Assessment of the retention properties of poly(vinyl alcohol) stationary phase for lipid class profiling in liquid chromatography
Potentialities of polymerized vinyl alcohol on silica gel were assessed for class separation of simple lipids, sphingolipids, glyceroglycolipids and phospholipids by high-performance liquid chromatography. A screening of pure solvents in binary gradient elution and a chemometric approach was used to...
Gespeichert in:
| Veröffentlicht in: | Journal of Chromatography A 2001-09, Vol.928 (2), p.127-137 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 137 |
|---|---|
| container_issue | 2 |
| container_start_page | 127 |
| container_title | Journal of Chromatography A |
| container_volume | 928 |
| creator | Deschamps, Frantz S. Chaminade, Pierre Ferrier, Danielle Baillet, Arlette |
| description | Potentialities of polymerized vinyl alcohol on silica gel were assessed for class separation of simple lipids, sphingolipids, glyceroglycolipids and phospholipids by high-performance liquid chromatography. A screening of pure solvents in binary gradient elution and a chemometric approach was used to define a rugged two segment linear gradient formed from four solvents for total lipid class separation. Triethylamine and formic acid were added in all mobile phase components for acidic phospholipid separation and evaporative light scattering response enhancement. Simple analytical procedures are described for the analysis of complex lipid materials. |
| doi_str_mv | 10.1016/S0021-9673(01)01137-2 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_71225888</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0021967301011372</els_id><sourcerecordid>71225888</sourcerecordid><originalsourceid>FETCH-LOGICAL-c390t-ffb840751994814e01233f9a87a6f9fd82c301fad82961312eb8fdcc60efc0773</originalsourceid><addsrcrecordid>eNqFkE1v1DAQhn0A0VL4CSAfEGoPKR57N05OqKqAVqrUQ-FseZ1xY-TEqSdbaY_95zjdFeXGyR_vM-Pxw9gHEOcgoP5yJ4SEqq21OhVwJgCUruQrdvz3-oi9JfotBGih5Rt2BLButFLimD1dECHRgOPMk-dzjzzjXE4hjXzKacI8B6Qlm1LcnT6GcRe5jS71KZ5xmu1C2rzjU28JuU-ZxzCFjrtoiZYWPsQw3vMwluBhuyR9ToOd0322U797x157GwnfH9YT9uv7t5-XV9XN7Y_ry4ubyqlWzJX3m2Yl9BradtXACgVIpXxrG21r3_qukU4J8LZs2hoUSNw0vnOuFuid0FqdsM_7vmWkhy3SbIZADmO0I6YtGQ1SrpumKeB6D7qciDJ6M-UwlC8aEGbxbZ59m0WsEWCefRtZ6j4eHthuBuxeqg6yC_DpAFhyNvpsRxfoH06BXtUF-7rHsNh4DJgNuYCjwy5kdLPpUvjPJH8AqEChIQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>71225888</pqid></control><display><type>article</type><title>Assessment of the retention properties of poly(vinyl alcohol) stationary phase for lipid class profiling in liquid chromatography</title><source>MEDLINE</source><source>Elsevier ScienceDirect Journals</source><creator>Deschamps, Frantz S. ; Chaminade, Pierre ; Ferrier, Danielle ; Baillet, Arlette</creator><creatorcontrib>Deschamps, Frantz S. ; Chaminade, Pierre ; Ferrier, Danielle ; Baillet, Arlette</creatorcontrib><description>Potentialities of polymerized vinyl alcohol on silica gel were assessed for class separation of simple lipids, sphingolipids, glyceroglycolipids and phospholipids by high-performance liquid chromatography. A screening of pure solvents in binary gradient elution and a chemometric approach was used to define a rugged two segment linear gradient formed from four solvents for total lipid class separation. Triethylamine and formic acid were added in all mobile phase components for acidic phospholipid separation and evaporative light scattering response enhancement. Simple analytical procedures are described for the analysis of complex lipid materials.