Highly sensitive analysis of methamphetamine and amphetamine in human whole blood using headspace solid-phase microextraction and gas chromatography–mass spectrometry

A simple and highly sensitive method for analysis of derivatized methamphetamine (MA) and amphetamine (AM) in whole blood was developed using headspace solid-phase microextraction (HS-SPME) and gas chromatography–mass spectrometry electron impact ionization selected ion monitoring (GC–MS-EI-SIM). A...

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Veröffentlicht in:	Forensic science international 2001-02, Vol.116 (1), p.15-22
Hauptverfasser:	Okajima, Kazuo, Namera, Akira, Yashiki, Mikio, Tsukue, Ichiro, Kojima, Tohru
Format:	Artikel
Sprache:	eng
Schlagworte:	Adsorption Alkalies - metabolism Amphetamine Amphetamine - blood Amphetamine - isolation & purification Amphetamine - metabolism Amphetamines Autopsies Autopsy Biological and medical sciences Blood Calibration Central Nervous System Stimulants - blood Central Nervous System Stimulants - isolation & purification Central Nervous System Stimulants - metabolism Deuteration Electron impact Equilibrium Forensic medicine Forensic Medicine - methods Gas chromatography Gas Chromatography-Mass Spectrometry - methods Headspace Heart Heart Ventricles Highly sensitive Hot Temperature HS-SPME Humans Ingestion Ionization Mass spectrometry Mass spectroscopy Medical sciences Methamphetamine Methamphetamine - blood Methamphetamine - isolation & purification Methamphetamine - metabolism Pentafluorobenzyl bromide Public health. Hygiene Public health. Hygiene-occupational medicine Reproducibility Reproducibility of Results Sensitivity and Specificity Solid phase methods Solid phases Temperature Time Factors Whole blood
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