Solvothermal synthesis of silver nanoparticles from thiolates
A new solvothermal method for the synthesis of thiol-protected silver nanoparticles starting from silver thiolates is reported. The method has been tried with thiols of different chain length, such as octane and octadecane thiols, and the particle size was found to be nearly the same for both molecu...
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| Veröffentlicht in: | Journal of colloid and interface science 2003-12, Vol.268 (1), p.81-84 |
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| container_end_page | 84 |
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| container_title | Journal of colloid and interface science |
| container_volume | 268 |
| creator | Rosemary, M.J. Pradeep, T. |
| description | A new solvothermal method for the synthesis of thiol-protected silver nanoparticles starting from silver thiolates is reported. The method has been tried with thiols of different chain length, such as octane and octadecane thiols, and the particle size was found to be nearly the same for both molecules. The synthesis was dependent on heating conditions and the best results were obtained when the temperature was between 180 and 200
°C. Addition of complexation agents such as acetyl acetone or triethylamine to the solvent did not change the product distribution significantly. |
| doi_str_mv | 10.1016/j.jcis.2003.08.009 |
| format | Article |
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| ispartof | Journal of colloid and interface science, 2003-12, Vol.268 (1), p.81-84 |
| issn | 0021-9797 1095-7103 |
| language | eng |
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| subjects | Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry Physical and chemical studies. Granulometry. Electrokinetic phenomena Solvothermal Thiol-protected nanoparticles Thiolates |
| title | Solvothermal synthesis of silver nanoparticles from thiolates |
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