New Convenient Dissolution of Iron-Rhodium Alloys Using Hydrochloric Acid Containing a Small Amount of Nitric Acid without Heating for an ICP-AES Analysis
A new convenient dissolution method for Fe-Rh alloys has been developed. Aqua regia has been used for the dissolution of rhodium alloy samples. However, it is difficult to dissolve high-concentration rhodium (more than 50 mass%) in aqua regia, because a rhodium-passivity on the alloys surface occurs...
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| Veröffentlicht in: | Analytical Sciences 2001, Vol.17(8), pp.1011-1013 |
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| container_title | Analytical Sciences |
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| creator | DANZAKI, Yuetsu ASHINO, Tetsuya |
| description | A new convenient dissolution method for Fe-Rh alloys has been developed. Aqua regia has been used for the dissolution of rhodium alloy samples. However, it is difficult to dissolve high-concentration rhodium (more than 50 mass%) in aqua regia, because a rhodium-passivity on the alloys surface occurs with nitric acid. By using hydrochloric acid containing a small volume of nitric acid, Fe-Rh (24 - 64 mass%) alloys could be completely decomposed and dissolved under mild experimental conditions. The principal advantages of this method are simplicity and time-saving compared with other dissolution methods. |
| doi_str_mv | 10.2116/analsci.17.1011 |
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Aqua regia has been used for the dissolution of rhodium alloy samples. However, it is difficult to dissolve high-concentration rhodium (more than 50 mass%) in aqua regia, because a rhodium-passivity on the alloys surface occurs with nitric acid. By using hydrochloric acid containing a small volume of nitric acid, Fe-Rh (24 - 64 mass%) alloys could be completely decomposed and dissolved under mild experimental conditions. The principal advantages of this method are simplicity and time-saving compared with other dissolution methods.</description><identifier>ISSN: 0910-6340</identifier><identifier>EISSN: 1348-2246</identifier><identifier>DOI: 10.2116/analsci.17.1011</identifier><identifier>PMID: 11708088</identifier><identifier>CODEN: ANSCEN</identifier><language>eng</language><publisher>Tokyo: The Japan Society for Analytical Chemistry</publisher><subject>Alloys ; Analysing. Testing. 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Aqua regia has been used for the dissolution of rhodium alloy samples. However, it is difficult to dissolve high-concentration rhodium (more than 50 mass%) in aqua regia, because a rhodium-passivity on the alloys surface occurs with nitric acid. By using hydrochloric acid containing a small volume of nitric acid, Fe-Rh (24 - 64 mass%) alloys could be completely decomposed and dissolved under mild experimental conditions. The principal advantages of this method are simplicity and time-saving compared with other dissolution methods.</description><subject>Alloys</subject><subject>Analysing. Testing. Standards</subject><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Chemistry</subject><subject>Exact sciences and technology</subject><subject>Hydrochloric acid</subject><subject>Metals. Metallurgy</subject><subject>Nitric acid</subject><subject>Rhodium</subject><subject>Spectrometric and optical methods</subject><subject>Standardization and quality control</subject><issn>0910-6340</issn><issn>1348-2246</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2001</creationdate><recordtype>article</recordtype><recordid>eNpdkUFv2yAYhtG0aU27nXebkDb15hQwNuRopd0SqeqmdT0jjHFDhKEDvCp_Zb92WLGyahe-w_vwfvr0APABoyXBuL6STtqozBKzJUYYvwILXFJeEELr12CBVhgVdUnRGTiPcY8QJpyQt-AMY4Y44nwB_tzpZ7j27rd2RrsEr02M3o7JeAd9D7fBu-LHzndmHGBjrT9E-BCNe4SbQxe82lkfjIKNMt3UkqRxUyjh_SCthc3gx1yai-5MOoHPJu38mOBGyzTRvQ9QOrhdfy-am3vY5JsO0cR34E2fr9Pv53kBHr7c_FxvittvX7fr5rZQNWWp4GWvWFVRiRirqVY1acu-1bjrZYspypNz1bUVWpGKVTVaKSRbShFDOCdtV16Ay2PvU_C_Rh2TGExU2lrptB-jYIQwTmuSwU__gXs_hsmAwJTyqqwooZm6OlIq-BiD7sVTMIMMB4GRmKSJWZrATEzS8o-Pc-_YDrr7x8-WMvB5BmRU0vZBOmXiCy77phN2fcT2MclHfcplSEZZ_XIvn5-8_hSrnQxCu_IvN-C5vA</recordid><startdate>2001</startdate><enddate>2001</enddate><creator>DANZAKI, Yuetsu</creator><creator>ASHINO, Tetsuya</creator><general>The