FIA-AAS determination of salicylic acid by a solid-phase reactor of copper carbonate incorporated in polyester resin beads
The determination of salicylic acid was carried out by reaction of the drug with copper carbonate entrapped in a polymeric material in a solid-phase reactor; the released cupric ions were monitored by flame atomic absorption at 324.8 nm. The calibration graph is linear over the range 4.0–75 μg ml −1...
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Veröffentlicht in: | Talanta (Oxford) 1995-09, Vol.42 (9), p.1285-1289 |
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creator | Rivas, G.A. Calatayud, J.Martínez |
description | The determination of salicylic acid was carried out by reaction of the drug with copper carbonate entrapped in a polymeric material in a solid-phase reactor; the released cupric ions were monitored by flame atomic absorption at 324.8 nm. The calibration graph is linear over the range 4.0–75 μg ml
−1 of salicylic acid, with a relative standard deviation of less than 1.5% and a sample throughout of 257 h
−1. The influence of foreign compounds was studied and the method was applied to the determination of salicylic acid content in two different pharmaceutical formulations. |
doi_str_mv | 10.1016/0039-9140(95)01575-V |
format | Article |
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−1. The influence of foreign compounds was studied and the method was applied to the determination of salicylic acid content in two different pharmaceutical formulations.</description><identifier>ISSN: 0039-9140</identifier><identifier>EISSN: 1873-3573</identifier><identifier>DOI: 10.1016/0039-9140(95)01575-V</identifier><identifier>PMID: 18966356</identifier><identifier>CODEN: TLNTA2</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Analysis ; Biological and medical sciences ; Flow injection analysis ; General pharmacology ; Medical sciences ; Pharmaceutical analysis ; Pharmacology. Drug treatments ; Solid-phase reactor</subject><ispartof>Talanta (Oxford), 1995-09, Vol.42 (9), p.1285-1289</ispartof><rights>1995</rights><rights>1995 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c454t-d8933d28833fd410c8938adcddc76dec118f9e9d0c9f3e8c838ae8947991dbc93</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/0039-9140(95)01575-V$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=3681792$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/18966356$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Rivas, G.A.</creatorcontrib><creatorcontrib>Calatayud, J.Martínez</creatorcontrib><title>FIA-AAS determination of salicylic acid by a solid-phase reactor of copper carbonate incorporated in polyester resin beads</title><title>Talanta (Oxford)</title><addtitle>Talanta</addtitle><description>The determination of salicylic acid was carried out by reaction of the drug with copper carbonate entrapped in a polymeric material in a solid-phase reactor; the released cupric ions were monitored by flame atomic absorption at 324.8 nm. The calibration graph is linear over the range 4.0–75 μg ml
−1 of salicylic acid, with a relative standard deviation of less than 1.5% and a sample throughout of 257 h
−1. The influence of foreign compounds was studied and the method was applied to the determination of salicylic acid content in two different pharmaceutical formulations.</description><subject>Analysis</subject><subject>Biological and medical sciences</subject><subject>Flow injection analysis</subject><subject>General pharmacology</subject><subject>Medical sciences</subject><subject>Pharmaceutical analysis</subject><subject>Pharmacology. Drug treatments</subject><subject>Solid-phase reactor</subject><issn>0039-9140</issn><issn>1873-3573</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1995</creationdate><recordtype>article</recordtype><recordid>eNp9kEtrGzEURkVpSJzHPyhFi0KTxaSSNQ9pUzAhTgKGLNJkKzT33qEq49FUGhecX185NumuCyF96NwHh7FPUlxLIetvQihTGFmKS1NdCVk1VfHygc2kblShqkZ9ZLN35ISdpvRLCDFXQh2zE6lNXauqnrHX5cOiWCyeONJEce0HN_kw8NDx5HoP23y4A4-83XLHU-g9FuNPl4hHcjCFuEMhjCNFDi62ITcg7gcIcQwxvzEHPoZ-SykPyFUp55YcpnN21Lk-0cXhPmPPy9sfN_fF6vHu4WaxKqCsyqlAbZTCudZKdVhKATlrh4AITY0EUurOkEEBplOkQedf0qZsjJHYglFn7Ou-7xjD701ew659Aup7N1DYJNsopedNKepMlnsSYkgpUmfH6Ncubq0Udifd7ozanVFrKvsm3b7kss-HAZt2Tfiv6GA5A18OgEvg-i66AXx651StZWPmGfu-xyjb-OMp2gSeBiD0kWCyGPz_F_kLeG6fSA</recordid><startdate>19950901</startdate><enddate>19950901</enddate><creator>Rivas, G.A.</creator><creator>Calatayud, J.Martínez</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>19950901</creationdate><title>FIA-AAS determination of salicylic acid by a solid-phase reactor of copper carbonate incorporated in polyester resin beads</title><author>Rivas, G.A. ; Calatayud, J.Martínez</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c454t-d8933d28833fd410c8938adcddc76dec118f9e9d0c9f3e8c838ae8947991dbc93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1995</creationdate><topic>Analysis</topic><topic>Biological and medical sciences</topic><topic>Flow injection analysis</topic><topic>General pharmacology</topic><topic>Medical sciences</topic><topic>Pharmaceutical analysis</topic><topic>Pharmacology. Drug treatments</topic><topic>Solid-phase reactor</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Rivas, G.A.</creatorcontrib><creatorcontrib>Calatayud, J.Martínez</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Talanta (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Rivas, G.A.</au><au>Calatayud, J.Martínez</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>FIA-AAS determination of salicylic acid by a solid-phase reactor of copper carbonate incorporated in polyester resin beads</atitle><jtitle>Talanta (Oxford)</jtitle><addtitle>Talanta</addtitle><date>1995-09-01</date><risdate>1995</risdate><volume>42</volume><issue>9</issue><spage>1285</spage><epage>1289</epage><pages>1285-1289</pages><issn>0039-9140</issn><eissn>1873-3573</eissn><coden>TLNTA2</coden><abstract>The determination of salicylic acid was carried out by reaction of the drug with copper carbonate entrapped in a polymeric material in a solid-phase reactor; the released cupric ions were monitored by flame atomic absorption at 324.8 nm. The calibration graph is linear over the range 4.0–75 μg ml
−1 of salicylic acid, with a relative standard deviation of less than 1.5% and a sample throughout of 257 h
−1. The influence of foreign compounds was studied and the method was applied to the determination of salicylic acid content in two different pharmaceutical formulations.</abstract><cop>Amsterdam</cop><cop>Oxford</cop><pub>Elsevier B.V</pub><pmid>18966356</pmid><doi>10.1016/0039-9140(95)01575-V</doi><tpages>5</tpages></addata></record> |
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subjects | Analysis Biological and medical sciences Flow injection analysis General pharmacology Medical sciences Pharmaceutical analysis Pharmacology. Drug treatments Solid-phase reactor |
title | FIA-AAS determination of salicylic acid by a solid-phase reactor of copper carbonate incorporated in polyester resin beads |
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