</description><identifier>ISSN: 0021-9673</identifier><identifier>DOI: 10.1016/S0021-9673(01)01137-2</identifier><identifier>PMID: 11587330</identifier><identifier>CODEN: JOCRAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Analytical chemistry ; Analytical, structural and metabolic biochemistry ; Biological and medical sciences ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Chromatography, High Pressure Liquid - methods ; Exact sciences and technology ; Fundamental and applied biological sciences. Psychology ; Light ; Lipids ; Lipids - isolation & purification ; Miscellaneous ; Other biological molecules ; Other chromatographic methods ; Poly(vinyl alcohol) ; Polyvinyl Alcohol - chemistry ; Scattering, Radiation</subject><ispartof>Journal of Chromatography A, 2001-09, Vol.928 (2), p.127-137</ispartof><rights>2001 Elsevier Science B.V.</rights><rights>2001 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-ffb840751994814e01233f9a87a6f9fd82c301fad82961312eb8fdcc60efc0773</citedby><cites>FETCH-LOGICAL-c390t-ffb840751994814e01233f9a87a6f9fd82c301fad82961312eb8fdcc60efc0773</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0021967301011372$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3536,27903,27904,65309</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=1131746$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/11587330$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Deschamps, Frantz S.</creatorcontrib><creatorcontrib>Chaminade, Pierre</creatorcontrib><creatorcontrib>Ferrier, Danielle</creatorcontrib><creatorcontrib>Baillet, Arlette</creatorcontrib><title>Assessment of the retention properties of poly(vinyl alcohol) stationary phase for lipid class profiling in liquid chromatography</title><title>Journal of Chromatography A</title><addtitle>J Chromatogr A</addtitle><description>Potentialities of polymerized vinyl alcohol on silica gel were assessed for class separation of simple lipids, sphingolipids, glyceroglycolipids and phospholipids by high-performance liquid chromatography. A screening of pure solvents in binary gradient elution and a chemometric approach was used to define a rugged two segment linear gradient formed from four solvents for total lipid class separation. Triethylamine and formic acid were added in all mobile phase components for acidic phospholipid separation and evaporative light scattering response enhancement. Simple analytical procedures are described for the analysis of complex lipid materials.</description><subject>Analytical chemistry</subject><subject>Analytical, structural and metabolic biochemistry</subject><subject>Biological and medical sciences</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Chromatography, High Pressure Liquid - methods</subject><subject>Exact sciences and technology</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Light</subject><subject>Lipids</subject><subject>Lipids - isolation & purification</subject><subject>Miscellaneous</subject><subject>Other biological molecules</subject><subject>Other chromatographic methods</subject><subject>Poly(vinyl alcohol)</subject><subject>Polyvinyl Alcohol - chemistry</subject><subject>Scattering, Radiation</subject><issn>0021-9673</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2001</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkE1v1DAQhn0A0VL4CSAfEGoPKR57N05OqKqAVqrUQ-FseZ1xY-TEqSdbaY_95zjdFeXGyR_vM-Pxw9gHEOcgoP5yJ4SEqq21OhVwJgCUruQrdvz3-oi9JfotBGih5Rt2BLButFLimD1dECHRgOPMk-dzjzzjXE4hjXzKacI8B6Qlm1LcnT6GcRe5jS71KZ5xmu1C2rzjU28JuU-ZxzCFjrtoiZYWPsQw3vMwluBhuyR9ToOd0322U797x157GwnfH9YT9uv7t5-XV9XN7Y_ry4ubyqlWzJX3m2Yl9BradtXACgVIpXxrG21r3_qukU4J8LZs2hoUSNw0vnOuFuid0FqdsM_7vmWkhy3SbIZADmO0I6YtGQ1SrpumKeB6D7qciDJ6M-UwlC8aEGbxbZ59m0WsEWCefRtZ6j4eHthuBuxeqg6yC_DpAFhyNvpsRxfoH06BXtUF-7rHsNh4DJgNuYCjwy5kdLPpUvjPJH8AqEChIQ</recordid><startdate>20010914</startdate><enddate>20010914</enddate><creator>Deschamps, Frantz S.