Japan Society for Analytical Chemistry</general><general>Japan Society for Analytical Chemistry</general><general>Japan Science and Technology Agency</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SE</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>H8G</scope><scope>JG9</scope><scope>L7M</scope><scope>P64</scope><scope>7X8</scope></search><sort><creationdate>2001</creationdate><title>New Convenient Dissolution of Iron-Rhodium Alloys Using Hydrochloric Acid Containing a Small Amount of Nitric Acid without Heating for an ICP-AES Analysis</title><author>DANZAKI, Yuetsu ; ASHINO, Tetsuya</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c647t-83fc7554a07764ec62b3fbe1dfab1401df88cdb5092575609c0ab440701f88bd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2001</creationdate><topic>Alloys</topic><topic>Analysing. Testing. Standards</topic><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Chemistry</topic><topic>Exact sciences and technology</topic><topic>Hydrochloric acid</topic><topic>Metals. Metallurgy</topic><topic>Nitric acid</topic><topic>Rhodium</topic><topic>Spectrometric and optical methods</topic><topic>Standardization and quality control</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>DANZAKI, Yuetsu</creatorcontrib><creatorcontrib>ASHINO, Tetsuya</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Biotechnology Research Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Analytical Sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>DANZAKI, Yuetsu</au><au>ASHINO, Tetsuya</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>New Convenient Dissolution of Iron-Rhodium Alloys Using Hydrochloric Acid Containing a Small Amount of Nitric Acid without Heating for an ICP-AES Analysis</atitle><jtitle>Analytical Sciences</jtitle><addtitle>Anal Sci</addtitle><date>2001</date><risdate>2001</risdate><volume>17</volume><issue>8</issue><spage>1011</spage><epage>1013</epage><pages>1011-1013</pages><issn>0910-6340</issn><eissn>1348-2246</eissn><coden>ANSCEN</coden><abstract>A new convenient dissolution method for Fe-Rh alloys has been developed. Aqua regia has been used for the dissolution of rhodium alloy samples. However, it is difficult to dissolve high-concentration rhodium (more than 50 mass%) in aqua regia, because a rhodium-passivity on the alloys surface occurs with nitric acid. By using hydrochloric acid containing a small volume of nitric acid, Fe-Rh (24 - 64 mass%) alloys could be completely decomposed and dissolved under mild experimental conditions. The principal advantages of this method are simplicity and time-saving compared with other dissolution methods.</abstract><cop>Tokyo</cop><pub>The Japan Society for Analytical Chemistry</pub><pmid>11708088</pmid><doi>10.2116/analsci.17.1011</doi><tpages>3</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | Analytical Sciences, 2001, Vol.17(8), pp.1011-1013 |
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| language | eng |
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| source | Springer Nature - Complete Springer Journals; J-STAGE (Japan Science & Technology Information Aggregator, Electronic) Freely Available Titles - Japanese; Open Access Titles of Japan; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; Free Full-Text Journals in Chemistry |
| subjects | Alloys Analysing. Testing. Standards Analytical chemistry Applied sciences Chemistry Exact sciences and technology Hydrochloric acid Metals. Metallurgy Nitric acid Rhodium Spectrometric and optical methods Standardization and quality control |
| title | New Convenient Dissolution of Iron-Rhodium Alloys Using Hydrochloric Acid Containing a Small Amount of Nitric Acid without Heating for an ICP-AES Analysis |
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