Identification and quantification of alkene-based drilling fluids in crude oils by comprehensive two-dimensional gas chromatography with flame ionization detection
Comprehensive two-dimensional gas chromatography with flame ionization detection (GC × GC-FID) was used to measure alkene-based drilling fluids in crude oils. Compared to one-dimensional gas chromatography, GC × GC-FID is more robust for detecting alkenes due to the increased resolution afforded by...
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| Veröffentlicht in: | Journal of Chromatography A 2007-04, Vol.1148 (1), p.100-107 |
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| container_end_page | 107 |
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| container_issue | 1 |
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| container_title | Journal of Chromatography A |
| container_volume | 1148 |
| creator | Reddy, Christopher M. Nelson, Robert K. Sylva, Sean P. Xu, Li Peacock, Emily A. Raghuraman, Bhavani Mullins, Oliver C. |
| description | Comprehensive two-dimensional gas chromatography with flame ionization detection (GC
×
GC-FID) was used to measure alkene-based drilling fluids in crude oils. Compared to one-dimensional gas chromatography, GC
×
GC-FID is more robust for detecting alkenes due to the increased resolution afforded by second dimension separations. Using GC
×
GC-FID to analyze four oil samples from one reservoir contaminated with the same drilling fluid, C
15, C
16, C
17, C
18 and C
20 alkenes were identified. The drilling fluid that contaminated these samples also differed from another commercially obtained fluid, which only contained C
16 and C
18 alkenes. These results should motivate the petroleum industry to consider GC
×
GC-FID for measuring drilling fluids. |
| doi_str_mv | 10.1016/j.chroma.2007.03.001 |
| format | Article |
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×
GC-FID) was used to measure alkene-based drilling fluids in crude oils. Compared to one-dimensional gas chromatography, GC
×
GC-FID is more robust for detecting alkenes due to the increased resolution afforded by second dimension separations. Using GC
×
GC-FID to analyze four oil samples from one reservoir contaminated with the same drilling fluid, C
15, C
16, C
17, C
18 and C
20 alkenes were identified. The drilling fluid that contaminated these samples also differed from another commercially obtained fluid, which only contained C
16 and C
18 alkenes. These results should motivate the petroleum industry to consider GC
×
GC-FID for measuring drilling fluids.</description><identifier>ISSN: 0021-9673</identifier><identifier>DOI: 10.1016/j.chroma.2007.03.001</identifier><identifier>PMID: 17376464</identifier><identifier>CODEN: JOCRAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Alkenes ; Alkenes - chemistry ; Analytical chemistry ; Applied sciences ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Chromatography, Gas - methods ; Chromatography, Gel ; Crude oil, natural gas and petroleum products ; Drilling fluids ; Energy ; Exact sciences and technology ; Flame Ionization - methods ; Fuels ; Gas chromatographic methods ; Gas Chromatography-Mass Spectrometry ; GC × GC ; Models, Theoretical ; Olefins ; Petroleum - analysis ; Petroleum exploration ; Prospecting and production of crude oil, natural gas, oil shales and tar sands ; Reproducibility of Results</subject><ispartof>Journal of Chromatography A, 2007-04, Vol.1148 (1), p.100-107</ispartof><rights>2007 Elsevier B.V.</rights><rights>2007 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-958c305915134a5a0e4608570d1de547bd06994155f18f6122a681e3f40d2bb73</citedby><cites>FETCH-LOGICAL-c390t-958c305915134a5a0e4608570d1de547bd06994155f18f6122a681e3f40d2bb73</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.chroma.2007.03.001$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3536,27903,27904,45974</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18660912$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17376464$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Reddy, Christopher M.</creatorcontrib><creatorcontrib>Nelson, Robert K.</creatorcontrib><creatorcontrib>Sylva, Sean P.</creatorcontrib><creatorcontrib>Xu, Li</creatorcontrib><creatorcontrib>Peacock, Emily A.</creatorcontrib><creatorcontrib>Raghuraman, Bhavani</creatorcontrib><creatorcontrib>Mullins, Oliver C.</creatorcontrib><title>Identification and quantification of alkene-based drilling fluids in crude oils by comprehensive two-dimensional gas chromatography with flame ionization detection</title><title>Journal of Chromatography A</title><addtitle>J Chromatogr A</addtitle><description>Comprehensive two-dimensional gas chromatography with flame ionization detection (GC
×
GC-FID) was used to measure alkene-based drilling fluids in crude oils. Compared to one-dimensional gas chromatography, GC
×
GC-FID is more robust for detecting alkenes due to the increased resolution afforded by second dimension separations. Using GC
×
GC-FID to analyze four oil samples from one reservoir contaminated with the same drilling fluid, C
15, C
16, C
17, C
18 and C
20 alkenes were identified. The drilling fluid that contaminated these samples also differed from another commercially obtained fluid, which only contained C
16 and C
18 alkenes. These results should motivate the petroleum industry to consider GC
×