</creator><creator>Chaminade, Pierre</creator><creator>Ferrier, Danielle</creator><creator>Baillet, Arlette</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20010914</creationdate><title>Assessment of the retention properties of poly(vinyl alcohol) stationary phase for lipid class profiling in liquid chromatography</title><author>Deschamps, Frantz S. ; Chaminade, Pierre ; Ferrier, Danielle ; Baillet, Arlette</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-ffb840751994814e01233f9a87a6f9fd82c301fad82961312eb8fdcc60efc0773</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2001</creationdate><topic>Analytical chemistry</topic><topic>Analytical, structural and metabolic biochemistry</topic><topic>Biological and medical sciences</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Chromatography, High Pressure Liquid - methods</topic><topic>Exact sciences and technology</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Light</topic><topic>Lipids</topic><topic>Lipids - isolation & purification</topic><topic>Miscellaneous</topic><topic>Other biological molecules</topic><topic>Other chromatographic methods</topic><topic>Poly(vinyl alcohol)</topic><topic>Polyvinyl Alcohol - chemistry</topic><topic>Scattering, Radiation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Deschamps, Frantz S.</creatorcontrib><creatorcontrib>Chaminade, Pierre</creatorcontrib><creatorcontrib>Ferrier, Danielle</creatorcontrib><creatorcontrib>Baillet, Arlette</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Deschamps, Frantz S.</au><au>Chaminade, Pierre</au><au>Ferrier, Danielle</au><au>Baillet, Arlette</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Assessment of the retention properties of poly(vinyl alcohol) stationary phase for lipid class profiling in liquid chromatography</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>2001-09-14</date><risdate>2001</risdate><volume>928</volume><issue>2</issue><spage>127</spage><epage>137</epage><pages>127-137</pages><issn>0021-9673</issn><coden>JOCRAM</coden><abstract>Potentialities of polymerized vinyl alcohol on silica gel were assessed for class separation of simple lipids, sphingolipids, glyceroglycolipids and phospholipids by high-performance liquid chromatography. A screening of pure solvents in binary gradient elution and a chemometric approach was used to define a rugged two segment linear gradient formed from four solvents for total lipid class separation. Triethylamine and formic acid were added in all mobile phase components for acidic phospholipid separation and evaporative light scattering response enhancement. Simple analytical procedures are described for the analysis of complex lipid materials.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>11587330</pmid><doi>10.1016/S0021-9673(01)01137-2</doi><tpages>11</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0021-9673 |
| ispartof | Journal of Chromatography A, 2001-09, Vol.928 (2), p.127-137 |
| issn | 0021-9673 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_71225888 |
| source | MEDLINE; Elsevier ScienceDirect Journals |
| subjects | Analytical chemistry Analytical, structural and metabolic biochemistry Biological and medical sciences Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, High Pressure Liquid - methods Exact sciences and technology Fundamental and applied biological sciences. Psychology Light Lipids Lipids - isolation & purification Miscellaneous Other biological molecules Other chromatographic methods Poly(vinyl alcohol) Polyvinyl Alcohol - chemistry Scattering, Radiation |
| title | Assessment of the retention properties of poly(vinyl alcohol) stationary phase for lipid class profiling in liquid chromatography |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-25T20%3A08%3A46IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Assessment%20of%20the%20retention%20properties%20of%20poly(vinyl%20alcohol)%20stationary%20phase%20for%20lipid%20class%20profiling%20in%20liquid%20chromatography&rft.jtitle=Journal%20of%20Chromatography%20A&rft.au=Deschamps,%20Frantz%20S.&rft.date=2001-09-14&rft.volume=928&rft.issue=2&rft.spage=127&rft.epage=137&rft.pages=127-137&rft.issn=0021-9673&rft.coden=JOCRAM&rft_id=info:doi/10.1016/S0021-9673(01)01137-2&rft_dat=%3Cproquest_cross%3E71225888%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=71225888&rft_id=info:pmid/11587330&rft_els_id=S0021967301011372&rfr_iscdi=true |