with large valency showed tendency to which the width of each peaks extended and retention time increased. However, it was possible to separate excellently for the analytes detected within 10
min. The developed method was then applied to the determination of organic acids in several food samples.</description><subject>Analytical chemistry</subject><subject>Benzoic acid</subject><subject>Cetyltrimethylammonium</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Electrochemical methods</subject><subject>Exact sciences and technology</subject><subject>Graphite carbon column</subject><subject>Ion chromatography</subject><subject>Organic acid</subject><subject>Other chromatographic methods</subject><issn>0039-9140</issn><issn>1873-3573</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqFkE2PFCEQhonRuOPqT9BwMZ5mhKYbmpMxGz822cSLnkkNFLNMuqEF2sR_L5PpZI9eIKl63ip4CHnL2YEzLj-eDxUmiBUOHWOy1Q6sY8_Ijo9K7MWgxHOyY0zoveY9uyGvSjkzxjrBxEtywzVTXHK9I-U-RWofc5qhplOG5TFY6rBinkOEGlo3eZryCWJrgA2u0BCpT8nRAvMyYaFrCfFEgS4tBBFjpTa1aKtdB1akFvLxsihN6xxfkxcepoJvtvuW_Pr65efd9_3Dj2_3d58f9raXrLZPYNc5L9thOTvCyHk_ymMH4Abp0Iteq1EozrXuQDsQ0isQvXPg_Yi-E7fkw3XuktPvFUs1cygWp6YN01qMEmJUSsqxkcOVtDmVktGbJYcZ8l_DmbnoNmez6TYX3Zdy091y77YN63FG95Ta_Dbg_QZAsTD5DNGG8sSNcuh1PzTu05XD5uNPwGyKDRgtupDRVuNS-M9T_gF9XKLY</recordid><startdate>20070415</startdate><enddate>20070415</enddate><creator>Yoshikawa, Kenji</creator><creator>Okamura, Miho</creator><creator>Inokuchi, Miki</creator><creator>Sakuragawa, Akio</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20070415</creationdate><title>Ion chromatographic determination of organic acids in food samples using a permanent coating graphite carbon column</title><author>Yoshikawa, Kenji ; Okamura, Miho ; Inokuchi, Miki ; Sakuragawa, Akio</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c460t-35e22df622dc10ba811486b2aad56def349783711992a9da36f7a34ddaff8ef23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Analytical chemistry</topic><topic>Benzoic acid</topic><topic>Cetyltrimethylammonium</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Electrochemical methods</topic><topic>Exact sciences and technology</topic><topic>Graphite carbon column</topic><topic>Ion chromatography</topic><topic>Organic acid</topic><topic>Other chromatographic methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yoshikawa, Kenji</creatorcontrib><creatorcontrib>Okamura, Miho</creatorcontrib><creatorcontrib>Inokuchi, Miki</creatorcontrib><creatorcontrib>Sakuragawa, Akio</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Talanta (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yoshikawa, Kenji</au><au>Okamura, Miho</au><au>Inokuchi, Miki</au><au>Sakuragawa, Akio</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ion chromatographic determination of organic acids in food samples using a permanent coating graphite carbon column</atitle><jtitle>Talanta (Oxford)</jtitle><addtitle>Talanta</addtitle><date>2007-04-15</date><risdate>2007</risdate><volume>72</volume><issue>1</issue><spage>305</spage><epage>309</epage><pages>305-309</pages><issn>0039-9140</issn><eissn>1873-3573</eissn><coden>TLNTA2</coden><abstract>From the viewpoint of a graphite carbon column with excellent durability, it was applied to the ion chromatography (IC) of several organic acids. The carbon column was permanently coated with the cetyltrimethylammonium (CTMA) ion, and the elution behaviors of several organic acids (acetic acid, lactic acid, succinic acid, malic acid, tartaric acid, citric acid) and inorganic anions (Cl
−, NO
2
−, NO
3
−, SO
4
2−) were examined according to a non-suppressed IC coupled with conductivity detector, when an ion-exchange ability was given to the graphite carbon column. When salicylic acid and sodium salicylate were used as a mobile phase, each organic acid are analyzed approximately 10
min. But the separation of malic acid, chloride and nitrite was difficult. When benzoic acid and 2-amino-2-hydroxymethyl-1,3-puropanediol (tris aminomethane) were used as a mobile phase, tartaric acid and citric acid, etc. with large valency showed tendency to which the width of each peaks extended and retention time increased. However, it was possible to separate excellently for the analytes detected within 10
min. The developed method was then applied to the determination of organic acids in several food samples.</abstract><cop>Amsterdam</cop><cop>Oxford</cop><pub>Elsevier B.V</pub><pmid>19071619</pmid><doi>10.1016/j.talanta.2006.10.020</doi><tpages>5</tpages></addata></record> |
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| ispartof | Talanta (Oxford), 2007-04, Vol.72 (1), p.305-309 |
| issn | 0039-9140 1873-3573 |
| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | Analytical chemistry Benzoic acid Cetyltrimethylammonium Chemistry Chromatographic methods and physical methods associated with chromatography Electrochemical methods Exact sciences and technology Graphite carbon column Ion chromatography Organic acid Other chromatographic methods |
| title | Ion chromatographic determination of organic acids in food samples using a permanent coating graphite carbon column |
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