Electrochemical processes in a wire-in-a-capillary bulk-loaded, nano-electrospray emitter

Experiments are described that illustrate solvent oxidation, emitter electrode corrosion, and analyte oxidation in positive ion mode nano-electrospray mass spectrometry using a wire-in-a-capillary, bulk-loaded nano-electrospray emitter geometry. Time-lapsed color photography of pH and metal specific...

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Veröffentlicht in:	Journal of the American Society for Mass Spectrometry 2001-07, Vol.12 (7), p.853-862
Hauptverfasser:	Van Berkel, Gary J, Asano, Keiji G, Schnier, Paul D
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Chemical reactions Chemistry Color photography Electrospraying Emitters Exact sciences and technology Ions Mass spectra Mass spectrometry Oxidation Photography Positive ions Scientific imaging Spectrometric and optical methods Spectroscopy Time dependence Wire
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