Synthesis of thiophenyl substituted cyclohexa-2,4-dien-1-one and its photocleavage coupling reaction with amines

Thiophenyl substituted cyclohexa-2,4-dien-1-ones were synthesized and photolyzed in the presence of various amines to afford the amides containing diene moeties via the ketene intermediate under visible light irradiation at 38 °C.

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Bibliographische Detailangaben
Veröffentlicht in:	Bioorganic & medicinal chemistry letters 2000-07, Vol.10 (14), p.1551-1553
Hauptverfasser:	Kwon, Tae Woo, Kim, Young Mee, Song, Suk Jin, Kwon, Yong Uk, Chung, Sung Kee
Format:	Artikel
Sprache:	eng
Schlagworte:	Amides - chemistry Amines - chemistry Chemistry Cyclohexanones - chemical synthesis Cyclohexanones - chemistry Exact sciences and technology General and physical chemistry Indicators and Reagents Light Molecular Structure Photochemistry Photolysis Physical chemistry of induced reactions (with radiations, particles and ultrasonics) Structure-Activity Relationship Sulfides - chemical synthesis Sulfides - chemistry
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Beschreibung
Zusammenfassung:	Thiophenyl substituted cyclohexa-2,4-dien-1-ones were synthesized and photolyzed in the presence of various amines to afford the amides containing diene moeties via the ketene intermediate under visible light irradiation at 38 °C.
ISSN:	0960-894X 1464-3405
DOI:	10.1016/S0960-894X(00)00291-2