Use of a Statistically Designed Experimental Approach to Optimize the Propylketal Derivatization of Barbiturates

The derivatization of barbiturates with dimethylformamide dipropylacetal and dimethylformamide diisopropylacetal is studied with respect to the optimization of reaction recovery and reliability. A second-order orthogonal experimental design is utilized in order to obtain regression equations for the...

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Veröffentlicht in:	Journal of chromatographic science 2001-04, Vol.39 (4), p.129-136
Hauptverfasser:	Kushnir, Mark M., Urry, Francis M.
Format:	Artikel
Sprache:	eng
Schlagworte:	Analysis Barbiturates - chemistry Biological and medical sciences Chromatography, Gas Dimethylformamide - analogs & derivatives Dimethylformamide - chemistry General pharmacology Medical sciences Pharmacology. Drug treatments Reference Standards Regression Analysis Reproducibility of Results
Online-Zugang:	Volltext
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