Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work
The identification of organic colorants used in artistic paintings is an important information source for reconstructing the working techniques found in a particular work and for defining a programme for the restoration and conservation of the painting. In this work, sodium dodecyl sulfate (SDS) was...
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| Veröffentlicht in: | Journal of Chromatography A 2007-06, Vol.1154 (1), p.429-436 |
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| creator | Maguregui, M.I. Alonso, R.M. Barandiaran, M. Jimenez, R.M. García, N. |
| description | The identification of organic colorants used in artistic paintings is an important information source for reconstructing the working techniques found in a particular work and for defining a programme for the restoration and conservation of the painting. In this work, sodium dodecyl sulfate (SDS) was used as a surfactant in micellar electrokinetic chromatography (MEKC) for separating a broad range of red organic pigments, based on their colouring matters: madder (colouring matters: alizarin, quinizarin and purpurin), cochineal (colouring matter: carminic acid), red sandalwood (colouring matter: santalin), brazilwood (colouring matter: brazilin), lac dye (colouring matter: laccaic acid) and dragon's blood (colouring matter: dracorhodin). The running electrolyte used was 20
mM borax (pH 9), containing 20
mM SDS and 10% acetonitrile as organic modifier. Separation was carried out by applying a +20
kV voltage at the injection end, 25
°C and 214
nm/254
nm as detection wavelengths. All colorants were separated within less than 13
min with a good baseline resolution. The method was applied to the analysis of paint samples obtained from the Diocesan Museum of Holy Art of Bilbao. |
| doi_str_mv | 10.1016/j.chroma.2007.03.089 |
| format | Article |
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mM borax (pH 9), containing 20
mM SDS and 10% acetonitrile as organic modifier. Separation was carried out by applying a +20
kV voltage at the injection end, 25
°C and 214
nm/254
nm as detection wavelengths. All colorants were separated within less than 13
min with a good baseline resolution. The method was applied to the analysis of paint samples obtained from the Diocesan Museum of Holy Art of Bilbao.</description><identifier>ISSN: 0021-9673</identifier><identifier>DOI: 10.1016/j.chroma.2007.03.089</identifier><identifier>PMID: 17452040</identifier><identifier>CODEN: JOCRAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject><![CDATA[Analytical chemistry ; Applied sciences ; Artistic work ; Azo Compounds - isolation & purification ; Benzopyrans - isolation & purification ; Caesalpinia - chemistry ; Carmine - analogs & derivatives ; Carmine - isolation & purification ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Chromatography, Micellar Electrokinetic Capillary - methods ; Coatings. Paints, varnishes and inks ; Color ; Coloring Agents - analysis ; Coloring Agents - isolation & purification ; Exact sciences and technology ; Lake pigments ; Liquid–liquid extraction ; MEKC ; Natural red dyestuff ; Other chromatographic methods ; Pigments, Biological - analysis ; Plant Extracts - analysis ; Plant Extracts - isolation & purification ; Polymer industry, paints, wood ; Reproducibility of Results ; Rubia ; Santalum - chemistry ; Sodium Dodecyl Sulfate ; Uncertainty]]></subject><ispartof>Journal of Chromatography A, 2007-06, Vol.1154 (1), p.429-436</ispartof><rights>2007 Elsevier B.V.</rights><rights>2007 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-9fee8ff405a6a620f7eba67498e994df3aa1f0bac52f190b3f99c7eedae5a61d3</citedby><cites>FETCH-LOGICAL-c390t-9fee8ff405a6a620f7eba67498e994df3aa1f0bac52f190b3f99c7eedae5a61d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.chroma.2007.03.089$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>315,782,786,3552,27931,27932,46002</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18811169$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17452040$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Maguregui, M.I.