Determination of heavy metals by ICP-OES and F-AAS after preconcentration with 2,2′-bipyridyl and erythrosine
The applicability of 2,2′-bipyridyl and erythrosine co-precipitation method for the separation and preconcentration of some heavy metals, such as Cd, Co, Cu, Ni, Pb and Zn in actual samples for their determination by ICP-OES and F-AAS was studied. Experimental conditions influencing the recovery of...
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| Veröffentlicht in: | Journal of hazardous materials 2008-04, Vol.152 (3), p.1122-1129 |
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| creator | Feist, Barbara Mikula, Barbara Pytlakowska, Katarzyna Puzio, Bozena Buhl, Franciszek |
| description | The applicability of 2,2′-bipyridyl and erythrosine co-precipitation method for the separation and preconcentration of some heavy metals, such as Cd, Co, Cu, Ni, Pb and Zn in actual samples for their determination by ICP-OES and F-AAS was studied. Experimental conditions influencing the recovery of the investigated metals, such as pH, molar ratio of 2,2′-bipyridyl to erythrosine, the effect of time on co-precipitation were optimized. The analytical characteristics of the method (e.g. limit of detection, sensitivity, linear range and preconcentration factor) were obtained. The limits of detection LOD (ng
mL
−1) of the ICP-OES (F-AAS) method were: Cd: 4.0 (7.75), Co: 3.1 (57.2), Cu: 18 (10.3), Ni 21.3 (32.8), Pb: 35.9 (29.2) and Zn: 10.2 (6.90). The recovery of all the elements tested was more than 93%. The influence of inorganic matrix was examined. The proposed method was applied to determination of Cd, Co, Cu, Ni, Pb and Zn in vegetables and certified reference material (NCS ZC85006 Tomato). |
| doi_str_mv | 10.1016/j.jhazmat.2007.07.095 |
| format | Article |
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mL
−1) of the ICP-OES (F-AAS) method were: Cd: 4.0 (7.75), Co: 3.1 (57.2), Cu: 18 (10.3), Ni 21.3 (32.8), Pb: 35.9 (29.2) and Zn: 10.2 (6.90). The recovery of all the elements tested was more than 93%. The influence of inorganic matrix was examined. The proposed method was applied to determination of Cd, Co, Cu, Ni, Pb and Zn in vegetables and certified reference material (NCS ZC85006 Tomato).</description><identifier>ISSN: 0304-3894</identifier><identifier>EISSN: 1873-3336</identifier><identifier>DOI: 10.1016/j.jhazmat.2007.07.095</identifier><identifier>PMID: 17850961</identifier><identifier>CODEN: JHMAD9</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>2,2'-Dipyridyl - chemistry ; 2,2′-Bipyridyl ; Applied sciences ; Calibration ; Chemical Precipitation ; Co-precipitation ; Erythrosine ; Erythrosine - chemistry ; Exact sciences and technology ; F-AAS ; Heavy metals ; ICP-OES ; Lycopersicon esculentum ; Metals, Heavy - analysis ; Plant materials ; Pollution ; Reference Standards ; Reproducibility of Results ; Sensitivity and Specificity ; Spectrophotometry, Atomic - methods</subject><ispartof>Journal of hazardous materials, 2008-04, Vol.152 (3), p.1122-1129</ispartof><rights>2007 Elsevier B.V.</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c455t-cdfb2e4a9af670e46bccb930bd744a10491be7f9c06da87da24ae6043265b8823</citedby><cites>FETCH-LOGICAL-c455t-cdfb2e4a9af670e46bccb930bd744a10491be7f9c06da87da24ae6043265b8823</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0304389407011193$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27903,27904,65308</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20217449$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17850961$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Feist, Barbara</creatorcontrib><creatorcontrib>Mikula, Barbara</creatorcontrib><creatorcontrib>Pytlakowska, Katarzyna</creatorcontrib><creatorcontrib>Puzio, Bozena</creatorcontrib><creatorcontrib>Buhl, Franciszek</creatorcontrib><title>Determination