Comparison of the Volatile Constituents of Elsholtzia fruiticosa Extracted by Hydrodistillation, Supercritical Fluid Extraction and Head Space Analysis

Volatile constituents of Elsholtzia fruiticosa (D. Don) Rehder were studied by two different extraction techniques, supercritical fluid extraction (SFE) and hydrodistillation (HD), and the results were compared with head space analysis (HS). Thirty-five constituents were identified in both the SFE a...

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Veröffentlicht in:Natural product communications 2010-04, Vol.5 (4), p.641-644
Hauptverfasser: Saini, Rikki, Guleria, Shailja, Kaul, Vijay K., Lal, Brij, Babu, Garikapati D. Kiran, Singh, Bikram
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container_title Natural product communications
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Guleria, Shailja
Kaul, Vijay K.
Lal, Brij
Babu, Garikapati D. Kiran
Singh, Bikram
description Volatile constituents of Elsholtzia fruiticosa (D. Don) Rehder were studied by two different extraction techniques, supercritical fluid extraction (SFE) and hydrodistillation (HD), and the results were compared with head space analysis (HS). Thirty-five constituents were identified in both the SFE and HD oils and fourteen in the HS, accounting for 94.2%, 97.7% and 96.9% of the total identifications, respectively. A distinctive feature of the results was the very high content of non-terpenes (59.8%) in the HS, the high content of oxygenated monoterpenes (41.1%) in the HD oil and the high content of sesquiterpene hydrocarbons (21.8%) in the SFE oil. Monoterpene hydrocarbons were represented in HS (13.6%), HD (19.4%) and SFE (4.3%). In SFE sesquiterpene hydrocarbons formed 21.8% of the total, as compared to 6.6% in the HD and 1.1% in the HS Oxygenated sesquiterpenes represented 3.0% in SFE, 0.8% in HD and were absent in HS. Diterpenes were only present in the SFE oil (3.4%). Non-terpenes were represented by 24.5% in the SFE oil and 29.8% in the HD oil.
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subjects Chromatography, Supercritical Fluid - methods
Distillation - methods
Gas Chromatography-Mass Spectrometry
Lamiaceae - chemistry
Monoterpenes - analysis
Oils, Volatile - chemistry
Oils, Volatile - isolation & purification
Plant Leaves - chemistry
Plant Oils - chemistry
Plant Oils - isolation & purification
title Comparison of the Volatile Constituents of Elsholtzia fruiticosa Extracted by Hydrodistillation, Supercritical Fluid Extraction and Head Space Analysis
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