</creatorcontrib><creatorcontrib>Alonso, R.M.</creatorcontrib><creatorcontrib>Barandiaran, M.</creatorcontrib><creatorcontrib>Jimenez, R.M.</creatorcontrib><creatorcontrib>García, N.</creatorcontrib><title>Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work</title><title>Journal of Chromatography A</title><addtitle>J Chromatogr A</addtitle><description>The identification of organic colorants used in artistic paintings is an important information source for reconstructing the working techniques found in a particular work and for defining a programme for the restoration and conservation of the painting. In this work, sodium dodecyl sulfate (SDS) was used as a surfactant in micellar electrokinetic chromatography (MEKC) for separating a broad range of red organic pigments, based on their colouring matters: madder (colouring matters: alizarin, quinizarin and purpurin), cochineal (colouring matter: carminic acid), red sandalwood (colouring matter: santalin), brazilwood (colouring matter: brazilin), lac dye (colouring matter: laccaic acid) and dragon's blood (colouring matter: dracorhodin). The running electrolyte used was 20
mM borax (pH 9), containing 20
mM SDS and 10% acetonitrile as organic modifier. Separation was carried out by applying a +20
kV voltage at the injection end, 25
°C and 214
nm/254
nm as detection wavelengths. All colorants were separated within less than 13
min with a good baseline resolution. The method was applied to the analysis of paint samples obtained from the Diocesan Museum of Holy Art of Bilbao.</description><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Artistic work</subject><subject>Azo Compounds - isolation & purification</subject><subject>Benzopyrans - isolation & purification</subject><subject>Caesalpinia - chemistry</subject><subject>Carmine - analogs & derivatives</subject><subject>Carmine - isolation & purification</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Chromatography, Micellar Electrokinetic Capillary - methods</subject><subject>Coatings. Paints, varnishes and inks</subject><subject>Color</subject><subject>Coloring Agents - analysis</subject><subject>Coloring Agents - isolation & purification</subject><subject>Exact sciences and technology</subject><subject>Lake pigments</subject><subject>Liquid–liquid extraction</subject><subject>MEKC</subject><subject>Natural red dyestuff</subject><subject>Other chromatographic methods</subject><subject>Pigments, Biological - analysis</subject><subject>Plant Extracts - analysis</subject><subject>Plant Extracts - isolation & purification</subject><subject>Polymer industry, paints, wood</subject><subject>Reproducibility of Results</subject><subject>Rubia</subject><subject>Santalum - chemistry</subject><subject>Sodium Dodecyl Sulfate</subject><subject>Uncertainty</subject><issn>0021-9673</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kU1v1DAQhnMA0VL6DxDyBW4bxkk2ji9IqOJLatULPVuz9rjr3cRebKdo_wC_Gy9ZqTdOI9nP-2r0TFW95VBz4P3HXa23MUxYNwCihraGQb6oLgEavpK9aC-q1yntALgA0byqLrjo1g10cFn9uXOaxhEjo5F0jmHvPGWn2VKYw2PEw_bIJsrbYJgNkeUtMUOZ4uQ8Zhc8C5YleqKIIysv82lGMswcKeXZWobesBH3xA7ucSKfE5tT-XeeYczsd4j7N9VLi2Oi6_O8qh6-fvl58311e__tx83n25VuJeSVtESDtR2ssce-AStog73o5EBSdsa2iNzCBvW6sVzCprVSakFkkEqCm_aq-rD0HmL4NZf11OTSPwGewpyUgHUvpGwK2C2gjiGlSFYdopswHhUHdXKudmpRpE7OFbSqOC-xd-f-eTOReQ6dhRfg_RnApHG0Eb126ZkbBs55fyr6tHBUbDw5iippR16TcbHcSZng_r_JX5psqBM</recordid><startdate>20070622</startdate><enddate>20070622</enddate><creator>Maguregui, M.I.</creator><creator>Alonso, R.M.</creator><creator>Barandiaran, M.</creator><creator>Jimenez, R.M.</creator><creator>García, N.