Rheological properties of PMMA bone cements during curing
The rheological behaviour of poly(methyl methacrylate) bone cements has been characterised during the curing phase using an oscillating parallel plate rheometer. Viscosity has been measured as a function of time for a range of commercial cements showing different viscosity–time profiles. Measurement...
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Veröffentlicht in: | Biomaterials 2001-11, Vol.22 (22), p.3005-3013 |
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description | The rheological behaviour of poly(methyl methacrylate) bone cements has been characterised during the curing phase using an oscillating parallel plate rheometer. Viscosity has been measured as a function of time for a range of commercial cements showing different viscosity–time profiles. Measurements have been made over a range of temperatures from 19–25°C, and the results show a strong dependence of rate of viscosity rise on temperature. Viscoelastic parameters, such as storage modulus, loss modulus and phase angle have been obtained and show the change from primarily viscous to elastic behaviour as the cements set. It is suggested that these parameters more completely describe the rheological behaviour of bone cements than viscosity alone and may provide a better measure of handling and setting characteristics. |
doi_str_mv | 10.1016/S0142-9612(01)00047-3 |
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Viscosity has been measured as a function of time for a range of commercial cements showing different viscosity–time profiles. Measurements have been made over a range of temperatures from 19–25°C, and the results show a strong dependence of rate of viscosity rise on temperature. Viscoelastic parameters, such as storage modulus, loss modulus and phase angle have been obtained and show the change from primarily viscous to elastic behaviour as the cements set. It is suggested that these parameters more completely describe the rheological behaviour of bone cements than viscosity alone and may provide a better measure of handling and setting characteristics.</description><identifier>ISSN: 0142-9612</identifier><identifier>EISSN: 1878-5905</identifier><identifier>DOI: 10.1016/S0142-9612(01)00047-3</identifier><identifier>PMID: 11575475</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Biological and medical sciences ; Bone cement ; Bone Cements - chemistry ; Curing ; Elasticity ; Humans ; In Vitro Techniques ; Materials Testing ; Medical sciences ; Poly(methyl methacrylate) ; Polymethyl Methacrylate - chemistry ; Polymethyl methacrylates ; Rheology ; Rheometers ; Setting ; Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases ; Technology. Biomaterials. 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Viscosity has been measured as a function of time for a range of commercial cements showing different viscosity–time profiles. Measurements have been made over a range of temperatures from 19–25°C, and the results show a strong dependence of rate of viscosity rise on temperature. Viscoelastic parameters, such as storage modulus, loss modulus and phase angle have been obtained and show the change from primarily viscous to elastic behaviour as the cements set. It is suggested that these parameters more completely describe the rheological behaviour of bone cements than viscosity alone and may provide a better measure of handling and setting characteristics.</description><subject>Biological and medical sciences</subject><subject>Bone cement</subject><subject>Bone Cements - chemistry</subject><subject>Curing</subject><subject>Elasticity</subject><subject>Humans</subject><subject>In Vitro Techniques</subject><subject>Materials Testing</subject><subject>Medical sciences</subject><subject>Poly(methyl methacrylate)</subject><subject>Polymethyl Methacrylate - chemistry</subject><subject>Polymethyl methacrylates</subject><subject>Rheology</subject><subject>Rheometers</subject><subject>Setting</subject><subject>Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases</subject><subject>Technology. Biomaterials. Equipments</subject><subject>Temperature</subject><subject>Thermal effects</subject><subject>Time Factors</subject><subject>Viscosity</subject><subject>Viscosity