Determination of trace elements in granites by inductively coupled plasma mass spectrometry
Proposed is a simple and reliable method for the dissolution of granite and the determination of 38 elements by inductively coupled plasma mass spectrometry. One hundred milligrams of sample are digested with 1 ml of HF and 0.5 ml of HNO 3 in screw top PTFE-lined stainless steel bombs at 190°C for 1...
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Veröffentlicht in: | Talanta (Oxford) 2000-03, Vol.51 (3), p.507-513 |
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creator | Liang, Qi Jing, Hu Gregoire, D.Conrad |
description | Proposed is a simple and reliable method for the dissolution of granite and the determination of 38 elements by inductively coupled plasma mass spectrometry. One hundred milligrams of sample are digested with 1 ml of HF and 0.5 ml of HNO
3 in screw top PTFE-lined stainless steel bombs at 190°C for 12 h. Insoluble residues are dissolved using 8 ml of 40% HNO
3 (v/v) heated to 110°C for 3 h. Six granite standard reference materials (GSR-1, JG-2, G-2, NIM-G, SG-3, SG-1a) were studied. Analytical calibration was accomplished using aqueous standard solutions. Rhodium was used as an internal standard to correct for matrix effects and instrument drift. We report data for: Li, Be, Sc, V, Cr, Co, Ni, Cu, Zn, Ga, Rb, Sr, Y, Zr, Nb, Mo, Cs, Ba, Hf, Ta, W, Pb, Th, U and 14 of the rare earth elements. The recoveries for most of these elements in granite ranged from 90 to 110%. |
doi_str_mv | 10.1016/S0039-9140(99)00318-5 |
format | Article |
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3 in screw top PTFE-lined stainless steel bombs at 190°C for 12 h. Insoluble residues are dissolved using 8 ml of 40% HNO
3 (v/v) heated to 110°C for 3 h. Six granite standard reference materials (GSR-1, JG-2, G-2, NIM-G, SG-3, SG-1a) were studied. Analytical calibration was accomplished using aqueous standard solutions. Rhodium was used as an internal standard to correct for matrix effects and instrument drift. We report data for: Li, Be, Sc, V, Cr, Co, Ni, Cu, Zn, Ga, Rb, Sr, Y, Zr, Nb, Mo, Cs, Ba, Hf, Ta, W, Pb, Th, U and 14 of the rare earth elements. The recoveries for most of these elements in granite ranged from 90 to 110%.</description><identifier>ISSN: 0039-9140</identifier><identifier>EISSN: 1873-3573</identifier><identifier>DOI: 10.1016/S0039-9140(99)00318-5</identifier><identifier>PMID: 18967881</identifier><identifier>CODEN: TLNTA2</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Crystalline rocks ; Earth sciences ; Earth, ocean, space ; Exact sciences and technology ; Geochemistry ; Geochemistry: general, methodology, regional studies ; Granites ; ICP mass spectrometry ; Igneous and metamorphic rocks petrology, volcanic processes, magmas ; Trace elements</subject><ispartof>Talanta (Oxford), 2000-03, Vol.51 (3), p.507-513</ispartof><rights>2000 Elsevier Science B.V.</rights><rights>2000 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c509t-f7cf11b252d60ae1154e6a883faa7cf3bb846fdd6e691be734369b27e2b688ef3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S0039-9140(99)00318-5$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3536,27903,27904,45974</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=1272125$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/18967881$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Liang, Qi</creatorcontrib><creatorcontrib>Jing, Hu</creatorcontrib><creatorcontrib>Gregoire, D.Conrad</creatorcontrib><title>Determination of trace elements in granites by inductively coupled plasma mass spectrometry</title><title>Talanta (Oxford)</title><addtitle>Talanta</addtitle><description>Proposed is a simple and reliable method for the dissolution of granite and the determination of 38 elements by inductively coupled plasma mass spectrometry. One hundred milligrams of sample are digested with 1 ml of HF and 0.5 ml of HNO
3 in screw top PTFE-lined stainless steel bombs at 190°C for 12 h. Insoluble residues are dissolved using 8 ml of 40% HNO