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20070622</creationdate><title>Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work</title><author>Maguregui, M.I. ; Alonso, R.M. ; Barandiaran, M. ; Jimenez, R.M. ; García, N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-9fee8ff405a6a620f7eba67498e994df3aa1f0bac52f190b3f99c7eedae5a61d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Artistic work</topic><topic>Azo Compounds - isolation & purification</topic><topic>Benzopyrans - isolation & purification</topic><topic>Caesalpinia - chemistry</topic><topic>Carmine - analogs & derivatives</topic><topic>Carmine - isolation & purification</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Chromatography, Micellar Electrokinetic Capillary - methods</topic><topic>Coatings. Paints, varnishes and inks</topic><topic>Color</topic><topic>Coloring Agents - analysis</topic><topic>Coloring Agents - isolation & purification</topic><topic>Exact sciences and technology</topic><topic>Lake pigments</topic><topic>Liquid–liquid extraction</topic><topic>MEKC</topic><topic>Natural red dyestuff</topic><topic>Other chromatographic methods</topic><topic>Pigments, Biological - analysis</topic><topic>Plant Extracts - analysis</topic><topic>Plant Extracts - isolation & purification</topic><topic>Polymer industry, paints, wood</topic><topic>Reproducibility of Results</topic><topic>Rubia</topic><topic>Santalum - chemistry</topic><topic>Sodium Dodecyl Sulfate</topic><topic>Uncertainty</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Maguregui, M.I.</creatorcontrib><creatorcontrib>Alonso, R.M.</creatorcontrib><creatorcontrib>Barandiaran, M.</creatorcontrib><creatorcontrib>Jimenez, R.M.</creatorcontrib><creatorcontrib>García, N.</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maguregui, M.I.</au><au>Alonso, R.M.</au><au>Barandiaran, M.</au><au>Jimenez, R.M.</au><au>García, N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>2007-06-22</date><risdate>2007</risdate><volume>1154</volume><issue>1</issue><spage>429</spage><epage>436</epage><pages>429-436</pages><issn>0021-9673</issn><coden>JOCRAM</coden><abstract>The identification of organic colorants used in artistic paintings is an important information source for reconstructing the working techniques found in a particular work and for defining a programme for the restoration and conservation of the painting. In this work, sodium dodecyl sulfate (SDS) was used as a surfactant in micellar electrokinetic chromatography (MEKC) for separating a broad range of red organic pigments, based on their colouring matters: madder (colouring matters: alizarin, quinizarin and purpurin), cochineal (colouring matter: carminic acid), red sandalwood (colouring matter: santalin), brazilwood (colouring matter: brazilin), lac dye (colouring matter: laccaic acid) and dragon's blood (colouring matter: dracorhodin). The running electrolyte used was 20
mM borax (pH 9), containing 20
mM SDS and 10% acetonitrile as organic modifier. Separation was carried out by applying a +20
kV voltage at the injection end, 25
°C and 214
nm/254
nm as detection wavelengths. All colorants were separated within less than 13
min with a good baseline resolution. The method was applied to the analysis of paint samples obtained from the Diocesan Museum of Holy Art of Bilbao.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>17452040</pmid><doi>10.1016/j.chroma.2007.03.089</doi><tpages>8</tpages></addata></record> |
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| subjects | Analytical chemistry Applied sciences Artistic work Azo Compounds - isolation & purification Benzopyrans - isolation & purification Caesalpinia - chemistry Carmine - analogs & derivatives Carmine - isolation & purification Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Micellar Electrokinetic Capillary - methods Coatings. Paints, varnishes and inks Color Coloring Agents - analysis Coloring Agents - isolation & purification Exact sciences and technology Lake pigments Liquid–liquid extraction MEKC Natural red dyestuff Other chromatographic methods Pigments, Biological - analysis Plant Extracts - analysis Plant Extracts - isolation & purification Polymer industry, paints, wood Reproducibility of Results Rubia Santalum - chemistry Sodium Dodecyl Sulfate Uncertainty |
| title | Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work |
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