Comparison of different derivatization approaches for mercury speciation in biological tissues by gas chromatography/inductively coupled plasma mass spectrometry

A novel interface design for coupling gas chromatography and inductively coupled plasma mass spectrometry (GC/ICP‐MS) was used to perform mercury speciation in biological tissues. Three derivatization approaches were optimized and compared for this purpose: anhydrous butylation using a Grignard reag...

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Veröffentlicht in:	Journal of mass spectrometry. 2000-05, Vol.35 (5), p.639-646
Hauptverfasser:	Garc a Fern ndez, Rub n, Montes Bay n, Mar a, Garc a Alonso, J. Ignacio, Sanz-Medel, Alfredo
Format:	Artikel
Sprache:	eng
Schlagworte:	Animals butylation Chromatography, Gas - methods ethylation gas chromatography inductively coupled plasma mass spectrometry Liver Mass Spectrometry - methods Mercury - analysis methylmercury propylation Sensitivity and Specificity
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