3 (v/v) heated to 110°C for 3 h. Six granite standard reference materials (GSR-1, JG-2, G-2, NIM-G, SG-3, SG-1a) were studied. Analytical calibration was accomplished using aqueous standard solutions. Rhodium was used as an internal standard to correct for matrix effects and instrument drift. We report data for: Li, Be, Sc, V, Cr, Co, Ni, Cu, Zn, Ga, Rb, Sr, Y, Zr, Nb, Mo, Cs, Ba, Hf, Ta, W, Pb, Th, U and 14 of the rare earth elements. The recoveries for most of these elements in granite ranged from 90 to 110%.</description><subject>Crystalline rocks</subject><subject>Earth sciences</subject><subject>Earth, ocean, space</subject><subject>Exact sciences and technology</subject><subject>Geochemistry</subject><subject>Geochemistry: general, methodology, regional studies</subject><subject>Granites</subject><subject>ICP mass spectrometry</subject><subject>Igneous and metamorphic rocks petrology, volcanic processes, magmas</subject><subject>Trace elements</subject><issn>0039-9140</issn><issn>1873-3573</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2000</creationdate><recordtype>article</recordtype><recordid>eNqFkMtrFTEUh4NY7LX6JyhZCNrF1DxmMslKpNoHFLqorlyETOZEUubVnEzh_vfm9l7ssqvDj_OdBx8hHzg744yrr3eMSVMZXrMvxpyWwHXVvCIbrltZyaaVr8nmP3JM3iLeM8aEZPINOebaqFZrviF_fkCGNMbJ5ThPdA40J-eBwgAjTBlpnOjf5KaYAWm3LbFffY6PMGypn9dlgJ4ug8PR0dEhUlzA5zSPkNP2HTkKbkB4f6gn5PfFz1_nV9XN7eX1-febyjfM5Cq0PnDeiUb0ijngvKlBOa1lcK60ZNfpWoW-V6AM76CVtVSmEy2ITmkNQZ6Qz_u9S5ofVsBsx4gehsFNMK9oWym10E0tCtnsSZ9mxATBLimOLm0tZ3an1T5ptTtn1hj7pNU2Ze7j4cLajdA_Tx08FuDTAXDo3RCKMR_xmROt4GK359seg6LjMUKy6CNMHvqYijfbz_GFT_4BzBqV3w</recordid><startdate>20000306</startdate><enddate>20000306</enddate><creator>Liang, Qi</creator><creator>Jing, Hu</creator><creator>Gregoire, D.Conrad</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20000306</creationdate><title>Determination of trace elements in granites by inductively coupled plasma mass spectrometry</title><author>Liang, Qi ; Jing, Hu ; Gregoire, D.Conrad</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c509t-f7cf11b252d60ae1154e6a883faa7cf3bb846fdd6e691be734369b27e2b688ef3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2000</creationdate><topic>Crystalline rocks</topic><topic>Earth sciences</topic><topic>Earth, ocean, space</topic><topic>Exact sciences and technology</topic><topic>Geochemistry</topic><topic>Geochemistry: general, methodology, regional studies</topic><topic>Granites</topic><topic>ICP mass spectrometry</topic><topic>Igneous and metamorphic rocks petrology, volcanic processes, magmas</topic><topic>Trace elements</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liang, Qi</creatorcontrib><creatorcontrib>Jing, Hu</creatorcontrib><creatorcontrib>Gregoire, D.Conrad</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Talanta (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liang, Qi</au><au>Jing, Hu</au><au>Gregoire, D.Conrad</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of trace elements in granites by inductively coupled plasma mass spectrometry</atitle><jtitle>Talanta (Oxford)</jtitle><addtitle>Talanta</addtitle><date>2000-03-06</date><risdate>2000</risdate><volume>51</volume><issue>3</issue><spage>507</spage><epage>513</epage><pages>507-513</pages><issn>0039-9140</issn><eissn>1873-3573</eissn><coden>TLNTA2</coden><abstract>Proposed is a simple and reliable method for the dissolution of granite and the determination of 38 elements by inductively coupled plasma mass spectrometry. One hundred milligrams of sample are digested with 1 ml of HF and 0.5 ml of HNO
3 in screw top PTFE-lined stainless steel bombs at 190°C for 12 h. Insoluble residues are dissolved using 8 ml of 40% HNO
3 (v/v) heated to 110°C for 3 h. Six granite standard reference materials (GSR-1, JG-2, G-2, NIM-G, SG-3, SG-1a) were studied. Analytical calibration was accomplished using aqueous standard solutions. Rhodium was used as an internal standard to correct for matrix effects and instrument drift. We report data for: Li, Be, Sc, V, Cr, Co, Ni, Cu, Zn, Ga, Rb, Sr, Y, Zr, Nb, Mo, Cs, Ba, Hf, Ta, W, Pb, Th, U and 14 of the rare earth elements. The recoveries for most of these elements in granite ranged from 90 to 110%.</abstract><cop>Amsterdam</cop><cop>Oxford</cop><pub>Elsevier B.V</pub><pmid>18967881</pmid><doi>10.1016/S0039-9140(99)00318-5</doi><tpages>7</tpages></addata></record> |
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subjects | Crystalline rocks Earth sciences Earth, ocean, space Exact sciences and technology Geochemistry Geochemistry: general, methodology, regional studies Granites ICP mass spectrometry Igneous and metamorphic rocks petrology, volcanic processes, magmas Trace elements |
title | Determination of trace elements in granites by inductively coupled plasma mass spectrometry |
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