GC-FID for measuring drilling fluids.</description><subject>Alkenes</subject><subject>Alkenes - chemistry</subject><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Chromatography, Gas - methods</subject><subject>Chromatography, Gel</subject><subject>Crude oil, natural gas and petroleum products</subject><subject>Drilling fluids</subject><subject>Energy</subject><subject>Exact sciences and technology</subject><subject>Flame Ionization - methods</subject><subject>Fuels</subject><subject>Gas chromatographic methods</subject><subject>Gas Chromatography-Mass Spectrometry</subject><subject>GC × GC</subject><subject>Models, Theoretical</subject><subject>Olefins</subject><subject>Petroleum - analysis</subject><subject>Petroleum exploration</subject><subject>Prospecting and production of crude oil, natural gas, oil shales and tar sands</subject><subject>Reproducibility of Results</subject><issn>0021-9673</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kc9u3CAQxn1o1aRp3iCquLQ3u4Oxwb5UqqLmjxSpl_aMMIx32WLYgJ1o-zp90bDySumpJ2D0m2-G7yuKKwoVBcq_7Cq9jWFSVQ0gKmAVAH1TnAPUtOy5YGfF-5R2uShA1O-KMyqY4A1vzou_9wb9bEer1WyDJ8ob8riof0thJMr9Ro_loBIaYqJ1zvoNGd1iTSLWEx0XgyRYl8hwIDpM-4hb9Mk-IZmfQ2nsdHwFrxzZqETWbeewiWq_PZBnO2-zmpqQZMb-WecanFEfbx-Kt6NyCS9P50Xx6-b7z-u78uHH7f31t4dSsx7msm87zaDtaUtZo1oF2HDoWgGGGmwbMRjgfd_Qth1pN3Ja14p3FNnYgKmHQbCL4vOqu4_hccE0y8kmjc4pj2FJUgBrOGcsg80K6hhSijjKfbSTigdJQR4DkTu5flEeA5HAZPY-t3086S_DhOa16ZRGBj6dAJW0cmNUXtv0ynWcQ0_rzH1dOcxuPFmMMmmLXqOxMVsmTbD_3-QFy_iwyA</recordid><startdate>20070427</startdate><enddate>20070427</enddate><creator>Reddy, Christopher M.</creator><creator>Nelson, Robert K.</creator><creator>Sylva, Sean P.</creator><creator>Xu, Li</creator><creator>Peacock, Emily A.</creator><creator>Raghuraman, Bhavani</creator><creator>Mullins, Oliver C.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20070427</creationdate><title>Identification and quantification of alkene-based drilling fluids in crude oils by comprehensive two-dimensional gas chromatography with flame ionization detection</title><author>Reddy, Christopher M. ; Nelson, Robert K. ; Sylva, Sean P. ; Xu, Li ; Peacock, Emily A. ; Raghuraman, Bhavani ; Mullins, Oliver C.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-958c305915134a5a0e4608570d1de547bd06994155f18f6122a681e3f40d2bb73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Alkenes</topic><topic>Alkenes - chemistry</topic><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Chromatography, Gas - methods</topic><topic>Chromatography, Gel</topic><topic>Crude oil, natural gas and petroleum products</topic><topic>Drilling fluids</topic><topic>Energy</topic><topic>Exact sciences and technology</topic><topic>Flame Ionization - methods</topic><topic>Fuels</topic><topic>Gas chromatographic methods</topic><topic>Gas Chromatography-Mass Spectrometry</topic><topic>GC × GC</topic><topic>Models, Theoretical</topic><topic>Olefins</topic><topic>Petroleum - analysis</topic><topic>Petroleum exploration</topic><topic>Prospecting and production of crude oil, natural gas, oil shales and tar sands</topic><topic>Reproducibility of Results</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Reddy, Christopher M.</creatorcontrib><creatorcontrib>Nelson, Robert K.</creatorcontrib><creatorcontrib>Sylva, Sean P.</creatorcontrib><creatorcontrib>Xu, Li</creatorcontrib><creatorcontrib>Peacock, Emily A.</creatorcontrib><creatorcontrib>Raghuraman, Bhavani</creatorcontrib><creatorcontrib>Mullins, Oliver C.</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Reddy, Christopher M.</au><au>Nelson, Robert K.</au><au>Sylva, Sean P.</au><au>Xu, Li</au><au>Peacock, Emily A.</au><au>Raghuraman, Bhavani</au><au>Mullins, Oliver C.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Identification and quantification of alkene-based drilling fluids in crude oils by comprehensive two-dimensional gas chromatography with flame ionization detection</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>2007-04-27</date><risdate>2007</risdate><volume>1148</volume><issue>1</issue><spage>100</spage><epage>107</epage><pages>100-107</pages><issn>0021-9673</issn><coden>JOCRAM</coden><abstract>Comprehensive two-dimensional gas chromatography with flame ionization detection (GC
×
GC-FID) was used to measure alkene-based drilling fluids in crude oils. Compared to one-dimensional gas chromatography, GC
×
GC-FID is more robust for detecting alkenes due to the increased resolution afforded by second dimension separations. Using GC
×
GC-FID to analyze four oil samples from one reservoir contaminated with the same drilling fluid, C
15, C
16, C
17, C
18 and C
20 alkenes were identified. The drilling fluid that contaminated these samples also differed from another commercially obtained fluid, which only contained C
16 and C
18 alkenes. These results should motivate the petroleum industry to consider GC
×
GC-FID for measuring drilling fluids.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>17376464</pmid><doi>10.1016/j.chroma.2007.03.001</doi><tpages>8</tpages></addata></record> |
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| language | eng |
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| source | MEDLINE; Elsevier ScienceDirect Journals Complete |
| subjects | Alkenes Alkenes - chemistry Analytical chemistry Applied sciences Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Gas - methods Chromatography, Gel Crude oil, natural gas and petroleum products Drilling fluids Energy Exact sciences and technology Flame Ionization - methods Fuels Gas chromatographic methods Gas Chromatography-Mass Spectrometry GC × GC Models, Theoretical Olefins Petroleum - analysis Petroleum exploration Prospecting and production of crude oil, natural gas, oil shales and tar sands Reproducibility of Results |
| title | Identification and quantification of alkene-based drilling fluids in crude oils by comprehensive two-dimensional gas chromatography with flame ionization detection |
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