measurement</subject><issn>0142-9612</issn><issn>1878-5905</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2001</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkU1P3DAQhq2qFSyUn9Aql1ZwCJ3xZ3yqECq0EggE3C2vM6aussnWzlbqvyf7ITjuxSNLz8y8876MfUI4R0D97RFQ8tpq5KeAZwAgTS3esRk2pqmVBfWezV6RQ3ZUyh-Y_iD5ATtEVEZJo2bMPvymoRueU_BdtczDkvKYqFRDrO5vby-q-dBTFWhB_ViqdpVT_1yFTfnIPkTfFTrZ1WP2dPXj6fJnfXN3_evy4qYOUomxjhwabKMyTbQxzIPWgoQ2aFuUinvrNY_cgvEkNUVPZpJmJCltgNugxTH7uh07ifu7ojK6RSqBus73NKyKM4hWotgPcm2FbKZnL4jSCAVrUG3BkIdSMkW3zGnh83-H4NYhuE0Ibu2wA3SbEJyY-j7vFqzmC2rfunauT8CXHeDL5HvMvg-pvHESDAe5Pun7lqPJ33-JsishUR-oTZnC6Noh7ZHyAr41oQY</recordid><startdate>20011101</startdate><enddate>20011101</enddate><creator>Farrar, D.F.</creator><creator>Rose, J.</creator><general>Elsevier Ltd</general><general>Elsevier Science</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>7X8</scope></search><sort><creationdate>20011101</creationdate><title>Rheological properties of PMMA bone cements during curing</title><author>Farrar, D.F. ; Rose, J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c453t-f2081df578f9fcbc663e36719d1452a9a62f2907ae46efae715774e567029c63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2001</creationdate><topic>Biological and medical sciences</topic><topic>Bone cement</topic><topic>Bone Cements - chemistry</topic><topic>Curing</topic><topic>Elasticity</topic><topic>Humans</topic><topic>In Vitro Techniques</topic><topic>Materials Testing</topic><topic>Medical sciences</topic><topic>Poly(methyl methacrylate)</topic><topic>Polymethyl Methacrylate - chemistry</topic><topic>Polymethyl methacrylates</topic><topic>Rheology</topic><topic>Rheometers</topic><topic>Setting</topic><topic>Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases</topic><topic>Technology. Biomaterials. Equipments</topic><topic>Temperature</topic><topic>Thermal effects</topic><topic>Time Factors</topic><topic>Viscosity</topic><topic>Viscosity measurement</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Farrar, D.F.</creatorcontrib><creatorcontrib>Rose, J.</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>MEDLINE - Academic</collection><jtitle>Biomaterials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Farrar, D.F.</au><au>Rose, J.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rheological properties of PMMA bone cements during curing</atitle><jtitle>Biomaterials</jtitle><addtitle>Biomaterials</addtitle><date>2001-11-01</date><risdate>2001</risdate><volume>22</volume><issue>22</issue><spage>3005</spage><epage>3013</epage><pages>3005-3013</pages><issn>0142-9612</issn><eissn>1878-5905</eissn><abstract>The rheological behaviour of poly(methyl methacrylate) bone cements has been characterised during the curing phase using an oscillating parallel plate rheometer. Viscosity has been measured as a function of time for a range of commercial cements showing different viscosity–time profiles. Measurements have been made over a range of temperatures from 19–25°C, and the results show a strong dependence of rate of viscosity rise on temperature. Viscoelastic parameters, such as storage modulus, loss modulus and phase angle have been obtained and show the change from primarily viscous to elastic behaviour as the cements set. It is suggested that these parameters more completely describe the rheological behaviour of bone cements than viscosity alone and may provide a better measure of handling and setting characteristics.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><pmid>11575475</pmid><doi>10.1016/S0142-9612(01)00047-3</doi><tpages>9</tpages></addata></record> |
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subjects | Biological and medical sciences Bone cement Bone Cements - chemistry Curing Elasticity Humans In Vitro Techniques Materials Testing Medical sciences Poly(methyl methacrylate) Polymethyl Methacrylate - chemistry Polymethyl methacrylates Rheology Rheometers Setting Surgery (general aspects). Transplantations, organ and tissue grafts. Graft diseases Technology. Biomaterials. Equipments Temperature Thermal effects Time Factors Viscosity Viscosity measurement |
title | Rheological properties of PMMA bone cements during curing |
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