of heavy metals by ICP-OES and F-AAS after preconcentration with 2,2′-bipyridyl and erythrosine</title><title>Journal of hazardous materials</title><addtitle>J Hazard Mater</addtitle><description>The applicability of 2,2′-bipyridyl and erythrosine co-precipitation method for the separation and preconcentration of some heavy metals, such as Cd, Co, Cu, Ni, Pb and Zn in actual samples for their determination by ICP-OES and F-AAS was studied. Experimental conditions influencing the recovery of the investigated metals, such as pH, molar ratio of 2,2′-bipyridyl to erythrosine, the effect of time on co-precipitation were optimized. The analytical characteristics of the method (e.g. limit of detection, sensitivity, linear range and preconcentration factor) were obtained. The limits of detection LOD (ng
mL
−1) of the ICP-OES (F-AAS) method were: Cd: 4.0 (7.75), Co: 3.1 (57.2), Cu: 18 (10.3), Ni 21.3 (32.8), Pb: 35.9 (29.2) and Zn: 10.2 (6.90). The recovery of all the elements tested was more than 93%. The influence of inorganic matrix was examined. The proposed method was applied to determination of Cd, Co, Cu, Ni, Pb and Zn in vegetables and certified reference material (NCS ZC85006 Tomato).</description><subject>2,2'-Dipyridyl - chemistry</subject><subject>2,2′-Bipyridyl</subject><subject>Applied sciences</subject><subject>Calibration</subject><subject>Chemical Precipitation</subject><subject>Co-precipitation</subject><subject>Erythrosine</subject><subject>Erythrosine - chemistry</subject><subject>Exact sciences and technology</subject><subject>F-AAS</subject><subject>Heavy metals</subject><subject>ICP-OES</subject><subject>Lycopersicon esculentum</subject><subject>Metals, Heavy - analysis</subject><subject>Plant materials</subject><subject>Pollution</subject><subject>Reference Standards</subject><subject>Reproducibility of Results</subject><subject>Sensitivity and Specificity</subject><subject>Spectrophotometry, Atomic - methods</subject><issn>0304-3894</issn><issn>1873-3336</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkc2O0zAQxy0EYsvCI4BygRMp44_E8QlVZRdWWmmRgLPlOBPVVT6K7e4qnHgmHoknwaERHCuNZB9-__F4foS8pLCmQMt3-_V-Z370Jq4ZgFzPpYpHZEUryXPOefmYrICDyHmlxAV5FsIeAKgsxFNyQWVVgCrpiowfMKLv3WCiG4dsbLMdmvsp6zGaLmT1lN1sP-d3V18yMzTZdb7ZpFubItnBox0Hi0P0p-yDi7uMvWW_f_7Ka3eYvGum7m8M_RR3fgxuwOfkSZsa44vlvCTfrq--bj_lt3cfb7ab29yKooi5bdqaoTDKtKUEFGVtba041I0UwlAQitYoW2WhbEwlG8OEwRIEZ2VRVxXjl-TNqe_Bj9-PGKLuXbDYdWbA8Ri0BAElVedBzjgTUqqzIFVlBZLNHYsTaNOXg8dWH7zrjZ80BT2703u9uNOzOz2XKlLu1fLAse6x-Z9aZCXg9QKYYE3XejNYF_5xDBhN25knfX_iMC343qHXwTpMqhqXnEXdjO7MKH8A4cq7GQ</recordid><startdate>20080415</startdate><enddate>20080415</enddate><creator>Feist, Barbara</creator><creator>Mikula, Barbara</creator><creator>Pytlakowska, Katarzyna</creator><creator>Puzio, Bozena</creator><creator>Buhl, Franciszek</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7TV</scope><scope>7U7</scope><scope>C1K</scope><scope>8FD</scope><scope>FR3</scope><scope>KR7</scope><scope>7X8</scope></search><sort><creationdate>20080415</creationdate><title>Determination of heavy metals by ICP-OES and F-AAS after preconcentration with 2,2′-bipyridyl and erythrosine</title><author>Feist, Barbara ; Mikula, Barbara ; Pytlakowska, Katarzyna ; Puzio, Bozena ; Buhl, Franciszek</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c455t-cdfb2e4a9af670e46bccb930bd744a10491be7f9c06da87da24ae6043265b8823</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>2,2'-Dipyridyl - chemistry</topic><topic>2,2′-Bipyridyl</topic><topic>Applied sciences</topic><topic>Calibration</topic><topic>Chemical Precipitation</topic><topic>Co-precipitation</topic><topic>Erythrosine</topic><topic>Erythrosine - chemistry</topic><topic>Exact sciences and technology</topic><topic>F-AAS</topic><topic>Heavy metals</topic><topic>ICP-OES</topic><topic>Lycopersicon esculentum</topic><topic>Metals, Heavy - analysis</topic><topic>Plant materials</topic><topic>Pollution</topic><topic>Reference Standards</topic><topic>Reproducibility of Results</topic><topic>Sensitivity and Specificity</topic><topic>Spectrophotometry, Atomic - methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Feist, Barbara</creatorcontrib><creatorcontrib>Mikula, Barbara</creatorcontrib><creatorcontrib>Pytlakowska, Katarzyna</creatorcontrib><creatorcontrib>Puzio, Bozena</creatorcontrib><creatorcontrib>Buhl, Franciszek</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Pollution Abstracts</collection><collection>Toxicology Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Civil Engineering Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of hazardous materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Feist, Barbara</au><au>Mikula, Barbara</au><au>Pytlakowska, Katarzyna</au><au>Puzio, Bozena</au><au>Buhl, Franciszek</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of heavy metals by ICP-OES and F-AAS after preconcentration with 2,2′-bipyridyl and erythrosine</atitle><jtitle>Journal of hazardous materials</jtitle><addtitle>J Hazard Mater</addtitle><date>2008-04-15</date><risdate>2008</risdate><volume>152</volume><issue>3</issue><spage>1122</spage><epage>1129</epage><pages>1122-1129</pages><issn>0304-3894</issn><eissn>1873-3336</eissn><coden>JHMAD9</coden><abstract>The applicability of 2,2′-bipyridyl and erythrosine co-precipitation method for the separation and preconcentration of some heavy metals, such as Cd, Co, Cu, Ni, Pb and Zn in actual samples for their determination by ICP-OES and F-AAS was studied. Experimental conditions influencing the recovery of the investigated metals, such as pH, molar ratio of 2,2′-bipyridyl to erythrosine, the effect of time on co-precipitation were optimized. The analytical characteristics of the method (e.g. limit of detection, sensitivity, linear range and preconcentration factor) were obtained. The limits of detection LOD (ng
mL
−1) of the ICP-OES (F-AAS) method were: Cd: 4.0 (7.75), Co: 3.1 (57.2), Cu: 18 (10.3), Ni 21.3 (32.8), Pb: 35.9 (29.2) and Zn: 10.2 (6.90). The recovery of all the elements tested was more than 93%. The influence of inorganic matrix was examined. The proposed method was applied to determination of Cd, Co, Cu, Ni, Pb and Zn in vegetables and certified reference material (NCS ZC85006 Tomato).</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>17850961</pmid><doi>10.1016/j.jhazmat.2007.07.095</doi><tpages>8</tpages></addata></record> |
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| subjects | 2,2'-Dipyridyl - chemistry 2,2′-Bipyridyl Applied sciences Calibration Chemical Precipitation Co-precipitation Erythrosine Erythrosine - chemistry Exact sciences and technology F-AAS Heavy metals ICP-OES Lycopersicon esculentum Metals, Heavy - analysis Plant materials Pollution Reference Standards Reproducibility of Results Sensitivity and Specificity Spectrophotometry, Atomic - methods |
| title | Determination of heavy metals by ICP-OES and F-AAS after preconcentration with 2,2′-bipyridyl and erythrosine |
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